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The structure and morphology of the binary electrodes were characterized by XRD, XPS, and SEM. Electrochemical studies (cyclic voltammetry and electrochemical impedance spectroscopy) revealed that the binary materials exhibited distinct electrochemical behavior for energy storage and water splitting. In fact, whereas Ni-Gly\/ZIF-67 was used as an electrode material for energy storage, Ni-Gly\/CoFe-ZIF-67 was used as an electrocatalyst for water splitting. The Ni-Gly\/ZIF-67 electrode material achieved a high specific capacity of 106.9 mA h g\u20131 at 1.0 A g\u20131 and retained 71.6% of its capacity after 5000 cycles, combining pseudocapacitive\/battery-type behavior. Furthermore, a symmetric supercapacitor device was assembled, achieving maximum energy and power densities of 0.765 W h kg\u20131 and 6076 W kg\u20131, respectively. The Ni-Gly\/CoFe-ZIF-67 electrode material exhibited excellent oxygen evolution reaction (OER) activity, with an overpotential of 430 mV at 10 mA cm\u20132, a Tafel slope of 108 mV dec\u20131, and stable operation for 10 h. These results demonstrate a synergism between MOF- and Ni-Gly-derived frameworks, providing valuable insights for the rational design of sustainable multifunctional electrodes for integrated energy storage and conversion systems.<\/jats:p>","DOI":"10.1021\/acsomega.6c06663","type":"journal-article","created":{"date-parts":[[2026,9,23]],"date-time":"2026-09-23T16:02:40Z","timestamp":1790179360000},"page":"59762-59772","source":"Crossref","is-referenced-by-count":0,"title":["Nickel-Glycerolate\/MOF-Based\nElectrode Materials for\nEnergy Storage and Water-Splitting Applications"],"prefix":"10.1021","volume":"11","author":[{"given":"Iara","family":"Schlag Dura\u0303es Campos","sequence":"first","affiliation":[{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8140-7889","authenticated-orcid":true,"given":"Abelardo","family":"Grego\u0301rio Banze","sequence":"additional","affiliation":[{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tarso Leandro","family":"Bastos","sequence":"additional","affiliation":[{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]},{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Raylander Rodrigues","family":"Silva","sequence":"additional","affiliation":[{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0006-5831-1700","authenticated-orcid":true,"given":"Nie\u0301lcio Batista da Silva","family":"Filho","sequence":"additional","affiliation":[{"name":"Federal University of Jequitinhonha and Mucuri\u2019s Valley , , Rodovia MGT 367, Km 583, 5000, Alto da Jacuba , , ,","place":["Diamantina, MG, Brazil, 39100-000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Leonardo Morais","family":"Da Silva","sequence":"additional","affiliation":[{"name":"Federal University of Jequitinhonha and Mucuri\u2019s Valley , , Rodovia MGT 367, Km 583, 5000, Alto da Jacuba , , ,","place":["Diamantina, MG, Brazil, 39100-000"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Josue\u0301","family":"Martins Gonc\u0327alves","sequence":"additional","affiliation":[{"name":"Mackenzie Presbyterian Institute , , Consolac\u0327a\u0303o Street 930 , , ,","place":["Sa\u0303o Paulo, Sa\u0303o Paulo, Brazil, 01302-907"]},{"name":"Mackenzie Presbyterian University , , Consolac\u0327a\u0303o Street 930 , , ,","place":["Sa\u0303o Paulo, Sa\u0303o Paulo, Brazil, 01302-907"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3227-0190","authenticated-orcid":true,"given":"Paulo Roberto","family":"Martins","sequence":"additional","affiliation":[{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]},{"name":"Federal University of Goias , , Av. Esperanc\u0327a S\/N , , ,","place":["Goia\u0302nia, GO, Brazil, 74690-900"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,23]]},"reference":[{"issue":"August","key":"2026100610490095800_cit1","doi-asserted-by":"publisher","first-page":"2179","DOI":"10.1016\/j.egyr.2024.08.019","article-title":"Navigating challenges\nin large-scale\nrenewable energy storage: Barriers, solutions, and innovations","volume":"12","author":"Jafarizadeh","year":"2024","journal-title":"Energy Reports"},{"issue":"March","key":"2026100610490095800_cit2","doi-asserted-by":"publisher","first-page":"142146","DOI":"10.1016\/j.electacta.2023.142146","article-title":"Ultrathin\n\u03b1-Ni(OH)2 nanosheets coated on MOF-derived\nFe2O3 nanorods as a potential electrode for solid-state hybrid supercapattery\ndevice","volume":"447","author":"Babu","year":"2023","journal-title":"Electrochim. 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Nano Mater."},{"issue":"28","key":"2026100610490095800_cit6","doi-asserted-by":"publisher","first-page":"12058","DOI":"10.1039\/D1NR01669E","article-title":"ZIF-67-based\ncatalysts for oxygen evolution reaction","volume":"13","author":"Wen","year":"2021","journal-title":"Nanoscale"},{"issue":"2","key":"2026100610490095800_cit7","doi-asserted-by":"publisher","first-page":"1190","DOI":"10.1002\/er.5807","article-title":"Recent advancements\nin MOF-based catalysts for applications in electrochemical\nand photoelectrochemical water splitting: A review","volume":"45","author":"Ali","year":"2021","journal-title":"Int. J. Energy Res."},{"key":"2026100610490095800_cit8","doi-asserted-by":"publisher","first-page":"100692","DOI":"10.1016\/j.apmt.2020.100692","article-title":"Advances and Challenges\nof Fe-MOFs Based Materials\nas Electrocatalysts for Water Splitting","volume":"20","author":"Yang","year":"2020","journal-title":"Appl.\nMater. 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Alloys Compd."},{"issue":"25","key":"2026100610490095800_cit16","doi-asserted-by":"publisher","first-page":"14243","DOI":"10.1002\/ange.202104366","article-title":"Large-Area Crystalline\nZeolitic Imidazolate Framework Thin Films","volume":"133","author":"Chen","year":"2021","journal-title":"Angew.\nChem."},{"issue":"May","key":"2026100610490095800_cit17","doi-asserted-by":"publisher","first-page":"107985","DOI":"10.1016\/j.est.2023.107985","article-title":"Dissipative effects\nin nonideal supercapacitors and batteries","volume":"69","author":"Da Silva","year":"2023","journal-title":"J.\nEnergy Storage"},{"issue":"3","key":"2026100610490095800_cit18","doi-asserted-by":"publisher","first-page":"1286","DOI":"10.1021\/acs.chemrev.0c00487","article-title":"Power\nof Infrared and\nRaman Spectroscopies to Characterize Metal-Organic Frameworks and\nInvestigate Their Interaction with Guest Molecules","volume":"121","author":"Hadjiivanov","year":"2021","journal-title":"Chem. 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China Chem."},{"issue":"February 2020","key":"2026100610490095800_cit22","doi-asserted-by":"publisher","first-page":"105514","DOI":"10.1016\/j.nanoen.2020.105514","article-title":"\u201cThe Fe Effect\u201d: A\nreview unveiling the critical roles of Fe in enhancing OER activity\nof Ni and Co based catalysts","volume":"80","author":"Anantharaj","year":"2021","journal-title":"Nano Energy"},{"issue":"June","key":"2026100610490095800_cit23","doi-asserted-by":"publisher","first-page":"1","DOI":"10.1038\/srep11095","article-title":"Synergistic\neffect between ultra-small\nnickel hydroxide nanoparticles and reduced graphene oxide sheets for\nthe application in high-performance asymmetric supercapacitor","volume":"5","author":"Liu","year":"2015","journal-title":"Sci. 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Energy Storage"},{"key":"2026100610490095800_cit31","doi-asserted-by":"publisher","first-page":"546","DOI":"10.1016\/j.jcis.2022.09.107","article-title":"In situ growth of ZIF-67-derived\nnickel-cobalt-manganese\nhydroxides on 2D V2CTx MXene for dual-functional orientation as high-performance\nasymmetric supercapacitor and electrochemical hydroquinone sensor","volume":"629","author":"Yu","year":"2023","journal-title":"J. Colloid Interface Sci."},{"issue":"September","key":"2026100610490095800_cit32","doi-asserted-by":"publisher","first-page":"116540","DOI":"10.1016\/j.synthmet.2020.116540","article-title":"Decoration\nof metal organic frameworks\nwith Fe2O3 for enhancing electrochemical performance of ZIF-(67 and\n8) in energy storage application","volume":"269","author":"Chameh","year":"2020","journal-title":"Synth. 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Hydrogen\nEnergy"},{"issue":"3","key":"2026100610490095800_cit35","doi-asserted-by":"publisher","first-page":"896","DOI":"10.1039\/D5NA00246J","article-title":"Two-dimensional Fe-MOF\nand bimetallic NiFe-MOFs with different Ni: Fe ratios for superior\nelectrochemical performance in supercapacitor applications","volume":"8","author":"Mohamedien","year":"2026","journal-title":"Nanoscale Adv."},{"issue":"6","key":"2026100610490095800_cit36","doi-asserted-by":"publisher","first-page":"3448","DOI":"10.1021\/acs.nanolett.5b04965","article-title":"Supercapacitors Based on Three-Dimensional\nHierarchical Graphene Aerogels with Periodic Macropores","volume":"16","author":"Zhu","year":"2016","journal-title":"Nano Lett."},{"issue":"13","key":"2026100610490095800_cit37","doi-asserted-by":"publisher","first-page":"3646","DOI":"10.1002\/slct.201900061","article-title":"Surface-Modification-Assisted\nConstruction\nof Hierarchical Double-Walled MnO 2 Hollow Nanofibers for High-Performance\nSupercapacitor Electrode","volume":"4","author":"Lu","year":"2019","journal-title":"ChemistrySelect"},{"issue":"November 2018","key":"2026100610490095800_cit38","doi-asserted-by":"publisher","first-page":"632","DOI":"10.1016\/j.est.2018.12.025","article-title":"Metal-organic frameworks\nfor energy storage devices: Batteries and supercapacitors","volume":"21","author":"Mehtab","year":"2019","journal-title":"J. Energy Storage"},{"issue":"39","key":"2026100610490095800_cit39","doi-asserted-by":"publisher","first-page":"1902007","DOI":"10.1002\/aenm.201902007","article-title":"Energy Storage Data\nReporting in Perspective\u2500Guidelines\nfor Interpreting the Performance of Electrochemical Energy Storage\nSystems","volume":"9","author":"Mathis","year":"2019","journal-title":"Adv. Energy Mater."},{"issue":"7","key":"2026100610490095800_cit40","doi-asserted-by":"publisher","first-page":"e202216477","DOI":"10.1002\/anie.202216477","article-title":"Non-Kinetic\nEffects Convolute Activity and Tafel Analysis for the Alkaline Oxygen\nEvolution Reaction on NiFeOOH Electrocatalysts","volume":"62","author":"van der Heijden","year":"2023","journal-title":"Angew. Chemie - Int. Ed"},{"key":"2026100610490095800_cit41","doi-asserted-by":"publisher","first-page":"115035","DOI":"10.1016\/j.jelechem.2021.115035","article-title":"Morphology-controllable nanocrystal \u03b2-Ni(OH)2\/NF\ndesigned by hydrothermal etching method as high-efficiency electrocatalyst\nfor overall water splitting","volume":"882","author":"Yang","year":"2021","journal-title":"J. Electroanal.\nChem."},{"issue":"1","key":"2026100610490095800_cit42","doi-asserted-by":"publisher","first-page":"1","DOI":"10.1038\/s41598-026-49517-9","article-title":"Synergistic interface\nengineering of Ni-integrated Co-ZIF67 on two-dimensional MXene for\nenhanced oxygen evolution reaction","volume":"16","author":"Pashajavid","year":"2026","journal-title":"Sci. Rep"},{"issue":"4","key":"2026100610490095800_cit43","doi-asserted-by":"publisher","first-page":"2300301","DOI":"10.1002\/aesr.202300301","article-title":"Unraveling the Electrical,\nDielectric, and Electrocatalytic Properties of Bimetallic Cobalt-Based\nMetal\u2013Organic Frameworks","volume":"6","author":"Godara","year":"2025","journal-title":"Adv. Energy\nSustain Res."}],"container-title":["ACS Omega"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/pubs.acs.org\/doi\/pdf\/10.1021\/acsomega.6c06663","content-type":"application\/pdf","content-version":"vor","intended-application":"unspecified"},{"URL":"https:\/\/pubs.acs.org\/acsodf\/article-pdf\/11\/39\/59762\/68624741\/acsomega.6c06663.pdf","content-type":"application\/pdf","content-version":"vor","intended-application":"syndication"},{"URL":"https:\/\/pubs.acs.org\/acsodf\/article-pdf\/11\/39\/59762\/68624741\/acsomega.6c06663.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2026,10,6]],"date-time":"2026-10-06T15:30:51Z","timestamp":1791300651000},"score":1,"resource":{"primary":{"URL":"https:\/\/pubs.acs.org\/acsodf\/article\/11\/39\/59762\/5436850\/Nickel-Glycerolate-MOF-Based-Electrode-Materials"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2026,9,23]]},"references-count":43,"journal-issue":{"issue":"39","published-online":{"date-parts":[[2026,9,23]]},"published-print":{"date-parts":[[2026,10,6]]}},"URL":"https:\/\/doi.org\/10.1021\/acsomega.6c06663","relation":{},"ISSN":["2470-1343"],"issn-type":[{"value":"2470-1343","type":"electronic"}],"subject":[],"published":{"date-parts":[[2026,9,23]]}}}