{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,12]],"date-time":"2026-09-12T06:07:01Z","timestamp":1789193221081,"version":"build-2803163510"},"reference-count":35,"publisher":"Georg Thieme Verlag KG","license":[{"start":{"date-parts":[[2026,9,11]],"date-time":"2026-09-11T00:00:00Z","timestamp":1789084800000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Eur J Dent"],"abstract":"<jats:title>Abstract<\/jats:title>\n                  <jats:p>To evaluate the shear bond strength (SBS) and post-debonding surface characteristics of three dual-cure self-adhesive resin cements\u2014SpeedCem Plus (Ivoclar Vivadent), BisCem (Bisco), and RelyX U200 (3M ESPE)\u2014bonded to sound and eroded human dentin.<\/jats:p>\n                  <jats:p>Sixty dentin specimens (n\u2009=\u200910 per subgroup) were prepared from freshly extracted caries-free human molars. Erosion was induced by immersion in 0.01\u2009M hydrochloric acid (pH 2.0) for 2\u2009minutes once daily over 14 consecutive days; all specimens were stored in artificial saliva at 37\u00b0C throughout. Each cement was applied according to the manufacturer's instructions and light-cured for 20\u2009seconds. After 24\u2009hours, SBS was measured with a universal testing machine. Atomic force microscopy (AFM) and scanning electron microscopy (SEM) were used to characterize post-debonding surface topography, roughness, and failure modes.<\/jats:p>\n                  <jats:p>SBS and surface roughness were analyzed by two-way analysis of variance (substrate condition\u2009\u00d7\u2009cement type) with Tukey's Honestly Significant Difference post-hoc test. Failure-mode distributions were compared using Fisher's exact test with the Freeman\u2013Halton extension. The significance level was set at \u03b1\u2009=\u20090.05.<\/jats:p>\n                  <jats:p>SBS was markedly lower on eroded than on sound dentin for all three cements, with values on eroded dentin approaching the lower measurement threshold. On sound dentin, RelyX U200 achieved the highest bond strength; on eroded dentin, SpeedCem Plus showed the least reduction. AFM and SEM revealed distinct failure patterns: cohesive and mixed failures predominated on sound dentin, whereas debonding on eroded dentin occurred almost entirely at the adhesive interface. Erosion of the dentin substrate substantially impaired the adhesive performance of all tested self-adhesive resin cements. The residual bond strengths recorded on eroded dentin were too low to be considered clinically reliable, indicating that the eroded substrate\u2014rather than the choice of cement\u2014is the dominant determinant of bonding outcome.<\/jats:p>\n                  <jats:p>Dental erosion severely compromises the bonding of dual-cure self-adhesive resin cements to dentin. Since no cement achieved a clinically adequate bond on eroded dentin, restoration of the eroded substrate before luting should be considered.<\/jats:p>","DOI":"10.1055\/s-0046-1827798","type":"journal-article","created":{"date-parts":[[2026,9,12]],"date-time":"2026-09-12T05:06:32Z","timestamp":1789189592000},"source":"Crossref","is-referenced-by-count":0,"title":["Bond Characteristics of Dual-Cure Self-Adhesive Resin Cements on Eroded Dentin"],"prefix":"10.1055","author":[{"given":"Andrea Maria","family":"Chisnoiu","sequence":"additional","affiliation":[{"name":"Department of Prosthetic Dentistry and Dental Materials, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj\u2013Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mihaela","family":"P\u0103strav","sequence":"additional","affiliation":[{"name":"Department of Orthodontics, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj-Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0774-8121","authenticated-orcid":false,"given":"Andreea","family":"Kui","sequence":"additional","affiliation":[{"name":"Department of Prosthetic Dentistry and Dental Materials, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj\u2013Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Marius","family":"Negucioiu","sequence":"additional","affiliation":[{"name":"Department of Prosthetic Dentistry and Dental Materials, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj\u2013Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Oana","family":"Burlacu","sequence":"additional","affiliation":[{"name":"Department of Prosthetic Dentistry and Dental Materials, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj\u2013Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ioana","family":"M\u0103rginean","sequence":"additional","affiliation":[{"name":"Department of Prosthetic Dentistry and Dental Materials, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj\u2013Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ioan","family":"Petean","sequence":"additional","affiliation":[{"name":"Faculty of Chemistry and Chemical Engineering, Babes-Bolyai University, Cluj-Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Stanca","family":"Cuc","sequence":"additional","affiliation":[{"name":"Department of Polymer Composites, Raluca Ripan Institute for Research in Chemistry, Babe\u0219-Bolyai University, Cluj-Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Codruta","family":"Sarosi","sequence":"additional","affiliation":[{"name":"Department of Polymer Composites, Raluca Ripan Institute for Research in Chemistry, Babe\u0219-Bolyai University, Cluj-Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Radu","family":"Chisnoiu","sequence":"additional","affiliation":[{"name":"Department of Odontology, Endodontics and Oral Pathology, Faculty of Dental Medicine, \u201cIuliu Ha\u021bieganu\u201d University of Medicine and Pharmacy, Cluj-Napoca, Romania"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"194","published-online":{"date-parts":[[2026,9,11]]},"reference":[{"issue":"01","key":"ref1","doi-asserted-by":"crossref","first-page":"78","DOI":"10.1111\/jerd.12706","article-title":"Contemporary diagnosis and management of dental erosion","volume":"33","author":"T Donovan","year":"2021","journal-title":"J Esthet Restor Dent"},{"issue":"04","key":"ref2","first-page":"275","article-title":"Etiology and pathogenesis of dental erosion","volume":"47","author":"P Kanzow","year":"2016","journal-title":"Quintessence Int"},{"issue":"01","key":"ref3","doi-asserted-by":"crossref","first-page":"2","DOI":"10.1159\/000503308","article-title":"Terminology of erosive tooth wear: consensus report of a workshop organized by the ORCA and the Cariology Research Group of the IADR","volume":"54","author":"N Schlueter","year":"2020","journal-title":"Caries Res"},{"issue":"01","key":"ref4","doi-asserted-by":"crossref","first-page":"14","DOI":"10.1186\/s12903-016-0231-y","article-title":"Does erosion progress differently on teeth already presenting clinical signs of erosive tooth wear than on sound teeth? An in vitro pilot trial","volume":"17","author":"T S Carvalho","year":"2016","journal-title":"BMC Oral Health"},{"issue":"03","key":"ref5","doi-asserted-by":"crossref","first-page":"291","DOI":"10.2341\/16-173-L","article-title":"Bond stability of a universal adhesive system to eroded\/abraded dentin after deproteinization","volume":"43","author":"M G Augusto","year":"2018","journal-title":"Oper Dent"},{"issue":"01","key":"ref6","first-page":"24","article-title":"Analysis of laboratory adhesion studies in eroded enamel and dentin: a scoping review","volume":"8","author":"M Belmar da Costa","year":"2021","journal-title":"Biomater Investig Dent"},{"key":"ref7","doi-asserted-by":"crossref","first-page":"104633","DOI":"10.1016\/j.jdent.2023.104633","article-title":"Bonding performance of universal adhesives to eroded dentine: a 6-year evaluation","volume":"136","author":"F SF Siqueira","year":"2023","journal-title":"J Dent"},{"issue":"02","key":"ref8","doi-asserted-by":"crossref","first-page":"72","DOI":"10.1177\/0022034512455029","article-title":"The role of matrix metalloproteinases in dental erosion","volume":"24","author":"M A R Buzalaf","year":"2012","journal-title":"Adv Dent Res"},{"issue":"01","key":"ref9","doi-asserted-by":"crossref","first-page":"60","DOI":"10.2341\/16-308-L","article-title":"Three-year effects of deproteinization on the in vitro durability of resin\/ dentin- eroded interfaces","volume":"43","author":"F Siqueira","year":"2018","journal-title":"Oper Dent"},{"issue":"02","key":"ref10","doi-asserted-by":"crossref","first-page":"809","DOI":"10.1007\/s00784-019-02918-9","article-title":"Improving bonding to eroded dentin by using collagen cross-linking agents: 2 years of water storage","volume":"24","author":"F SF de Siqueira","year":"2020","journal-title":"Clin Oral Investig"},{"issue":"05","key":"ref11","doi-asserted-by":"crossref","first-page":"500","DOI":"10.2341\/22-050-L","article-title":"Effect of the absence of HEMA on the bonding properties of universal adhesive systems containing 10-MDP: an in vitro study","volume":"48","author":"M Wendlinger","year":"2023","journal-title":"Oper Dent"},{"issue":"05","key":"ref12","doi-asserted-by":"crossref","first-page":"525","DOI":"10.1016\/j.jdent.2015.03.004","article-title":"Bonding of universal adhesives to dentine\u2013old wine in new bottles?","volume":"43","author":"C Chen","year":"2015","journal-title":"J Dent"},{"issue":"02","key":"ref13","doi-asserted-by":"crossref","first-page":"133","DOI":"10.1016\/j.dental.2016.11.015","article-title":"Academy of Dental Materials guidance on in vitro testing of dental composite bonding effectiveness to dentin\/enamel using micro-tensile bond strength (\u03bcTBS) approach","volume":"33","author":"S Armstrong","year":"2017","journal-title":"Dent Mater"},{"issue":"02","key":"ref14","doi-asserted-by":"crossref","first-page":"74","DOI":"10.1016\/S0109-5641(97)80015-2","article-title":"The use of extracted teeth for in vitro bonding studies: a review of infection control considerations","volume":"13","author":"J P DeWald","year":"1997","journal-title":"Dent Mater"},{"issue":"01","key":"ref15","first-page":"33","article-title":"Dental erosion in patients with gastroesophageal reflux disease (GERD) in a sample of patients referred to the Motahari Clinic, Shiraz, Iran","volume":"15","author":"G Alavi","year":"2014","journal-title":"J Dent (Shiraz)"},{"key":"ref16","doi-asserted-by":"crossref","first-page":"e20180107","DOI":"10.1590\/1678-7757-2018-0107","article-title":"Comparison of in vitro erosion protocols in bovine teeth to simulate natural erosion lesion: analysis of mechanical properties and surface gloss","volume":"27","author":"M D Moda","year":"2019","journal-title":"J Appl Oral Sci"},{"issue":"12","key":"ref17","doi-asserted-by":"crossref","first-page":"1845","DOI":"10.1016\/j.dental.2021.09.014","article-title":"Adhesion to eroded enamel and dentin: systematic review and meta-analysis","volume":"37","author":"A Wiegand","year":"2021","journal-title":"Dent Mater"},{"issue":"S 01","key":"ref18","doi-asserted-by":"crossref","first-page":"2","DOI":"10.1159\/000325915","article-title":"Dental erosion\u2013an overview with emphasis on chemical and histopathological aspects","volume":"45","author":"A Lussi","year":"2011","journal-title":"Caries Res"},{"issue":"01","key":"ref19","doi-asserted-by":"crossref","first-page":"25","DOI":"10.1016\/j.dental.2019.08.106","article-title":"The tooth: an analogue for biomimetic materials design and processing","volume":"36","author":"V P Thompson","year":"2020","journal-title":"Dent Mater"},{"key":"ref20","doi-asserted-by":"crossref","first-page":"103809","DOI":"10.1016\/j.ijadhadh.2024.103809","article-title":"Do in vitro and in situ erosive challenges alter the bonding performance of universal adhesives?","volume":"134","author":"P H de Aguiar Moreira","year":"2024","journal-title":"Int J Adhes Adhes"},{"issue":"09","key":"ref21","doi-asserted-by":"crossref","first-page":"3573","DOI":"10.1016\/j.actbio.2010.03.024","article-title":"Nano-controlled molecular interaction at adhesive interfaces for hard tissue reconstruction","volume":"6","author":"K Yoshihara","year":"2010","journal-title":"Acta Biomater"},{"issue":"04","key":"ref22","doi-asserted-by":"crossref","first-page":"428","DOI":"10.1902\/jop.2003.74.4.428","article-title":"Permeability and morphology of dentin after erosion induced by acidic drinks","volume":"74","author":"C Prati","year":"2003","journal-title":"J Periodontol"},{"issue":"02","key":"ref23","doi-asserted-by":"crossref","first-page":"96","DOI":"10.1016\/j.jebdp.2016.03.003","article-title":"Longevity of self-etch dentin bonding adhesives compared to etch-and-rinse dentin bonding adhesives: a systematic review","volume":"16","author":"N Masarwa","year":"2016","journal-title":"J Evid Based Dent Pract"},{"issue":"03","key":"ref24","doi-asserted-by":"crossref","first-page":"254","DOI":"10.1177\/00220345221145673","article-title":"Progress in dental adhesive materials","volume":"102","author":"M Cadenaro","year":"2023","journal-title":"J Dent Res"},{"issue":"04","key":"ref25","doi-asserted-by":"crossref","first-page":"306","DOI":"10.1590\/S1806-83242012005000009","article-title":"Eroded dentin does not jeopardize the bond strength of adhesive restorative materials","volume":"26","author":"J B Cruz","year":"2012","journal-title":"Braz Oral Res"},{"issue":"06","key":"ref26","doi-asserted-by":"crossref","first-page":"4391","DOI":"10.1007\/s00784-022-04402-3","article-title":"Bonding performance and ultramorphology of the resin-dentine interface of contemporary universal adhesives","volume":"26","author":"P Maciel Pires","year":"2022","journal-title":"Clin Oral Investig"},{"issue":"05","key":"ref27","doi-asserted-by":"crossref","first-page":"814","DOI":"10.3390\/polym13050814","article-title":"Bond strength of universal adhesives to dentin: a systematic review and meta-analysis","volume":"13","author":"L Hardan","year":"2021","journal-title":"Polymers (Basel)"},{"key":"ref28","doi-asserted-by":"crossref","first-page":"1501","DOI":"10.3390\/coatings12101501","article-title":"Universal adhesives: evaluation of the relationship between bond strength and application strategies\u2014a systematic review and meta-analyses","volume":"12","author":"F Triani","year":"2022","journal-title":"Coatings"},{"issue":"02","key":"ref29","doi-asserted-by":"crossref","first-page":"118","DOI":"10.1177\/154405910508400204","article-title":"A critical review of the durability of adhesion to tooth tissue: methods and results","volume":"84","author":"J De Munck","year":"2005","journal-title":"J Dent Res"},{"issue":"01","key":"ref30","doi-asserted-by":"crossref","first-page":"24","DOI":"10.1016\/j.jdsr.2019.10.001","article-title":"The microtensile bond strength test: Its historical background and application to bond testing","volume":"56","author":"H Sano","year":"2020","journal-title":"Jpn Dent Sci Rev"},{"issue":"01","key":"ref31","first-page":"57","article-title":"Do dentin bond strength tests serve a useful purpose?","volume":"1","author":"S Sudsangiam","year":"1999","journal-title":"J Adhes Dent"},{"key":"ref32","first-page":"S1806","article-title":"Bonding stability of adhesive systems to eroded dentin","volume":"29","author":"J B Cruz","year":"2015","journal-title":"Braz Oral Res"},{"issue":"05","key":"ref33","doi-asserted-by":"crossref","first-page":"1451","DOI":"10.1007\/s00784-011-0650-8","article-title":"Long-term bonding to eroded dentin requires superficial bur preparation","volume":"16","author":"B Zimmerli","year":"2012","journal-title":"Clin Oral Investig"},{"issue":"01","key":"ref34","doi-asserted-by":"crossref","first-page":"153","DOI":"10.1055\/s-0041-1734469","article-title":"Comparative evaluation of resin dentin interface using universal and total- etch adhesive systems on sound and eroded dentin: in vitro study","volume":"16","author":"G Kanniappan","year":"2022","journal-title":"Eur J Dent"},{"issue":"04","key":"ref35","doi-asserted-by":"crossref","first-page":"391","DOI":"10.2341\/17-023-L","article-title":"Effect of different adhesive systems used for immediate dentin sealing on bond strength of a self-adhesive resin cement to dentin","volume":"43","author":"R C Ferreira-Filho","year":"2018","journal-title":"Oper Dent"}],"container-title":["European Journal of Dentistry"],"original-title":[],"language":"en","link":[{"URL":"http:\/\/www.thieme-connect.de\/products\/ejournals\/pdf\/10.1055\/s-0046-1827798.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2026,9,12]],"date-time":"2026-09-12T05:06:36Z","timestamp":1789189596000},"score":1,"resource":{"primary":{"URL":"http:\/\/www.thieme-connect.de\/DOI\/DOI?10.1055\/s-0046-1827798"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2026,9,11]]},"references-count":35,"URL":"https:\/\/doi.org\/10.1055\/s-0046-1827798","archive":["Portico","CLOCKSS"],"relation":{},"ISSN":["1305-7456","1305-7464"],"issn-type":[{"value":"1305-7456","type":"print"},{"value":"1305-7464","type":"electronic"}],"subject":[],"published":{"date-parts":[[2026,9,11]]}}}