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However, the lack of fast and mild synthesis methods of Ln-based metal halides, as one of the technical challenges, limits their applications. Here, benefiting from the innovative selection of methanol and ethanol as the solvent and anti-solvent, respectively, a series of Cs\n                    <jats:sub>3<\/jats:sub>\n                    LnCl\n                    <jats:sub>6<\/jats:sub>\n                    (Ln = Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) microcrystals (MCs) were prepared via the recrystallization method at room temperature for the first time. This recrystallization method could also realize large-scale production at one time and recyclable recrystallization of single-element MCs and the preparation of high-entropy five-element Cs\n                    <jats:sub>3<\/jats:sub>\n                    {TbDyHoErTm}\n                    <jats:sub>1<\/jats:sub>\n                    Cl\n                    <jats:sub>6<\/jats:sub>\n                    crystals. Among these Cs\n                    <jats:sub>3<\/jats:sub>\n                    LnCl\n                    <jats:sub>6<\/jats:sub>\n                    MCs, Cs\n                    <jats:sub>3<\/jats:sub>\n                    TbCl\n                    <jats:sub>6<\/jats:sub>\n                    MCs with 4f\u2009\u2192\u20095d absorption transition possess the highest photoluminescence quantum yield of 90.8%. Besides, under X-ray irradiation, Cs\n                    <jats:sub>3<\/jats:sub>\n                    TbCl\n                    <jats:sub>6<\/jats:sub>\n                    MCs show a high light yield of ~51,800 photons MeV\n                    <jats:sup>\u22121<\/jats:sup>\n                    and the as-fabricated thin films possess promising X-ray imaging ability and excellent spatial resolutions (12\u2009lp\u2009mm\n                    <jats:sup>\u22121<\/jats:sup>\n                    ). This work provides a new method for ultrafast preparing Ln-based metal halides under mild synthetic conditions and highlights their excellent potential as scintillators for X-ray imaging.\n                  <\/jats:p>","DOI":"10.1038\/s41377-025-01839-5","type":"journal-article","created":{"date-parts":[[2025,5,13]],"date-time":"2025-05-13T23:26:17Z","timestamp":1747178777000},"update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":23,"title":["Lanthanide-based metal halides prepared at room temperature by recrystallization method for X-ray imaging"],"prefix":"10.1038","volume":"14","author":[{"given":"Huwei","family":"Li","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kai","family":"Li","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zheyu","family":"Li","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinyu","family":"Fu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qingxing","family":"Yang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nan","family":"Wang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xinyu","family":"Wang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2850-0990","authenticated-orcid":false,"given":"Jing","family":"Feng","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7758-752X","authenticated-orcid":false,"given":"Shuyan","family":"Song","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5433-8611","authenticated-orcid":false,"given":"Hongjie","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"297","published-online":{"date-parts":[[2025,5,14]]},"reference":[{"key":"1839_CR1","doi-asserted-by":"publisher","first-page":"88","DOI":"10.1038\/s41586-018-0451-1","volume":"561","author":"QS Chen","year":"2018","unstructured":"Chen, Q. 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