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Crystal data for compound 8b: C23H34O5P2, M = 452.44, triclinic, a = 8.6935(7) \u00c5, b = 23.972(2) \u00c5, c = 24.195(2) \u00c5, \u03b1 = 73.726(5)\u00b0, \u03b2 = 88.844(5)\u00b0, \u03b3 = 88.865(5)\u00b0, V = 4838.6(7) \u00c53, T = 173(2) K, space group P1\u0304, Z = 8, 249\u2009416 reflections measured, 17\u2009037 independent reflections (Rint = 0.2501). The final R1 values were 0.0698 (I > 2\u03c3(I)). The final wR(F2) values were 0.1404 (I > 2\u03c3(I)). The final R1 values were 0.1964 (all data). The final wR(F2) values were 0.1694 (all data). Crystal data for compound 8c\/d C23H34O5P2, M = 452.44, colourless needle, trigonal, space group R3\u0304 (No. 148), a = b = 20.3573(4), c = 31.9361(12) \u00c5, V = 11461.8(5) \u00c53, Z = 18, Dc = 1.180 g cm\u22123, F000 = 4356, MoK\u03b1 radiation, \u03bb = 0.71073 \u00c5, T = 120(2)K, 2\u03b8max = 55.0\u00b0, 40\u2009132 reflections collected, 5866 unique (Rint = 0.0444). Final GooF = 1.046, R1 = 0.0455, wR2 = 0.1010, R indices based on 4616 reflections with I >2\u03c3(I) (refinement on F2), 326 parameters, 0 restraints. Lp and absorption corrections applied, \u03bc = 0.199 mm\u22121"}],"container-title":["Org. Biomol. 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