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Herein, luminescent platforms (PE-\u00a0g\u00a0-MC-1-X) based on a [Pt(NCN)Cl] complex (NCN = 1,3-bis(benzimidazol-2-yl)benzene derivative bearing two tetraethylene glycol (TEG) chains) (1) anchored onto polyethylene grafted with methacryloyl chloride (PE-\u00a0g\u00a0-MC) by gamma irradiation at different doses (X = 2, 4, 6, and 8 kGy) were synthesized and characterized. Among luminescent platforms, PE-\u00a0g\u00a0-MC-1-8kGy film was studied as a chemosensor for anions, nucleotides, and oxyanions in ethanol\/water (1:1, v\/v). The luminescent polymer exhibited a selective quenching response toward iodide (I\u2013), with a quenching constant (Kq) of 4.67(\u00b10.49) \u00d7 103 M\u20131 and a limit of detection of 6.55(\u00b10.26) ppm. Based on analyses by attenuated total reflectance Fourier-transform infrared (ATR-FTIR) spectroscopy, scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy (SEM-EDS), and X-ray photoelectron spectroscopy (XPS), the binding mode of iodide was attributed to its accumulation within hydrophobic domains of TEG chains through an ion-specific effect, perturbing the electronic environment of the [Pt(NCN)Cl] unit. Sequential addition of mercury (Hg2+) in the presence of hydrochloric acid (HCl) restored the emission intensity, with a limit of detection of 2.40(\u00b10.11) ppm. The luminescent material exhibited reversibility and reusability over multiple I\u2013\/Hg2+ sensing cycles. These results confirm that immobilization of the Pt-NCN complex onto a polymer matrix functionalized by gamma irradiation provides a solid-state sensing platform for the sequential detection of I\u2013 and Hg2+.<\/jats:p>","DOI":"10.1021\/acsomega.6c08055","type":"journal-article","created":{"date-parts":[[2026,9,28]],"date-time":"2026-09-28T09:01:47Z","timestamp":1790586107000},"page":"61966-61983","source":"Crossref","is-referenced-by-count":0,"title":["A Luminescent Pt-NCN\nComplex Anchored onto a Polyethylene\nFilm for Sequential Detection of Iodide and Mercury"],"prefix":"10.1021","volume":"11","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-0689-8806","authenticated-orcid":true,"given":"Josue","family":"Valdes-Garci\u0301a","sequence":"first","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3467-9678","authenticated-orcid":true,"given":"Mireille","family":"Vonlanthen","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7920-1176","authenticated-orcid":true,"given":"Fabia\u0301n","family":"Cue\u0301tara-Guadarrama","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ernesto","family":"Rivera","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Roxana Marisol","family":"Caldero\u0301n-Olvera","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7250-8757","authenticated-orcid":true,"given":"Juan Carlos","family":"Alonso-Huitro\u0301n","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"David","family":"Garcia-Bassoco","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hector Luis","family":"Valde\u0301s-Negri\u0301n","sequence":"additional","affiliation":[{"name":"Instituto de Investigaciones en Materiales, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Guillermina","family":"Burillo","sequence":"additional","affiliation":[{"name":"Instituto de Ciencias Nucleares, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7056-4237","authenticated-orcid":true,"given":"Alejandro","family":"Dorazco-Gonza\u0301lez","sequence":"additional","affiliation":[{"name":"Instituto de Qui\u0301mica, Universidad Nacional Auto\u0301noma de Me\u0301xico , Circuito Exterior, Ciudad Universitaria , ,","place":["Ciudad de Mexico, Me\u0301xico, C.P. 04510"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,9,28]]},"reference":[{"key":"2026101315083863100_cit1","doi-asserted-by":"publisher","first-page":"118417","DOI":"10.1016\/j.watres.2022.118417","article-title":"Iodide sources in the aquatic environment\nand its fate during oxidative water treatment \u2013 A 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Thyroid J."},{"key":"2026101315083863100_cit3","doi-asserted-by":"publisher","DOI":"10.1180\/gbi.2024.6","article-title":"The crucial\nand versatile roles of bacteria in global biogeochemical cycling of\niodine","volume":"1","author":"Jiang","year":"2024","journal-title":"Geo-Bio Interfaces"},{"key":"2026101315083863100_cit4","doi-asserted-by":"publisher","first-page":"162356","DOI":"10.1016\/j.cej.2025.162356","article-title":"Innovative electrooxidation-adsorption technology for\nefficient iodine recovery from ultrahigh Cl\/I ratio underground brine","volume":"512","author":"Yu","year":"2025","journal-title":"Chem. Eng. J."},{"issue":"12","key":"2026101315083863100_cit5","doi-asserted-by":"publisher","first-page":"4469","DOI":"10.3390\/nu13124469","article-title":"Iodine: Its role in thyroid hormone\nbiosynthesis and beyond","volume":"13","author":"Sorrenti","year":"2021","journal-title":"Nutrients"},{"issue":"2","key":"2026101315083863100_cit6","doi-asserted-by":"publisher","first-page":"100168","DOI":"10.1016\/j.advnut.2024.100168","article-title":"Iodine","volume":"15","author":"Brough","year":"2024","journal-title":"Adv. Nutr."},{"issue":"8","key":"2026101315083863100_cit7","doi-asserted-by":"publisher","first-page":"474","DOI":"10.1038\/s41574-024-00983-z","article-title":"Thyroid\nfunction and iodine intake: Global recommendations and relevant dietary\ntrends","volume":"20","author":"Bath","year":"2024","journal-title":"Nat. Rev. Endocrinol."},{"issue":"9","key":"2026101315083863100_cit8","doi-asserted-by":"publisher","first-page":"1488","DOI":"10.1017\/S0007114524000084","article-title":"Study of iodine\ntransport and thyroid hormone levels in the human\nplacenta under different iodine nutritional status","volume":"131","author":"Fu","year":"2024","journal-title":"Br. J. Nutr."},{"key":"2026101315083863100_cit9","doi-asserted-by":"publisher","first-page":"1234918","DOI":"10.3389\/fendo.2023.1234918","article-title":"Effect of iodine nutritional status on the recurrence of hyperthyroidism\nand antithyroid drug efficacy in adult patients with Graves\u2019\ndisease: A systemic review","volume":"14","author":"Xie","year":"2023","journal-title":"Front. Endocrinol."},{"key":"2026101315083863100_cit10","doi-asserted-by":"publisher","first-page":"1239038","DOI":"10.3389\/fendo.2023.1239038","article-title":"Iodine-induced thyroid\ndysfunction: A scientometric study and visualization\nanalysis","volume":"14","author":"Gong","year":"2023","journal-title":"Front. Endocrinol."},{"key":"2026101315083863100_cit11","doi-asserted-by":"publisher","first-page":"127413","DOI":"10.1016\/j.jtemb.2024.127413","article-title":"The association between endothelial\nfunction and autoimmune thyroiditis\ninduced by iodine excess","volume":"83","author":"Wang","year":"2024","journal-title":"J. Trace Elem. Med.\nBiol."},{"issue":"17","key":"2026101315083863100_cit12","doi-asserted-by":"publisher","first-page":"3474","DOI":"10.3390\/nu14173474","article-title":"Iodine\nand iodine deficiency: A comprehensive review\nof a re-emerging issue","volume":"14","author":"Hatch-McChesney","year":"2022","journal-title":"Nutrients"},{"issue":"23","key":"2026101315083863100_cit13","doi-asserted-by":"publisher","first-page":"7063","DOI":"10.3390\/molecules26237063","article-title":"Organic nanoplatforms for iodinated\ncontrast media in CT imaging","volume":"26","author":"Zhang","year":"2021","journal-title":"Molecules"},{"issue":"3","key":"2026101315083863100_cit14","doi-asserted-by":"publisher","first-page":"551","DOI":"10.3390\/molecules31030551","article-title":"Iodinated\ncontrast media\u2500from clinical use to\nenvironmental concern and treatment possibilities","volume":"31","author":"Wrzesin\u0301ska","year":"2026","journal-title":"Molecules"},{"key":"2026101315083863100_cit15","doi-asserted-by":"publisher","first-page":"144846","DOI":"10.1016\/j.scitotenv.2020.144846","article-title":"Comprehensive review on iodinated\nX-ray contrast media:\nComplete fate, occurrence, and formation of disinfection byproducts","volume":"769","author":"Sengar","year":"2021","journal-title":"Sci. Total Environ."},{"issue":"4","key":"2026101315083863100_cit16","doi-asserted-by":"publisher","first-page":"581","DOI":"10.1007\/s40121-019-00260-x","article-title":"Infectious\ndisease management and control with povidone iodine","volume":"8","author":"Eggers","year":"2019","journal-title":"Infect. Dis. Ther."},{"issue":"3","key":"2026101315083863100_cit17","doi-asserted-by":"publisher","first-page":"376","DOI":"10.1111\/j.1742-481X.2007.00405.x","article-title":"Povidone-iodine: Use in hand disinfection,\nskin preparation\nand antiseptic irrigation","volume":"5","author":"Durani","year":"2008","journal-title":"Int. Wound J."},{"issue":"14","key":"2026101315083863100_cit18","doi-asserted-by":"publisher","first-page":"3019","DOI":"10.3390\/molecules30143019","article-title":"Advances in \u03b1-arylation\nof carbonyl compounds: Diaryliodonium\nsalts as arylating agents","volume":"30","author":"Chen","year":"2025","journal-title":"Molecules"},{"issue":"21","key":"2026101315083863100_cit19","doi-asserted-by":"publisher","first-page":"3409","DOI":"10.1039\/b410128f","article-title":"Iodide effects in transition metal\ncatalyzed reactions","volume":"33","author":"Maitlis","year":"2004","journal-title":"Dalton Trans."},{"key":"2026101315083863100_cit20","doi-asserted-by":"publisher","first-page":"545","DOI":"10.1016\/j.envres.2017.08.051","article-title":"The toxicology of mercury:\nCurrent research and emerging trends","volume":"159","author":"Bj\u00f8rklund","year":"2017","journal-title":"Environ.\nRes."},{"issue":"5","key":"2026101315083863100_cit21","doi-asserted-by":"publisher","first-page":"5100","DOI":"10.1021\/acsomega.3c07047","article-title":"The toxicity of mercury and its chemical compounds:\nMolecular mechanisms and environmental and human health implications:\nA comprehensive review","volume":"9","author":"Wu","year":"2024","journal-title":"ACS Omega"},{"key":"2026101315083863100_cit22","doi-asserted-by":"publisher","first-page":"1559968","DOI":"10.3389\/fenvc.2025.1559968","article-title":"Mercury interaction with S-containing\nmolecules: Implications\nfor methylation and demethylation processes in a sulfate reducing\nbacteria","volume":"6","author":"Bakour","year":"2025","journal-title":"Front. Environ. Chem."},{"key":"2026101315083863100_cit23","doi-asserted-by":"publisher","first-page":"27","DOI":"10.1016\/bs.ant.2018.03.005","article-title":"Neurodevelopmental\neffects of mercury","volume":"2","author":"Oliveira","year":"2018","journal-title":"Adv. Neurotoxicol."},{"key":"2026101315083863100_cit24","doi-asserted-by":"publisher","first-page":"173577","DOI":"10.1016\/j.scitotenv.2024.173577","article-title":"Mercury-induced toxicity:\nMechanisms, molecular pathways, and gene regulation","volume":"943","author":"Kang","year":"2024","journal-title":"Sci. Total Environ."},{"key":"2026101315083863100_cit25","doi-asserted-by":"publisher","first-page":"949048","DOI":"10.1155\/2012\/949048","article-title":"Toxic effects of mercury\non the cardiovascular and central nervous systems","volume":"2012","author":"Azevedo","year":"2012","journal-title":"J. Biomed. Biotechnol."},{"issue":"6","key":"2026101315083863100_cit26","doi-asserted-by":"publisher","first-page":"1189","DOI":"10.1016\/j.ekir.2022.03.009","article-title":"Toxic nephropathy\nsecondary to chronic mercury poisoning: Clinical characteristics and\noutcomes","volume":"7","author":"Gao","year":"2022","journal-title":"Kidney Int. Rep."},{"issue":"5","key":"2026101315083863100_cit27","doi-asserted-by":"publisher","first-page":"320","DOI":"10.4082\/kjfm.2012.33.5.320","article-title":"Improved chronic\nfatigue symptoms after removal of\nmercury in patient with increased mercury concentration in hair toxic\nmineral assay: A case","volume":"33","author":"Shin","year":"2012","journal-title":"Korean J. Fam. Med."},{"key":"2026101315083863100_cit28","doi-asserted-by":"publisher","first-page":"1148357","DOI":"10.3389\/ftox.2023.1148357","article-title":"Mercury intoxication\nand ophthalmic involvement: An update review","volume":"5","author":"de Los Santos","year":"2023","journal-title":"Front. Toxicol."},{"issue":"4","key":"2026101315083863100_cit29","doi-asserted-by":"publisher","first-page":"493","DOI":"10.1017\/cjn.2021.146","article-title":"Mercury and movement disorders: The\ntoxic legacy continues","volume":"49","author":"Ganguly","year":"2022","journal-title":"Can. J. Neurol. Sci."},{"key":"2026101315083863100_cit30","doi-asserted-by":"publisher","first-page":"19","DOI":"10.1007\/s44397-026-00050-4","article-title":"Recent advances\nin luminescent chemosensors\nfor sensitive and selective detection of heavy metal ions in aqueous\nenvironments","volume":"2","author":"Prasad","year":"2026","journal-title":"Discovery Sens."},{"key":"2026101315083863100_cit31","doi-asserted-by":"publisher","first-page":"117493","DOI":"10.1016\/j.trac.2023.117493","article-title":"A comprehensive\nreview on recent advances in fluorescence-based\nbio-analytes sensing","volume":"171","author":"Mal","year":"2024","journal-title":"TrAC, Trends Anal. Chem."},{"issue":"3","key":"2026101315083863100_cit32","doi-asserted-by":"publisher","first-page":"109701","DOI":"10.1016\/j.jece.2023.109701","article-title":"A review on\npyrene based chemosensors\nfor the specific detection on d-transition metal ions and their various\napplications","volume":"11","author":"Prabakaran","year":"2023","journal-title":"J. Environ. Chem. Eng."},{"key":"2026101315083863100_cit33","doi-asserted-by":"publisher","first-page":"49","DOI":"10.1016\/j.jphotochem.2014.07.015","article-title":"Fluorescence\ndetection of iodide anion using a donor-acceptor (D-A) thiourea derivative","volume":"292","author":"Yang","year":"2014","journal-title":"J. Photochem. Photobiol., A"},{"issue":"89","key":"2026101315083863100_cit34","doi-asserted-by":"publisher","first-page":"86627","DOI":"10.1039\/c6ra18490a","article-title":"A highly\nselective colorimetric chemosensor for detection of iodide ions in\naqueous solution","volume":"6","author":"Chen","year":"2016","journal-title":"RSC Adv."},{"issue":"11","key":"2026101315083863100_cit35","doi-asserted-by":"publisher","first-page":"9730","DOI":"10.1021\/acsomega.1c07279","article-title":"Fluorenone-based fluorescent and\ncolorimetric sensors for selective detection of I\u2013 ions: Applications in HeLa cell imaging and logic gate","volume":"7","author":"Junaid","year":"2022","journal-title":"ACS Omega"},{"issue":"46","key":"2026101315083863100_cit36","doi-asserted-by":"publisher","first-page":"15543","DOI":"10.1021\/acs.analchem.1c03719","article-title":"Halogen\nbonding ionophore for potentiometric iodide sensing","volume":"93","author":"Seah","year":"2021","journal-title":"Anal. Chem."},{"issue":"43","key":"2026101315083863100_cit37","doi-asserted-by":"publisher","first-page":"14972","DOI":"10.1021\/ja054862h","article-title":"A halogen-bonding-based\nheteroditopic receptor for alkali metal halides","volume":"127","author":"Mele","year":"2005","journal-title":"J. Am. Chem. Soc."},{"issue":"8","key":"2026101315083863100_cit38","doi-asserted-by":"publisher","first-page":"4311","DOI":"10.1021\/acs.analchem.5b04461","article-title":"Simple, robust, and plasticizer-free\niodide-selective sensor based on copolymerized triazole-based ionic\nliquid","volume":"88","author":"Mendecki","year":"2016","journal-title":"Anal. Chem."},{"issue":"9","key":"2026101315083863100_cit39","doi-asserted-by":"publisher","first-page":"4512","DOI":"10.1021\/acs.inorgchem.5b00344","article-title":"Iodide\nion pairing with highly charged ruthenium polypyridyl\ncations in CH3CN","volume":"54","author":"Swords","year":"2015","journal-title":"Inorg. Chem."},{"issue":"43","key":"2026101315083863100_cit40","doi-asserted-by":"publisher","first-page":"15007","DOI":"10.1021\/ie401373m","article-title":"Reactivity of tetrabutylammonium\niodide with a heteronuclear 6Copper(II)-4Na(I) complex: Selective\nrecognition of iodide ion","volume":"52","author":"Kumari","year":"2013","journal-title":"Ind. Eng. Chem. Res."},{"issue":"19","key":"2026101315083863100_cit41","doi-asserted-by":"publisher","first-page":"2925","DOI":"10.1002\/asia.202000758","article-title":"Recent advances\nin luminescent recognition\nand chemosensing of iodide in water","volume":"15","author":"Valdes-Garci\u0301a","year":"2020","journal-title":"Chem. \u2013\nAsian J."},{"key":"2026101315083863100_cit42","doi-asserted-by":"publisher","first-page":"152877","DOI":"10.1016\/j.tetlet.2021.152877","article-title":"Colorimetric detection of iodide ion by a nuclear fast\nred-based Hg2+ complex in aqueous media","volume":"67","author":"Fukushima","year":"2021","journal-title":"Tetrahedron Lett."},{"key":"2026101315083863100_cit43","doi-asserted-by":"publisher","first-page":"121939","DOI":"10.1016\/j.molliq.2023.121939","article-title":"The switchable fluorescent\ndetection of mercury, copper, and iodine in real water samples using\nbola-amphiphilic-tetraphenylethene","volume":"382","author":"Bayindir","year":"2023","journal-title":"J. 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