{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,14]],"date-time":"2026-09-14T18:40:11Z","timestamp":1789411211212,"version":"build-2803163510"},"reference-count":44,"publisher":"American Chemical Society (ACS)","issue":"23","license":[{"start":{"date-parts":[[2026,6,1]],"date-time":"2026-06-01T00:00:00Z","timestamp":1780272000000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-029"},{"start":{"date-parts":[[2026,6,1]],"date-time":"2026-06-01T00:00:00Z","timestamp":1780272000000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-037"},{"start":{"date-parts":[[2026,6,1]],"date-time":"2026-06-01T00:00:00Z","timestamp":1780272000000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-045"}],"funder":[{"DOI":"10.13039\/na","name":"U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences","doi-asserted-by":"publisher","award":["DE-AC02-76SF00515"],"award-info":[{"award-number":["DE-AC02-76SF00515"]}],"id":[{"id":"10.13039\/na","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/na","name":"National Science Foundation","doi-asserted-by":"publisher","award":["ECCS-2026822"],"award-info":[{"award-number":["ECCS-2026822"]}],"id":[{"id":"10.13039\/na","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,6,17]]},"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>The solid\u2013electrolyte interphase (SEI) on lithium metal forms through electrolyte reduction at a dynamically evolving metal surface, yet how its chemistry and spatial organization develop during lithium plating and stripping remains poorly understood. Here, using a 1,2-dimethoxyethane (DME)\/1 M lithium bis(fluorosulfonyl)imide (LiFSI) electrolyte system, we show that three-dimensional lithium growth drives spatiochemical segregation of interphase products into chemically heterogeneous domains that are mechanically reorganized during stripping into a porous electrolyte-retaining framework. Correlative X-ray photoelectron spectroscopy, scanning electron microscopy, nanoscale secondary ion mass spectrometry (NanoSIMS), and synchrotron X-ray absorption spectroscopy reveal that FSI\u2013-derived inorganic species, dominated by LiF, become enriched in regions spatially decoupled from oxygen-containing phases near the lithium surface. Stripping-induced contraction compacts these chemically distinct domains into confined intergranular volumes, where supersaturation promotes precipitation and consolidation, yielding a porous SEI that retains electrolyte-derived species within a buried pore network beyond the reach of surface-sensitive probes. Spatiochemical segregation thus couples interfacial reaction pathways to lithium chemo-mechanics, dictating interphase composition, architecture, and permeability. These findings establish a chemo-mechanical framework for SEI evolution and suggest strategies to mitigate electrolyte retention and interphase instability in lithium\u2013metal batteries.<\/jats:p>","DOI":"10.1021\/jacs.6c04430","type":"journal-article","created":{"date-parts":[[2026,6,1]],"date-time":"2026-06-01T19:34:01Z","timestamp":1780342441000},"page":"24084-24095","source":"Crossref","is-referenced-by-count":1,"title":["Spatiochemical Segregation\nin Porous Lithium\u2013Metal\nInterphases"],"prefix":"10.1021","volume":"148","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-9420-0702","authenticated-orcid":true,"given":"Weilai","family":"Yu","sequence":"first","affiliation":[{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]},{"name":"University of Toronto , , , ,","place":["Toronto, Ontario, Canada, M5S 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94025"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6875-0057","authenticated-orcid":true,"given":"Jagjit","family":"Nanda","sequence":"additional","affiliation":[{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]},{"name":"SLAC National Accelerator Laboratory , , , ,","place":["Menlo Park, California, United States, 94025"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6271-068X","authenticated-orcid":true,"given":"Jian","family":"Qin","sequence":"additional","affiliation":[{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6103-6352","authenticated-orcid":true,"given":"Yi","family":"Cui","sequence":"additional","affiliation":[{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]},{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]},{"name":"SLAC National Accelerator Laboratory , , , ,","place":["Menlo Park, California, United States, 94025"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0972-1715","authenticated-orcid":true,"given":"Zhenan","family":"Bao","sequence":"additional","affiliation":[{"name":"Stanford University , , , ,","place":["Stanford, California, United States, 94305"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,6,1]]},"reference":[{"issue":"3","key":"2026073023131200400_cit1","doi-asserted-by":"publisher","first-page":"180","DOI":"10.1038\/s41560-019-0338-x","article-title":"Pathways for Practical High-Energy\nLong-Cycling Lithium\nMetal Batteries","volume":"4","author":"Liu","year":"2019","journal-title":"Nat. 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