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To address this, a kind of spatially separable oxidation-reduction assignment in fluorine substituted molecular organic junction catalyst (covalent triazine framework, CTF-TF-0.5) is constructed. By modulating the coordination of F-substituted benzene linkers, we controlled the redox nature of triazine ring in CTFs to obtain the separable oxidation-reduction assignment. It achieves a interfacial hydrogen peroxide (H\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    ) photosynthesis rate of 4664 \u00b5mol g\n                    <jats:sup>\u22121<\/jats:sup>\n                    h\n                    <jats:sup>\u22121<\/jats:sup>\n                    at triphasic interface with simulated sunlight and ultrasonic forces. With external forces, the photogenerated-holes allow to transfer to the oxidation site (triazine connected two benzene and a F-substituted benzene) and photogenerated-electrons to the reduction site (triazine connected a benzene and two F-substituted benzene) via benzene bridges for a dual-pathway of water oxidation and oxygen reduction reactions to synthesize H\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    . Additionally, this heterogeneous interfacial reaction system exhibits efficient purification capability for arsenic-containing mining wastewater. This study using the separable oxidation-reduction sites for addressing the coupling reaction at manipulable active sites to improve overall catalytic efficiency via molecular junction catalyst.\n                  <\/jats:p>","DOI":"10.1038\/s41467-026-70959-2","type":"journal-article","created":{"date-parts":[[2026,3,25]],"date-time":"2026-03-25T15:04:10Z","timestamp":1774451050000},"update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":5,"title":["Substituent-induced oxidation-reduction molecular organic junction for interfacial hydrogen peroxide photosynthesis"],"prefix":"10.1038","volume":"17","author":[{"given":"Zhi","family":"Li","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lin","family":"An","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lijiang","family":"Guan","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jingyi","family":"Yang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5067-0278","authenticated-orcid":false,"given":"Renli","family":"Yin","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2456-3540","authenticated-orcid":false,"given":"Shangbin","family":"Jin","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5926-5383","authenticated-orcid":false,"given":"Mingshan","family":"Zhu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0009-4806-1252","authenticated-orcid":false,"given":"Junhao","family":"Qin","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"297","published-online":{"date-parts":[[2026,3,25]]},"reference":[{"key":"70959_CR1","doi-asserted-by":"publisher","first-page":"1007","DOI":"10.1021\/acs.chemrev.0c01060","volume":"121","author":"BW Chen","year":"2020","unstructured":"Chen, B. 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