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We proposed a synthesis method based on microwave plasma torches. High-resolution mass spectrometry was used to monitor rapid reaction products. 2-Alkylbenzimidazole can be formed through the reaction of phenylnitrenium ion and nitriles on a millisecond scale. This reaction can achieve the one-step formation of benzimidazoles from benzene ring single-substituted compounds without the addition of external oxidants or catalysts. A similar C\u2013H bond activation reaction can be accomplished with ketones. Meanwhile, the microwave plasma reactor was modified, and the resulting 2-methylbenzimidazole was successfully collected, indicating the device has good application potential in organic reactions such as C\u2013H bond activation reaction.<\/jats:p>","DOI":"10.1021\/jasms.4c00011","type":"journal-article","created":{"date-parts":[[2024,4,10]],"date-time":"2024-04-10T09:00:21Z","timestamp":1712739621000},"page":"951-959","source":"Crossref","is-referenced-by-count":0,"title":["Ortho C\u2013H Bond\nActivations in an Atmospheric\nMicrowave Plasma Ion Source"],"prefix":"10.1021","volume":"35","author":[{"given":"Guanru","family":"Chen","sequence":"first","affiliation":[{"name":"Zhejiang University , , ,","place":["Hangzhou, Zhejiang, P. R. China, 310027"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fengjian","family":"Chu","sequence":"additional","affiliation":[{"name":"Zhejiang University , , , ,","place":["Hangzhou, Zhejiang, P. R. 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