{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,2,21]],"date-time":"2025-02-21T21:20:49Z","timestamp":1740172849168,"version":"3.37.3"},"reference-count":31,"publisher":"IOP Publishing","issue":"7","license":[{"start":{"date-parts":[[2023,7,19]],"date-time":"2023-07-19T00:00:00Z","timestamp":1689724800000},"content-version":"vor","delay-in-days":18,"URL":"http:\/\/creativecommons.org\/licenses\/by\/4.0\/"},{"start":{"date-parts":[[2023,7,19]],"date-time":"2023-07-19T00:00:00Z","timestamp":1689724800000},"content-version":"tdm","delay-in-days":18,"URL":"https:\/\/iopscience.iop.org\/info\/page\/text-and-data-mining"}],"content-domain":{"domain":["iopscience.iop.org"],"crossmark-restriction":false},"short-container-title":["Mater. Res. Express"],"published-print":{"date-parts":[[2023,7,1]]},"abstract":"Abstract<\/jats:title>\n It is presented a \u2018shocking thermal treatment\u2019 methodology as a modification to the molten salts process to rapidly obtain pure phase nickel ferrite nanoparticles within a high-scalable green synthesis scheme. Analysis from x-ray diffraction and electron microscopy (SEM and TEM) confirms the formation of the nanostructures, with the most frequent crystallite sizes between 55\u201385 nm. Room temperature magnetic characterization, from M\u00f6ssbauer spectroscopy and magnetic measurements M(H), evidences their superparamagnetic distribution with a magnetic saturation of 47.9 emu g\u22121<\/jats:sup>. An approximated stoichiometry of \n \n\n<\/jats:tex-math>\n \n \n \n \n \n \n \n Ni<\/mml:mi>\n <\/mml:mrow>\n \n 0.03<\/mml:mn>\n <\/mml:mrow>\n <\/mml:msub>\n \n \n Fe<\/mml:mi>\n <\/mml:mrow>\n \n 0.97<\/mml:mn>\n <\/mml:mrow>\n <\/mml:msub>\n <\/mml:mrow>\n <\/mml:mfenced>\n <\/mml:mrow>\n \n A<\/mml:mi>\n <\/mml:mrow>\n <\/mml:msub>\n \n \n \n \n \n \n Ni<\/mml:mi>\n <\/mml:mrow>\n \n 0.97<\/mml:mn>\n <\/mml:mrow>\n <\/mml:msub>\n \n \n Fe<\/mml:mi>\n <\/mml:mrow>\n \n 1.03<\/mml:mn>\n <\/mml:mrow>\n <\/mml:msub>\n <\/mml:mrow>\n <\/mml:mfenced>\n <\/mml:mrow>\n \n B<\/mml:mi>\n <\/mml:mrow>\n <\/mml:msub>\n \n \n O<\/mml:mi>\n <\/mml:mrow>\n \n 4<\/mml:mn>\n <\/mml:mrow>\n <\/mml:msub>\n <\/mml:math>\n \n <\/jats:inline-formula> was proposed from Rietveld refinement, M\u00f6ssbauer and energy-dispersive x-ray spectroscopies. The effect on the electronic structure due to the shocking thermal treatment was elucidated by estimating the optical band gap with values between 1.78 and 2.38 eV.<\/jats:p>","DOI":"10.1088\/2053-1591\/ace593","type":"journal-article","created":{"date-parts":[[2023,7,7]],"date-time":"2023-07-07T22:42:11Z","timestamp":1688769731000},"page":"076102","update-policy":"https:\/\/doi.org\/10.1088\/crossmark-policy","source":"Crossref","is-referenced-by-count":3,"title":["Rapid synthesis of nickel ferrite nanoparticles by the molten salt method"],"prefix":"10.1088","volume":"10","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-5518-5386","authenticated-orcid":false,"given":"J","family":"Le\u00f3n-Flores","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7126-6522","authenticated-orcid":true,"given":"J L","family":"P\u00e9rez-Mazariego","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"E T","family":"Olmedo-Res\u00e9ndiz","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"M L","family":"Marquina","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6876-0351","authenticated-orcid":true,"given":"R","family":"Escamilla","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3709-148X","authenticated-orcid":true,"given":"R","family":"G\u00f3mez","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"J","family":"Arenas-Alatorre","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"266","published-online":{"date-parts":[[2023,7,19]]},"reference":[{"key":"mrxace593bib1","doi-asserted-by":"publisher","first-page":"231","DOI":"10.1016\/j.jallcom.2010.04.152","volume":"502","author":"Fawzi","year":"2010","journal-title":"J. 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