{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,29]],"date-time":"2026-07-29T03:02:54Z","timestamp":1785294174556,"version":"3.55.0"},"reference-count":28,"publisher":"Oxford University Press (OUP)","issue":"7","license":[{"start":{"date-parts":[[2025,7,24]],"date-time":"2025-07-24T00:00:00Z","timestamp":1753315200000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/academic.oup.com\/pages\/standard-publication-reuse-rights"}],"funder":[{"name":"Research Project of Nanjing Customs","award":["2025KJ38"],"award-info":[{"award-number":["2025KJ38"]}]},{"DOI":"10.13039\/501100019939","name":"General Administration of Customs of the People's Republic of China","doi-asserted-by":"publisher","award":["2022HK063"],"award-info":[{"award-number":["2022HK063"]}],"id":[{"id":"10.13039\/501100019939","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100019939","name":"General Administration of Customs of the People's Republic of China","doi-asserted-by":"publisher","award":["2024HK094"],"award-info":[{"award-number":["2024HK094"]}],"id":[{"id":"10.13039\/501100019939","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2025,7,24]]},"abstract":"<jats:title>Abstract<\/jats:title>\n               <jats:p>A screening method was developed for the determination of per- and polyfluoroalkyl substances in textiles by combustion and ion chromatography. In this work, a new type of high-temperature combustion absorption device was designed, and the samples were burned, cracked and gasified by temperature programmed heating mode. The produced free fluorine and hydrogen fluoride gases were absorbed by water vapor and completely transformed into inorganic fluoride anion. After condensation and collection, it was separated and determined by ion chromatography. The pre-treatment conditions were optimized including the sample weight, the combustion method, the combustion gas and its flow rate, the water evaporation rate and the condensate collection method. Method validation was performed in negative samples of cotton, wool and polyester, at spiked levels of 5, 50 and 200\u00a0mg\/kg, respectively. The average recoveries were between 85.7 and 95.0% with relative standard deviations &amp;lt;20% (n\u2009=\u20097) indicating satisfactory accuracy and repeatability. The calibration curve was performed with the correlation coefficients (R2) higher than 0.999 within a linearity range of 0.01\u20132.0\u00a0mg\/L. The limit of quantification was 5.0\u00a0mg\/kg. The developed method was successfully used to determine the total fluorine in market samples. It can meet the screening determination of PFAS in various textiles.<\/jats:p>","DOI":"10.1093\/chromsci\/bmaf043","type":"journal-article","created":{"date-parts":[[2025,7,25]],"date-time":"2025-07-25T04:52:11Z","timestamp":1753419131000},"source":"Crossref","is-referenced-by-count":1,"title":["Screening Method for the Determination of per- and Polyfluoroalkyl Substances (PFAS) in Textiles by Combustion and Ion Chromatography"],"prefix":"10.1093","volume":"63","author":[{"ORCID":"https:\/\/orcid.org\/0009-0007-8935-8277","authenticated-orcid":false,"given":"Lihua","family":"Cao","sequence":"first","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Youchao","family":"Ding","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Kai","family":"Qian","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiangxiang","family":"Wang","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiaoqiong","family":"Wang","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jia","family":"Zhou","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Juan","family":"Tang","sequence":"additional","affiliation":[{"name":"Industrial Products Testing Center , Nanjing Customs, No. 39, Chuangzhi Road, Jianye District, Nanjing 210019 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"286","published-online":{"date-parts":[[2025,7,25]]},"reference":[{"issue":"4","key":"2025072500520508500_ref1","doi-asserted-by":"crossref","first-page":"513","DOI":"10.1002\/ieam.258","article-title":"Perfluoroalkyl and polyfluoroalkyl substances in the environment: Terminology, classification, and origins","volume":"7","author":"Buck","year":"2011","journal-title":"Integrated Environmental Assessment and Management"},{"issue":"12","key":"2025072500520508500_ref2","doi-asserted-by":"publisher","first-page":"2345","DOI":"10.1039\/d0em00291g","article-title":"An overview of the uses of per- and polyfluoroalkyl substances (PFAS)","volume":"22","author":"Gl\u00fcge","year":"2020","journal-title":"Environmental Science: Processes Impacts"},{"issue":"12","key":"2025072500520508500_ref3","first-page":"2307","article-title":"The high persistence of PFAS is sufficient for their management as a chemical class","volume":"22","author":"Cousins","year":"2020","journal-title":"Environmental Science: Processes Impacts"},{"issue":"3","key":"2025072500520508500_ref4","doi-asserted-by":"crossref","first-page":"543","DOI":"10.1002\/etc.4784","article-title":"Estimating environmental hazard and risks from exposure to per- and polyfluoroalkyl substances (PFAS): Outcome of a SETAC focused topic meeting","volume":"40","author":"Johnson","year":"2020","journal-title":"Environmental Toxicology and Chemistry"},{"issue":"1\u20132","key":"2025072500520508500_ref5","doi-asserted-by":"crossref","first-page":"100879","DOI":"10.1016\/j.eti.2020.100879","article-title":"Recent advances in the analysis of per- and polyfluoroalkyl substances (PFAS)\u2014A review","volume":"19","author":"Amin","year":"2020","journal-title":"Environmental Technology & Innovation"},{"key":"2025072500520508500_ref6","doi-asserted-by":"crossref","first-page":"142044","DOI":"10.1016\/j.chemosphere.2024.142044","article-title":"Per-and polyfluoroalkyl (PFAS) eternal pollutants: Sources, environmental impacts and treatment processes","volume":"358","author":"Rekik","year":"2024","journal-title":"Chemosphere"},{"key":"2025072500520508500_ref7","doi-asserted-by":"publisher","first-page":"437","DOI":"10.1016\/j.psep.2024.01.005","article-title":"PFAS in textile wastewater: An integrated scenario analysis for interventions prioritization to reduce environmental risk","volume":"183","author":"Cantoni","year":"2024","journal-title":"Process Safety and Environmental Protection"},{"issue":"82\u201389","key":"2025072500520508500_ref8","first-page":"93","article-title":"History, current situation and future of water- and oil- repellents for textiles","volume":"5","author":"Tu","year":"2022","journal-title":"China Dyeing & Finishing"},{"issue":"6580","key":"2025072500520508500_ref9","doi-asserted-by":"crossref","first-page":"512","DOI":"10.1126\/science.abg9065","article-title":"Per- and polyfluoroalkyl substances in the environment","volume":"375","author":"Evich","year":"2022","journal-title":"Science"},{"key":"2025072500520508500_ref10","doi-asserted-by":"crossref","first-page":"100086","DOI":"10.1016\/j.hazl.2023.100086","article-title":"Per- and polyfluoroalkyl substances (PFAS) in consumer products: Current knowledge and research gaps","volume":"4","author":"Dewapriya","year":"2023","journal-title":"Journal of Hazardous Materials 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REACH Annex XII-Substances restricted under REACH (01.08.2024)"},{"key":"2025072500520508500_ref13","author":"AB-1817 Product safety: textile articles: perfluoroalkyl and polyfluoroalkyl substances (PFAS)","year":"2021-2022"},{"key":"2025072500520508500_ref14","author":"OEKO-TEX\u00ae. OEKO-TEX STANDARD 100 (Edition 02. 2024, 01.04.2024)."},{"issue":"2","key":"2025072500520508500_ref15","first-page":"1","article-title":"Interpretation of the list of new pollutants under key control (2023 edition)","volume":"40","author":"Wang","year":"2023","journal-title":"Textile Auxiliaries"},{"issue":"2","key":"2025072500520508500_ref16","first-page":"321","article-title":"Simultaneous determination and exposure assessment of 12 volatile per- and polyfluoroalkyl substances in infant and child textiles","volume":"44","author":"Li","year":"2023","journal-title":"Journal of Chinese Mass Spectrometry Society"},{"key":"2025072500520508500_ref17","first-page":"21","article-title":"Determination of perfluorinated compounds by liquid chromatography-tandem mass spectrometry","volume":"5","author":"Zhang","year":"2020","journal-title":"Textile Testing and Standard"},{"key":"2025072500520508500_ref18","doi-asserted-by":"crossref","first-page":"465041","DOI":"10.1016\/j.chroma.2024.465041","article-title":"A sensitive method for the determination of per- and polyfluoroalkyl substances in food and food contact material using high-performance liquid chromatography coupled with tandem mass spectrometry","volume":"1730","author":"A\u00dfhoff","year":"2024","journal-title":"Journal of Chromatography A"},{"key":"2025072500520508500_ref19","doi-asserted-by":"crossref","first-page":"129","DOI":"10.1016\/j.talanta.2017.09.008","article-title":"Carboxylated carbon nanospheres as solid-phase extraction adsorbents for the determination of perfluorinated compounds in water samples by liquid chromatography\u2013tandem mass spectrometry","volume":"178","author":"Wang","year":"2018","journal-title":"Talanta"},{"key":"2025072500520508500_ref20","doi-asserted-by":"crossref","first-page":"123365","DOI":"10.1016\/j.jchromb.2022.123365","article-title":"Optimization and application of a method to determine 24 perfluorinated compounds in umbilical cord serum by using liquid chromatography tandem mass spectrometry","volume":"1207","author":"Liu","year":"2022","journal-title":"Journal of Chromatography B"},{"key":"2025072500520508500_ref21","author":"Environmental Protection Agency","year":"2021"},{"issue":"5","key":"2025072500520508500_ref22","doi-asserted-by":"crossref","first-page":"525","DOI":"10.1080\/19440049.2024.2332334","article-title":"Analysis of per- and polyfluoroalkyl substances (PFAS) in raw materialsintended for the production of paper-based food contact materials\u2013evaluating LC-MS\/MS versus total fluorine and extractable organic fluorine","volume":"41","author":"Jovanovi\u0107","year":"2024","journal-title":"Food Additives & Contaminants: Part A"},{"key":"2025072500520508500_ref23","first-page":"1298","article-title":"Non-extractable PFAS in functional textiles \u2013 Characterization by complementary methods: Oxidation, hydrolysis, and fluorine sum parameters","volume":"25","author":"Zweigle","year":"2023","journal-title":"Environmental Science: Processes & Impacts"},{"key":"2025072500520508500_ref24","doi-asserted-by":"crossref","first-page":"353","DOI":"10.1016\/j.talanta.2016.02.022","article-title":"Fast and simple determination of perfluorinated compounds and their potential precursors in different packaging materials","volume":"152","author":"Zabaleta","year":"2016","journal-title":"Talanta"},{"key":"2025072500520508500_ref25","first-page":"1","article-title":"1-background and type of textile materials processed in textile industry","author":"Vhanbatte","year":"2022","journal-title":"Applications of Biotechnology for Sustainable Textile Production"},{"key":"2025072500520508500_ref26","volume-title":"Pulp, paper and board \u2014 Determination of total chlorine and organically bound chlorine","year":"2017"},{"key":"2025072500520508500_ref27","volume-title":"Water quality \u2014 Determination of adsorbable organically bound halogens (AOX)","year":"2004"},{"key":"2025072500520508500_ref28","author":"EN 14582: 2016. Characterization of Waste \u2014 Halogen and Sulfur Content \u2014 Oxygen Combustion in Closed Systems and Determination Methods"}],"container-title":["Journal of Chromatographic Science"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/academic.oup.com\/chromsci\/article-pdf\/63\/7\/bmaf043\/63842876\/bmaf043.pdf","content-type":"application\/pdf","content-version":"vor","intended-application":"syndication"},{"URL":"https:\/\/academic.oup.com\/chromsci\/article-pdf\/63\/7\/bmaf043\/63842876\/bmaf043.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,7,25]],"date-time":"2025-07-25T04:52:14Z","timestamp":1753419134000},"score":1,"resource":{"primary":{"URL":"https:\/\/academic.oup.com\/chromsci\/article\/doi\/10.1093\/chromsci\/bmaf043\/8212020"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2025,7,24]]},"references-count":28,"journal-issue":{"issue":"7","published-print":{"date-parts":[[2025,7,24]]}},"URL":"https:\/\/doi.org\/10.1093\/chromsci\/bmaf043","relation":{},"ISSN":["0021-9665","1945-239X"],"issn-type":[{"value":"0021-9665","type":"print"},{"value":"1945-239X","type":"electronic"}],"subject":[],"published-other":{"date-parts":[[2025,8]]},"published":{"date-parts":[[2025,7,24]]},"article-number":"bmaf043"}}