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Herein, a CdS-MnO<jats:sub>2<\/jats:sub> composite synthesized through a facile electrostatic self-assembly method was employed as an effective catalyst for photocatalytic CO<jats:sub>2<\/jats:sub> reduction. The engineered CdS-MnO<jats:sub>2<\/jats:sub> minimized the recombination of photogenerated electrons and holes, thereby facilitating the charge transfer and boosting the catalytic activity of pristine CdS. The introduction of NaOH solution into the reaction environment further enhanced the interfacial electron transfer and increased the affinity to the key intermediate *CO, facilitating additional multielectron reactions for methanol production. The alkaline characteristics of NaOH solution not only promotes the adsorption and activation of inert CO<jats:sub>2<\/jats:sub> molecules, but also function as hole scavengers, significantly reducing the photogenerated carrier recombination and further promoting the CO<jats:sub>2<\/jats:sub> reduction, especially in multielectron reactions towards methanol. A notable yield of 13.4 <jats:italic>\u03bc<\/jats:italic>mol g<jats:sup>\u22121<\/jats:sup> h<jats:sup>\u22121<\/jats:sup> for methanol and 7.6 <jats:italic>\u03bc<\/jats:italic>mol g<jats:sup>\u22121<\/jats:sup> h<jats:sup>\u22121<\/jats:sup> for CO was obtained with the CdS-MnO<jats:sub>2<\/jats:sub>. The results obtained herein may provide insights into the design of a highly efficient photocatalytic systems aimed at converting CO<jats:sub>2<\/jats:sub> into higher value-added products.<\/jats:p>","DOI":"10.1088\/1361-6528\/adbcb5","type":"journal-article","created":{"date-parts":[[2025,3,5]],"date-time":"2025-03-05T22:48:37Z","timestamp":1741214917000},"page":"165402","update-policy":"https:\/\/doi.org\/10.1088\/crossmark-policy","source":"Crossref","is-referenced-by-count":4,"title":["Boosted photocatalytic CO<sub>2<\/sub> reduction through interface engineering by constructing CdS-MnO<sub>2<\/sub> heterojunction"],"prefix":"10.1088","volume":"36","author":[{"ORCID":"https:\/\/orcid.org\/0009-0009-7006-3430","authenticated-orcid":true,"given":"Wenqiang","family":"Jiang","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shijie","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hui","family":"Li","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaoying","family":"Liu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Honglei","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0009-3256-7160","authenticated-orcid":true,"given":"Yunyi","family":"Xiao","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Runze","family":"Bi","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0002-0929-436X","authenticated-orcid":true,"given":"Siyuan","family":"Du","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0000-9713-271X","authenticated-orcid":true,"given":"Yawei","family":"Gu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"266","published-online":{"date-parts":[[2025,3,14]]},"reference":[{"key":"nanoadbcb5bib1","doi-asserted-by":"publisher","first-page":"690","DOI":"10.1038\/s41560-019-0431-1","article-title":"Selective visible-light-driven photocatalytic CO2 reduction to CH4 mediated by atomically thin CuIn5S8 layers","volume":"4","author":"Li","year":"2019","journal-title":"Nat. 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