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Here, we report a dual-interlocking electrocatalyst interface design method that integrates the current collector, catalyst support, and active sites into a mechanically and electronically coherent architecture to address these issues. A graphdiyne-mediated hierarchical interlock promotes the interpenetrated growth of vacancy-rich distorted NiTe on nickel foam, enabling robust collector\u2013support coupling and low interfacial resistance, while a spatial interlock locally confines ultrasmall Ru clusters within defect-rich NiTe domains through Ru\u2013Ni\/Te coordination and defect-mediated confinement, mitigating migration, aggregation, and active-site loss. The catalyst exhibits a low overpotential of 60.5 \u00b1 13.9 mV at \u22121.0 A cm\u20132 and operates stably for over 10,000 h and 3500 h at \u22121.0 and \u22122.0 A cm\u20132, respectively, in 1 M KOH. In a practical AEMWE device (80 \u00b0C, 4 cm2), the electrolyzer delivers 1.79 V at 3.0 A cm\u20132, meeting the U.S. DOE 2026 low-temperature electrolysis stack target, and sustains continuous operation for 1,030 h and 4100 h at 1.0 and 2.0 A cm\u20132, respectively. This work provides a broadly applicable electrode-architecture strategy for stabilizing high-rate gas\u2013liquid\u2013solid electrochemical interfaces through multiscale dual interlocking.<\/jats:p>","DOI":"10.1021\/jacs.6c14322","type":"journal-article","created":{"date-parts":[[2026,8,10]],"date-time":"2026-08-10T07:02:29Z","timestamp":1786345349000},"page":"35156-35168","source":"Crossref","is-referenced-by-count":1,"title":["A Dual-Interlocked\nElectrocatalyst Design Principle\nfor Durable AEM Water Electrolysis at Industrial Current Densities"],"prefix":"10.1021","volume":"148","author":[{"given":"Xiangyao","family":"Gu","sequence":"first","affiliation":[{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]},{"name":"University of Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yaozhong","family":"Guo","sequence":"additional","affiliation":[{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]},{"name":"University of Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Meiping","family":"Li","sequence":"additional","affiliation":[{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tongtong","family":"Ye","sequence":"additional","affiliation":[{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]},{"name":"University of Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100049"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8108-0975","authenticated-orcid":true,"given":"Yi","family":"Xu","sequence":"additional","affiliation":[{"name":"University of Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100049"]},{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5169-0855","authenticated-orcid":true,"given":"Changshui","family":"Huang","sequence":"additional","affiliation":[{"name":"Institute of Chemistry, Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100190"]},{"name":"University of Chinese Academy of Sciences , , ,","place":["Beijing, People\u2019s Republic of China, 100049"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,8,10]]},"reference":[{"key":"2026081910245364900_cit1","doi-asserted-by":"publisher","first-page":"673","DOI":"10.1038\/s41586-022-05379-5","article-title":"A membrane-based seawater\nelectrolyser for hydrogen generation","volume":"612","author":"Xie","year":"2022","journal-title":"Nature"},{"key":"2026081910245364900_cit2","doi-asserted-by":"publisher","first-page":"430","DOI":"10.1126\/science.ads1466","article-title":"Polyoxometalated\nmetal-organic framework superstructure for stable water oxidation","volume":"388","author":"Yue","year":"2025","journal-title":"Science"},{"key":"2026081910245364900_cit3","doi-asserted-by":"publisher","first-page":"944","DOI":"10.1038\/s41929-024-01209-1","article-title":"Seed-assisted\nformation of NiFe anode catalysts for anion exchange membrane water\nelectrolysis at industrial-scale current density","volume":"7","author":"Li","year":"2024","journal-title":"Nat. Catal."},{"key":"2026081910245364900_cit4","doi-asserted-by":"publisher","first-page":"1022","DOI":"10.1038\/s41563-023-01584-3","article-title":"Amorphous\nnickel hydroxide shell\ntailors local chemical environment on platinum surface for alkaline\nhydrogen evolution reaction","volume":"22","author":"Wan","year":"2023","journal-title":"Nat. Mater."},{"key":"2026081910245364900_cit5","doi-asserted-by":"publisher","first-page":"2404658","DOI":"10.1002\/adma.202404658","article-title":"Unlocking Efficiency:\nMinimizing energy loss in electrocatalysts for water splitting","volume":"36","author":"Li","year":"2024","journal-title":"Adv. Mater."},{"key":"2026081910245364900_cit6","doi-asserted-by":"publisher","first-page":"2305844","DOI":"10.1002\/adma.202370370","article-title":"Efficient alkaline hydrogen evolution\nreaction using superaerophobic\nni nanoarrays with accelerated H2 bubble release","volume":"35","author":"Kim","year":"2023","journal-title":"Adv. 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Mater."},{"key":"2026081910245364900_cit37","doi-asserted-by":"publisher","first-page":"3376","DOI":"10.1038\/s41467-018-05878-y","article-title":"Selectively nitrogen-doped\ncarbon materials as superior metal-free catalysts for oxygen reduction","volume":"9","author":"Lv","year":"2018","journal-title":"Nat. Commun."},{"key":"2026081910245364900_cit38","doi-asserted-by":"publisher","first-page":"4048","DOI":"10.1039\/D2EE01337A","article-title":"Breaking the symmetry\nof single-atom catalysts enables an extremely low energy barrier and\nhigh stability for large-current-density water splitting","volume":"15","author":"Mu","year":"2022","journal-title":"Energy Environ. Sci."},{"key":"2026081910245364900_cit39","doi-asserted-by":"publisher","first-page":"1342","DOI":"10.1038\/s41467-024-45533-3","article-title":"Microenvironment\nreconstitution of highly active Ni single atoms on oxygen-incorporated\nMo2C for water splitting","volume":"15","author":"Hou","year":"2024","journal-title":"Nat. Commun."},{"key":"2026081910245364900_cit40","doi-asserted-by":"publisher","first-page":"1799","DOI":"10.1039\/D0EE00666A","article-title":"Phosphine vapor-assisted\nconstruction\nof heterostructured Ni2P\/NiTe2 catalysts for\nefficient hydrogen evolution","volume":"13","author":"Li","year":"2020","journal-title":"Energy Environ.\nSci."},{"key":"2026081910245364900_cit41","doi-asserted-by":"publisher","first-page":"10587","DOI":"10.1038\/s41467-024-54987-4","article-title":"Tackling activity-stability\nparadox of reconstructed\nNiIrOx electrocatalysts by bridged W-O moiety","volume":"15","author":"Abdullah","year":"2024","journal-title":"Nat. Commun."},{"key":"2026081910245364900_cit42","doi-asserted-by":"publisher","first-page":"46360","DOI":"10.1021\/jacs.5c15759","article-title":"Lignin-directed construction of vertical\nRu\/RuO2 electron-bridge\ninterfaces for low-input self-powered hydrazine-water splitting","volume":"147","author":"Liu","year":"2025","journal-title":"J. Am. Chem. Soc."},{"key":"2026081910245364900_cit43","doi-asserted-by":"publisher","first-page":"3976","DOI":"10.1038\/s41467-025-58346-9","article-title":"Atomic Ga\ntriggers spatiotemporal coordination of oxygen radicals for efficient\nwater oxidation on crystalline RuO2","volume":"16","author":"Wang","year":"2025","journal-title":"Nat. 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Adv."},{"key":"2026081910245364900_cit46","doi-asserted-by":"publisher","first-page":"2416012","DOI":"10.1002\/adma.202416012","article-title":"Proton exchange\nmembrane water splitting: Advances in electrode structure and mass-charge\ntransport optimization","volume":"37","author":"Feng","year":"2025","journal-title":"Adv. Mater."},{"key":"2026081910245364900_cit47","doi-asserted-by":"publisher","first-page":"36763","DOI":"10.1021\/jacs.5c12507","article-title":"Potential Pulsing-Induced Fe Undercoordination\nin NiFe (Oxy)Hydroxide Enhances Electrochemical Oxygen Evolution","volume":"147","author":"Wu","year":"2025","journal-title":"J. Am. Chem. Soc."},{"key":"2026081910245364900_cit48","doi-asserted-by":"publisher","DOI":"10.1002\/anie.202414647","article-title":"Pioneering\nbuilt-in interfacial electric field for enhanced anion exchange membrane\nwater electrolysis","volume":"64","author":"Huang","year":"2025","journal-title":"Angew. Chem., Int. 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Mater."},{"key":"2026081910245364900_cit52","doi-asserted-by":"publisher","first-page":"8827","DOI":"10.1038\/s41467-025-63870-9","article-title":"Boosting and stabilizing oxygen evolution\nreaction through Ru single atoms anchored amorphous NiMoOx electrocatalyst","volume":"16","author":"Li","year":"2025","journal-title":"Nat. Commun."},{"key":"2026081910245364900_cit53","doi-asserted-by":"publisher","first-page":"5884","DOI":"10.1038\/s41467-020-19571-6","article-title":"Synthetic strategies\nof supported atomic clusters for heterogeneous catalysis","volume":"11","author":"Rong","year":"2020","journal-title":"Nat. Commun."},{"key":"2026081910245364900_cit54","doi-asserted-by":"publisher","first-page":"2307017","DOI":"10.1002\/adma.202307017","article-title":"The secret\nof nanoarrays toward efficient electrochemical water splitting: a\nvision of self-dynamic electrolyte","volume":"35","author":"He","year":"2023","journal-title":"Adv. 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