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Aggregation of two, three, or four units of [{Ag(SnB11H11)(PR3)}n]n- (PPh3, n = 2; PEt3, n = 3; PMe3, n = 4) was found, depending on the size of the coordinating phosphine. The structures of the silver\u2212tin clusters in the solid state were determined by single-crystal X-ray diffraction. In these phosphine silver coordination compounds, the tin ligand exhibits \u03bc2- and \u03bc3-coordination with the silver atoms. From the reaction with silver nitrate, an octaanionic stanna-closo-dodecaborate coordination compound, [Et4N]8[Ag4(SnB11H11)6], was isolated. In this cluster, arranged as butterfly, the stannaborate shows various coordination modes at four silver atoms. In the reported silver\u2212tin complexes, the silver\u2212silver interatomic distances are in a range of 2.6326(10)\u22123.1424(6) \u00c5. Silver\u2212tin distances were found between 2.6416(5) and 3.1460(6) \u00c5. Analysis of the molecular orbitals calculated by means of density functional theory shows that the LUMO of the core compound without [SnB11H11]2- units is always a totally symmetric combination of (mainly) s-orbitals of Ag atoms. This core is filled with electrons of the HOMOs of the [SnB11H11]2- units and is leading, in this way, to a stable compound.<\/jats:p>","DOI":"10.1021\/ic700464d","type":"journal-article","created":{"date-parts":[[2007,6,30]],"date-time":"2007-06-30T07:39:59Z","timestamp":1183189199000},"page":"6775-6784","source":"Crossref","is-referenced-by-count":39,"title":["Silver Aggregation Caused by Stanna-\n                    <i>closo<\/i>\n                    -dodecaborate Coordination:\u2009\nSyntheses, Solid-State Structures and Theoretical Studies"],"prefix":"10.1021","volume":"46","author":[{"given":"Siegbert","family":"Hagen","sequence":"first","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hartmut","family":"Schubert","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"C\u00e4cilia","family":"Maichle-M\u00f6ssmer","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ingo","family":"Pantenburg","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Florian","family":"Weigend","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lars","family":"Wesemann","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie, Universit\u00e4t T\u00fcbingen, Auf der Morgenstelle 18, 72076 T\u00fcbingen, Germany, Institut f\u00fcr Nanotechnologie, Forschungszentrum Karlsruhe, Postfach 3640, 76021 Karlsruhe, Germany, and Institut f\u00fcr Anorganische Chemie, Universit\u00e4t zu K\u00f6ln, Greinstrasse 6, 50939 K\u00f6ln, Germany"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2007,6,30]]},"reference":[{"key":"2026091506572179500_micit1","unstructured":"Metal Clusters in Chemistry; BraunsteinP., OroL. 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