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Here we introduce a low-temperature sulfur chemical vapor deposition (S-CVD) technique that effectively converts SO\n                    <jats:sub>2<\/jats:sub>\n                    , with intermittently introduced H\n                    <jats:sub>2<\/jats:sub>\n                    S, into deposited sulfur (S\n                    <jats:sub>d<\/jats:sub>\n                    <jats:sup>0<\/jats:sup>\n                    ) on metal sulfides (MS), facilitating self-sustained adsorption of Hg\n                    <jats:sup>0<\/jats:sup>\n                    . ZnS, as a representative MS model, undergoes a decrease in the coordination number of Zn\u2013S from 3.9 to 3.5 after S\n                    <jats:sub>d<\/jats:sub>\n                    <jats:sup>0<\/jats:sup>\n                    deposition, accompanied by the generation of unsaturated-coordinated polysulfide species (S\n                    <jats:sub>n<\/jats:sub>\n                    <jats:sup>2\u2013<\/jats:sup>\n                    , named S\n                    <jats:sub>d<\/jats:sub>\n                    <jats:sup>*<\/jats:sup>\n                    ) with significantly enhanced Hg\n                    <jats:sup>0<\/jats:sup>\n                    adsorption performance. Surprisingly, the adsorption product, HgS (ZnS@HgS), can serve as a fresh interface for the activation of S\n                    <jats:sub>d<\/jats:sub>\n                    <jats:sup>0<\/jats:sup>\n                    to S\n                    <jats:sub>d<\/jats:sub>\n                    <jats:sup>*<\/jats:sup>\n                    through the S-CVD method, thereby achieving a self-sustained Hg\n                    <jats:sup>0<\/jats:sup>\n                    adsorption capacity exceeding 300\u2009mg\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    without saturation limitations. Theoretical calculations substantiate the self-sustained adsorption mechanism that S\n                    <jats:sub>8<\/jats:sub>\n                    ring on both ZnS and ZnS@HgS can be activated to chemical bond S\n                    <jats:sub>4<\/jats:sub>\n                    chain, exhibiting a stronger Hg\n                    <jats:sup>0<\/jats:sup>\n                    adsorption energy than pristine ones. Importantly, this S-CVD strategy is applicable to the in-situ activation of synthetic or natural MS containing chalcophile metal elements for Hg\n                    <jats:sup>0<\/jats:sup>\n                    removal and also holds potential applications for various purposes requiring MS adsorbents.\n                  <\/jats:p>","DOI":"10.1038\/s41467-024-47725-3","type":"journal-article","created":{"date-parts":[[2024,4,18]],"date-time":"2024-04-18T15:01:50Z","timestamp":1713452510000},"update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":47,"title":["In-situ low-temperature sulfur CVD on metal sulfides with SO2 to realize self-sustained adsorption of mercury"],"prefix":"10.1038","volume":"15","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-0733-7402","authenticated-orcid":false,"given":"Qinyuan","family":"Hong","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3736-4548","authenticated-orcid":false,"given":"Haomiao","family":"Xu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaoming","family":"Sun","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jiaxing","family":"Li","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenjun","family":"Huang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2193-2715","authenticated-orcid":false,"given":"Zan","family":"Qu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6842-9167","authenticated-orcid":false,"given":"Lizhi","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7821-1997","authenticated-orcid":false,"given":"Naiqiang","family":"Yan","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"297","published-online":{"date-parts":[[2024,4,18]]},"reference":[{"key":"47725_CR1","doi-asserted-by":"publisher","first-page":"201","DOI":"10.1038\/nature22997","volume":"547","author":"D Obrist","year":"2017","unstructured":"Obrist, D. et al. 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