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Currently, zinc oxide (ZnO) is one of the most popular metal oxide semiconductors for VOCs detection but suffering from a lack of selectivity, poor response, and slow response\/recovery speeds. Herein, we successfully synthesized the ZnO\/Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> nanocomposites via a facile hydrothermal method, in which ZnO nanoparticles were uniformly grown on two-dimensional (2D) Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> nanosheets. As a result, the ZnO\/Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> nanocomposites showed a significant improvement in the ethanol-sensing performance, when it compared to the pure ZnO and Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> samples. In particular, ZnO doped with 5 mg of Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> showed an ultra-high response (79) to 100 ppm ethanol, a short response\/recovery time (22 s\/34 s to 50 ppm ethanol), a low limit of detection (1 ppm) and a long-term stability. The excellent ethanol sensing properties are mainly attributed to the coupling effect between ZnO and Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> of composites. The ZnO nanoparticles are uniformly distributed on the 2D Ti<jats:sub>3<\/jats:sub>C<jats:sub>2<\/jats:sub>T<jats:italic>\n                     <jats:sub>x<\/jats:sub>\n                  <\/jats:italic> platform, which can provide more gas adsorption sites. Simultaneously, the presence of hybrid heterojunctions further enhances the response in the sensing process.<\/jats:p>","DOI":"10.1088\/1361-6528\/aca8b1","type":"journal-article","created":{"date-parts":[[2022,12,5]],"date-time":"2022-12-05T17:11:27Z","timestamp":1670260287000},"page":"105707","update-policy":"https:\/\/doi.org\/10.1088\/crossmark-policy","source":"Crossref","is-referenced-by-count":13,"title":["The highly sensitive ethanol sensor based on nanocomposites of ZnO <i>in situ<\/i> grown on 2D Ti<sub>3<\/sub>C<sub>2<\/sub>T<i>\n                     <sub>x<\/sub>\n                  <\/i> nanosheet"],"prefix":"10.1088","volume":"34","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-4428-9382","authenticated-orcid":true,"given":"Xiangrui","family":"Bu","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1450-1557","authenticated-orcid":true,"given":"Qiang","family":"Wu","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yubin","family":"Yuan","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Haiyang","family":"Wu","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5748-3021","authenticated-orcid":true,"given":"Weihua","family":"Liu","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xin","family":"Li","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Chuanyu","family":"Han","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"266","published-online":{"date-parts":[[2022,12,23]]},"reference":[{"key":"nanoaca8b1bib1","doi-asserted-by":"publisher","first-page":"55","DOI":"10.1016\/j.snb.2017.12.167","type":"journal-article","article-title":"A highly sensitive gas-sensing platform based on a metal-oxide nanowire forest grown on a suspended carbon nanowire fabricated at a wafer level","volume":"260","author":"Lim","year":"2018","journal-title":"Sensors Actuators B"},{"key":"nanoaca8b1bib2","doi-asserted-by":"publisher","first-page":"6313","DOI":"10.1039\/C6CP07799D","type":"journal-article","article-title":"Metal-oxide-semiconductor based gas sensors: screening, preparation, and integration","volume":"19","author":"Zhang","year":"2017","journal-title":"Phys. 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