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Herein, we introduced a dual-anode electrochemical reactor employing sequential hydroxylation and direct electron transfer (DET) mechanisms for the efficient destruction of chlorinated aromatics coupled with carbon resource recovery. The reactor integrated a Ce-doped tin antimony oxide (Ce-ATO) anode and a defective ATO anode. As a proof of concept, 2,4-dichlorophenoxyacetic acid (2,4-D), a widely produced pesticide, was first converted into 2,4-dichlorophenol via hydroxylation reaction at the Ce-ATO anode. This intermediate subsequently underwent DET at the downstream defective ATO anode, generating organic radicals that underwent radical\u2013radical coupling to form oligomers. The inclusion of a proton exchange membrane into the reactor maintained an acidic microenvironment, which enhanced \u2022OH-mediated oxidation and promoted adsorption. The system achieved over 95% removal of 0.45 mM 2,4-D at a current of 1 mA and a membrane flux of 150 LMH, and a corresponding hydraulic retention time of 0.8 min, with an oligomer recovery rate of 62% obtained at 5 mM 2,4-D under otherwise identical conditions. The recovered oligomers were readily pyrolyzed into microporous carbon with a high surface area (454.47 m2\u00b7g\u20131) and demonstrated excellent adsorption capacity for 4-chlorophenol (217.31 mg\u00b7g\u20131). Furthermore, the system demonstrated robust performance when applied to complex pharmaceutical wastewater. This work offered a sustainable strategy for simultaneous decontamination and resource upcycling in high-salinity wastewater streams.<\/jats:p>","DOI":"10.1021\/jacs.6c04140","type":"journal-article","created":{"date-parts":[[2026,6,5]],"date-time":"2026-06-05T09:55:25Z","timestamp":1780653325000},"page":"24053-24065","source":"Crossref","is-referenced-by-count":0,"title":["Tandem\nDual-Anode Electrochemical Reactor for Valorizing\nChlorinated Aromatic Pollutants into Tailorable Polymeric Adsorbent"],"prefix":"10.1021","volume":"148","author":[{"ORCID":"https:\/\/orcid.org\/0009-0004-5745-3710","authenticated-orcid":true,"given":"Xuechuan","family":"Li","sequence":"first","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ting","family":"Zhou","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5486-5673","authenticated-orcid":true,"given":"Sen","family":"Lu","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenhui","family":"Li","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiao","family":"Li","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaoxiao","family":"Lu","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jia","family":"Zhou","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Guan","family":"Zhang","sequence":"additional","affiliation":[{"name":"Harbin Institute of Technology, Shenzhen (HITSZ) , , ,","place":["Shenzhen, China, 518055"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,6,5]]},"reference":[{"key":"2026073023134278300_cit1","doi-asserted-by":"publisher","DOI":"10.1016\/j.coelec.2020.100678","article-title":"Electrochemical advanced oxidation\nprocesses for wastewater treatment: Advances in formation and detection\nof reactive species and mechanisms","volume":"27","author":"Ganiyu","year":"2021","journal-title":"Curr. 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