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The complex Na[3,3\u2032-Co(8-O(CH2CH2O)2C(O)-(CH2\u2013pyrene)(1,2-C2B9H10)(1\u2032,2\u2032-C2B9H11], denoted as Na[3], was obtained via a ring-opening reaction of a cyclic oxonium derivative with pyreneacetic acid. Subsequent cation exchange yielded the tetramethylammonium salt, [N(CH3)4][3,3\u2032-Co(8-O(CH2CH2O)2C(O)(CH2\u2013pyrene-1,2-C2B9H10)(1,2-C2B9H11)], [N(CH3)4][3]. Electrochemical analysis revealed irreversible oxidation peaks for the pyrene moiety alongside well-defined Co(IV)\/Co(III) and Co(III)\/Co(II) redox couples. Noncovalent anchoring of [Na][3] onto GO produced the hybrid material GO@3, which was thoroughly characterized by TEM, SEM, XPS, UV\u2013vis, and DPV. GO@3 exhibited the narrowest optical and electrochemical bandgaps among the studied species. All complexes demonstrated exceptional catalytic efficiency and selectivity for the UVA-driven photooxidation of alcohols in water. Notably, homogeneous Na[3] achieved high conversions at a remarkably low loading of 0.01 mol %. While the insoluble [N(CH3)4][3], acted as a robust heterogeneous catalyst, the hybrid GO@3 surpassed the activity of the homogeneous system, showing enhanced performance in shorter reaction times. This enhancement is attributed to the synergistic role of GO in facilitating electron transfer and suppressing charge recombination. GO@3 was easily recovered by filtration and reused over six cycles without loss of activity, reaching turnover numbers (TON) exceeding 45,000.<\/jats:p>","DOI":"10.1021\/acsomega.6c07608","type":"journal-article","created":{"date-parts":[[2026,9,11]],"date-time":"2026-09-11T15:01:56Z","timestamp":1789138916000},"page":"56419-56433","source":"Crossref","is-referenced-by-count":0,"title":["Pyrene-Functionalized\n                    <i>o<\/i>\n                    -COSAN\nNoncovalently Anchored onto Graphene Oxide for Advanced Photocatalytic\nAlcohol Oxidation"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-2034-0593","authenticated-orcid":true,"given":"Syrine","family":"Affe\u0300s","sequence":"first","affiliation":[{"name":"Universitat de Girona , , C\/M. Aure\u0300lia Capmany, 69 , ,","place":["Girona, Spain, E-17003"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nabila","family":"Mimouni","sequence":"additional","affiliation":[{"name":"Universitat de Girona , , C\/M. Aure\u0300lia Capmany, 69 , ,","place":["Girona, Spain, E-17003"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Isabel","family":"Guerrero","sequence":"additional","affiliation":[{"name":"Institut de Ciencia de Materials de Barcelona (ICMAB-CSIC) , Carrer dels Til\u00b7lers , ,","place":["Cerdanyola del Valle\u0300s, Spain, 08193"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4582-5148","authenticated-orcid":true,"given":"Rosario","family":"Nu\u0301n\u0303ez","sequence":"additional","affiliation":[{"name":"Institut de Ciencia de Materials de Barcelona (ICMAB-CSIC) , Carrer dels Til\u00b7lers , ,","place":["Cerdanyola del Valle\u0300s, Spain, 08193"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ahlem","family":"Kabadou","sequence":"additional","affiliation":[{"name":"Universite\u0301 de Sfax , , ,","place":["Sfax, Tunisie, 3029"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Clara","family":"Vin\u0303as","sequence":"additional","affiliation":[{"name":"Institut de Ciencia de Materials de Barcelona (ICMAB-CSIC) , Carrer dels Til\u00b7lers , ,","place":["Cerdanyola del Valle\u0300s, Spain, 08193"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3010-2417","authenticated-orcid":true,"given":"Francesc","family":"Teixidor","sequence":"additional","affiliation":[{"name":"Institut de Ciencia de Materials de Barcelona (ICMAB-CSIC) , Carrer dels Til\u00b7lers , ,","place":["Cerdanyola del Valle\u0300s, Spain, 08193"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4805-8394","authenticated-orcid":true,"given":"Isabel","family":"Romero","sequence":"additional","affiliation":[{"name":"Universitat de Girona , , C\/M. Aure\u0300lia Capmany, 69 , ,","place":["Girona, Spain, E-17003"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,11]]},"reference":[{"key":"2026092211031463200_cit1","volume-title":"Oxidations in Organic\nChemistry","author":"Hudlicky","year":"1990"},{"key":"2026092211031463200_cit2","doi-asserted-by":"publisher","first-page":"774","DOI":"10.1021\/ar010075n","article-title":"Green, Catalytic\nOxidations\nof Alcohols","volume":"35","author":"Sheldon","year":"2002","journal-title":"Acc. Chem. Res."},{"key":"2026092211031463200_cit3","volume-title":"Oxidation of Alcohols\nto Aldehydes and Ketones","author":"Tojo","year":"2006"},{"key":"2026092211031463200_cit4","doi-asserted-by":"publisher","first-page":"4022","DOI":"10.1021\/cr050193e","article-title":"Hydrogen Production by Molecular\nCatalysis","volume":"107","author":"Esswein","year":"2007","journal-title":"Chem. 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Rev."},{"key":"2026092211031463200_cit22","volume-title":"Handbook of Boron Science: With Applications in\nOrganometallics,\nCatalysis, Materials and Medicine","author":"Hosmane","year":"2018"},{"key":"2026092211031463200_cit23","doi-asserted-by":"publisher","DOI":"10.1016\/j.jece.2025.119643","article-title":"Metallacarborane-functionalized graphene oxide as a\nrecyclable UVC\/UVA photocatalyst for micropollutant removal","volume":"13","author":"Mimouni","year":"2025","journal-title":"J. Environ. Chem. Eng."},{"issue":"20","key":"2026092211031463200_cit24","doi-asserted-by":"publisher","first-page":"9396","DOI":"10.1021\/jacs.0c02228","article-title":"Too persistent to give up: Aromaticity\nin boron clusters\nsurvives radical structural changes","volume":"142","author":"Poater","year":"2020","journal-title":"J. Am.\nChem. Soc."},{"key":"2026092211031463200_cit25","doi-asserted-by":"publisher","first-page":"5027","DOI":"10.1002\/chem.201905395","article-title":"Metallacarboranes\nas Photoredox Catalysts in Water","volume":"26","author":"Guerrero","year":"2020","journal-title":"Chem. - Eur.\nJ."},{"key":"2026092211031463200_cit26","doi-asserted-by":"publisher","first-page":"8898","DOI":"10.1021\/acs.inorgchem.1c00751","article-title":"Aqueous Persistent\nNoncovalent Ion-Pair Cooperative Coupling in a Ruthenium Cobaltabis(dicarbollide)\nSystem as a Highly Efficient Photoredox Oxidation Catalyst","volume":"60","author":"Guerrero","year":"2021","journal-title":"Inorg. Chem."},{"key":"2026092211031463200_cit27","doi-asserted-by":"publisher","first-page":"10123","DOI":"10.1039\/D1GC03119H","article-title":"A stand-alone\nCobalt\nbis(dicarbollide) Photoredox Catalyst Epoxidates Alkenes in Water\nat Extremely Low Catalyst Load","volume":"23","author":"Guerrero","year":"2021","journal-title":"Green Chem."},{"issue":"10","key":"2026092211031463200_cit28","doi-asserted-by":"publisher","DOI":"10.3390\/molecules29102378","article-title":"Unveiling Non-Covalent\nInteractions in Novel Cooperative Photoredox Systems for Efficient\nAlkene Oxidation in Water","volume":"29","author":"Guerrero","year":"2024","journal-title":"Molecules"},{"issue":"4","key":"2026092211031463200_cit29","doi-asserted-by":"publisher","first-page":"879","DOI":"10.1021\/ja01006a008","article-title":"pi.-Dicarbollyl\nderivatives of the transition metals. Metallocene analogs","volume":"90","author":"Hawthorne","year":"1968","journal-title":"J. Am. Chem. Soc."},{"key":"2026092211031463200_cit30","doi-asserted-by":"publisher","first-page":"7188","DOI":"10.1039\/D2DT01015A","article-title":"Water soluble organometallic small molecules as promising\nantibacterial agents: synthesis, physical\u2013chemical properties\nand biological evaluation to tackle bacterial infections","volume":"51","author":"Bennour","year":"2022","journal-title":"Dalton Trans."},{"key":"2026092211031463200_cit31","doi-asserted-by":"publisher","first-page":"3088","DOI":"10.1002\/anie.201913257","article-title":"Atomistic Simulations\nof COSAN: Amphiphiles without a Head-and-Tail Design Display \u201cHead\nand Tail\u201d Surfactant Behavior","volume":"59","author":"Malaspina","year":"2020","journal-title":"Angew.\nChem., Int. 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Chem., Int. Ed."},{"key":"2026092211031463200_cit38","volume-title":"Carboranes","author":"Grimes","year":"2016","edition":"3"},{"key":"2026092211031463200_cit39","doi-asserted-by":"publisher","first-page":"3318","DOI":"10.1039\/c2cs35441a","article-title":"Methods to Produce\nB\u2013C, B\u2013P, B\u2013N and B\u2013S Bonds in Boron Clusters","volume":"42","author":"Olid","year":"2013","journal-title":"Chem. Soc. 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Syntheses,\nProperties and Structures of Its 8, 8\u2019-\u03bc-Sulfato, 8-Phenyland\n8-Dioxane Derivatives","volume":"62","author":"Ples\u030cek","year":"1997","journal-title":"Collect. Czech. Chem.\nCommun."},{"key":"2026092211031463200_cit43","doi-asserted-by":"publisher","first-page":"3414","DOI":"10.1021\/om030135o","article-title":"Chameleonic capacity of [3, 3 \u2018-Co\n(1, 2-C2B9H11)2]- in coordination. Generation of the highly uncommon S (thioether)\u2212Na bond","volume":"22","author":"Teixidor","year":"2003","journal-title":"Organometallics"},{"issue":"20","key":"2026092211031463200_cit44","doi-asserted-by":"publisher","first-page":"9497","DOI":"10.1021\/ic801139x","article-title":"Metallacarboranes\nas\nbuilding blocks for polyanionic polyarmed aryl-ether materials","volume":"47","author":"Farra\u0300s","year":"2008","journal-title":"Inorg. chem."},{"issue":"23","key":"2026092211031463200_cit45","doi-asserted-by":"publisher","first-page":"4253","DOI":"10.1021\/acs.organomet.0c00315","article-title":"Metallacarborane\nassemblies as effective antimicrobial agents, including a highly potent\nanti-MRSA agent","volume":"39","author":"Romero","year":"2020","journal-title":"Organometallics"},{"issue":"7","key":"2026092211031463200_cit46","doi-asserted-by":"publisher","first-page":"785","DOI":"10.1070\/RCR5000","article-title":"Cyclic oxonium derivatives\nof cobalt and iron bis (dicarbollides) and their use in organic synthesis","volume":"90","author":"Druzina","year":"2021","journal-title":"Russ. 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