{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,1,23]],"date-time":"2026-01-23T21:00:53Z","timestamp":1769202053915,"version":"3.49.0"},"reference-count":56,"publisher":"AIP Publishing","issue":"5","content-domain":{"domain":["pubs.aip.org"],"crossmark-restriction":true},"short-container-title":[],"published-print":{"date-parts":[[2011,9,1]]},"abstract":"<jats:p>Ti-rich PbZr1\u2212xTixO3 (x\u2009=\u20090.65, PZT65) single crystals with the dimensions of 1\u2009\u00d7\u20091\u2009\u00d7\u20090.2 mm3 were grown by the self-flux method. Micron-sized ferroelectric domains were observed and characterized via piezoresponse force microscopy (PFM) and switching spectroscopy PFM. Both out-of-plane and in-plane components of polarization were obtained by detecting vertical and lateral vibrations of the PFM cantilever. The piezoresponse image examination revealed a clear lamellar domain structure due to apparent twinning and the formation of 90\u00b0 domains. A negative self-polarization was observed in the studied crystals leading to the asymmetry of piezoresponse hysteresis loops and the polarization imprint. The polarization switching mechanism under the external electric field applied via a PFM tip was investigated. The 90\u00b0 domain wall width was determined from the local PFM measurements and tentatively attributed to the oblique domain walls and chemical disorder. The time-dependent PFM imaging revealed a slow polarization relaxation process with a characteristic time of about 200 min.<\/jats:p>","DOI":"10.1063\/1.3623768","type":"journal-article","created":{"date-parts":[[2011,9,2]],"date-time":"2011-09-02T14:37:08Z","timestamp":1314974228000},"update-policy":"https:\/\/doi.org\/10.1063\/aip-crossmark-policy-page","source":"Crossref","is-referenced-by-count":37,"title":["Ferroelectric domain structure of PbZr0.35Ti0.65O3 single crystals by piezoresponse force microscopy"],"prefix":"10.1063","volume":"110","author":[{"given":"I. K.","family":"Bdikin","sequence":"first","affiliation":[{"name":"University of Aveiro 1 Department of Mechanical Engineering & TEMA, , 3810-193 Aveiro, Portugal"}]},{"given":"J. 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