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Herein, we construct a fullerene-based polymer interphase (PC60) on Zn to confine interfacial electrons and regulate Zn redox chemistry. A fullerene-derived monomer integrating an electron-deficient C60 cage with polar ester and amine groups undergoes thermal polymerization to form a dense and uniform interphase. Owing to the high electron affinity and deep LUMO of C60, PC60 induces interfacial charge redistribution, yielding an electronegative passivating layer that suppresses hydrogen evolution and sulfate\/polyiodide-involved corrosion, while facilitating Zn2+ desolvation and selective transport. In situ DEMS, XRD, Raman spectroscopy, and KPFM collectively reveal suppressed HER, reduced basic zinc sulfate formation, enhanced Zn2+ transference, and homogenized surface potential. Consequently, PC60\/Zn enables stable cycling over 5500 h in symmetric cells, &amp;gt; 99.9% Coulombic efficiency for 5500 cycles in half cells, and &amp;gt;96% capacity retention after 1000 cycles in PC60\/Zn||ZnI2 full cells. This work establishes electron confinement as an effective lever to reconstruct the interfacial electronic landscape and decouple Zn redox chemistry from parasitic reactions in aqueous Zn metal batteries.<\/jats:p>","DOI":"10.1021\/jacs.6c11153","type":"journal-article","created":{"date-parts":[[2026,8,31]],"date-time":"2026-08-31T22:26:33Z","timestamp":1788215193000},"page":"38291-38303","source":"Crossref","is-referenced-by-count":0,"title":["A Fullerene-Based Interphase\nConfines Interfacial\nElectrons for Long-Lived Zinc Metal Anodes in Aqueous Electrolytes"],"prefix":"10.1021","volume":"148","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-5235-7157","authenticated-orcid":true,"given":"Baoshan","family":"Wu","sequence":"first","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]},{"name":"Energy and Information Materials Key Laboratory of Sichuan Province , ,","place":["Chengdu, China, 611731"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0000-1635-0177","authenticated-orcid":true,"given":"Wei","family":"Tang","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]},{"name":"Energy and Information Materials Key Laboratory of Sichuan Province , ,","place":["Chengdu, China, 611731"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tingkuo","family":"Zhang","sequence":"additional","affiliation":[{"name":"Fujian Normal University , , ,","place":["Fuzhou, China, 350007"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mingwei","family":"An","sequence":"additional","affiliation":[{"name":"Fujian Normal University , , ,","place":["Fuzhou, China, 350007"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ziyang","family":"Hao","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]},{"name":"Energy and Information Materials Key Laboratory of Sichuan Province , ,","place":["Chengdu, China, 611731"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zuochang","family":"Chen","sequence":"additional","affiliation":[{"name":"Xiamen University , , ,","place":["Xiamen, China, 361005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hanrui","family":"Tian","sequence":"additional","affiliation":[{"name":"Xiamen University , , ,","place":["Xiamen, China, 361005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nan","family":"Zhao","sequence":"additional","affiliation":[{"name":"Singapore University of Technology and Design , , ,","place":["Singapore, Singapore, 487372"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jianbiao","family":"Fan","sequence":"additional","affiliation":[{"name":"Xiamen University , , ,","place":["Xiamen, China, 361005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Peng","family":"Du","sequence":"additional","affiliation":[{"name":"Xiamen University , , ,","place":["Xiamen, China, 361005"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3669-0192","authenticated-orcid":true,"given":"Yang","family":"Wang","sequence":"additional","affiliation":[{"name":"Fujian Normal University , , ,","place":["Fuzhou, China, 350007"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Panfeng","family":"Zhao","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]},{"name":"Energy and Information Materials Key Laboratory of Sichuan Province , ,","place":["Chengdu, China, 611731"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5348-3013","authenticated-orcid":true,"given":"Xiaobin","family":"Niu","sequence":"additional","affiliation":[{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]},{"name":"Energy and Information Materials Key Laboratory of Sichuan Province , ,","place":["Chengdu, China, 611731"]},{"name":"University of Electronic Science and Technology of China , , ,","place":["Chengdu, China, 611731"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,25]]},"reference":[{"issue":"7","key":"2026090910083164900_cit1","doi-asserted-by":"publisher","first-page":"1415","DOI":"10.1016\/j.joule.2023.06.007","article-title":"Zinc-ion batteries\nfor stationary energy 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