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However, overreliance on deliberate phase selection significantly hinders access to most members of the anticipated electrode material family, limiting the utilization of capacity and high-potential redox couples. Herein, we demonstrate that the activated anionic redox can overcome the performance limitations arising from pristine crystalline-phase selectivity, and we validate the strategy in a series of zinc-storage copper selenides with variable stoichiometries (CuySe, y = 0.5\u20132). Using hexagonal CuSe as an example, we show that once the selenium anionic redox is activated, this most thermodynamically stable yet zincophobic phase achieves a hundred-fold increase in capacity from 4 mAh g\u20131 to 413 mAh g\u20131 and a doubled battery voltage. Combined structural and spectroscopic evidence during the in situ electrochemical process reveals that CuSe is reconstructed into the favored phase, interwoven with active selenium (Se0) via nucleophile-induced anionic redox, promoting deep and reversible multielectron conversions that transcend inherent capacity constraints. The anion-anchored phase with selenium redox enables the copper selenide family to operate as a stable, high-capacity cathode in zinc batteries for the first time, with a lifespan reaching 4000 cycles. We also confirm the robust applicability of this strategy to other nucleophilic additives, offering new avenues for revitalizing this long-dormant material family.<\/jats:p>","DOI":"10.1021\/jacs.6c14588","type":"journal-article","created":{"date-parts":[[2026,10,8]],"date-time":"2026-10-08T03:01:45Z","timestamp":1791428505000},"page":"44833-44843","source":"Crossref","is-referenced-by-count":0,"title":["Beyond\nPhase Selectivity in Conversion Copper Selenides\nCathode through Activated Anionic Redox"],"prefix":"10.1021","volume":"148","author":[{"given":"Yuanhe","family":"Sun","sequence":"first","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Junwei","family":"Yang","sequence":"additional","affiliation":[{"name":"Shanghai Dianji University , , ,","place":["Shanghai, China, 201306"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mengru","family":"Lin","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hao","family":"Shi","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tao","family":"Liu","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6015-5694","authenticated-orcid":true,"given":"Yi","family":"Gao","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jingyuan","family":"Ma","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5139-9889","authenticated-orcid":true,"given":"Wen","family":"Wen","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaolong","family":"Li","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2094-8360","authenticated-orcid":true,"given":"Daming","family":"Zhu","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences , , ,","place":["Shanghai, China, 201204"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"316","published-online":{"date-parts":[[2026,10,7]]},"reference":[{"issue":"7575","key":"2026102111080062500_cit1","doi-asserted-by":"publisher","first-page":"S105","DOI":"10.1038\/526S105a","article-title":"Batteries:\n4 big questions","volume":"526","author":"Bourzac","year":"2015","journal-title":"Nature"},{"issue":"4","key":"2026102111080062500_cit2","doi-asserted-by":"publisher","first-page":"268","DOI":"10.1038\/s41578-025-00773-7","article-title":"Chalcogens for high-energy\nbatteries","volume":"10","author":"Chen","year":"2025","journal-title":"Nat.\nRev. 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