{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,5,14]],"date-time":"2026-05-14T22:19:50Z","timestamp":1778797190196,"version":"3.51.4"},"reference-count":40,"publisher":"Oxford University Press (OUP)","issue":"4","license":[{"start":{"date-parts":[[2025,12,24]],"date-time":"2025-12-24T00:00:00Z","timestamp":1766534400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"name":"Jilin Province Science and Technology Development Program","award":["20240101019JC"],"award-info":[{"award-number":["20240101019JC"]}]},{"name":"Hong Kong Research Grant Council","award":["C6011-20GF and JLFS\/P-602\/24"],"award-info":[{"award-number":["C6011-20GF and JLFS\/P-602\/24"]}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,2,5]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>Aqueous-phase reforming of methanol (APRM) offers a promising route for efficient hydrogen generation and safe transportation, yet it typically requires harsh conditions (above 200\u00b0C, 25\u201350\u00a0bar) and energy-intensive purification. Here, we report a heterogeneous catalyst featuring synergistic Ir single-atom and cluster dual sites that enables efficient hydrogen production from methanol and water at record-low temperatures (75\u00b0C\u201395\u00b0C) and ambient pressure. This unique ensemble effect drives a tandem reaction pathway, with Ir clusters promoting methanol dehydrogenation to formic acid, while adjacent Ir single atoms facilitate rapid formic acid decomposition into H2 and CO2 to suppress CO intermediates. As a result, the developed catalyst achieves a remarkable hydrogen production rate of 346.9\u00a0molH2\u00a0molIr\u22121\u00a0h\u22121 and 100% H2 selectivity with no detectable CO formation. To the best of our knowledge, this represents one of the lowest temperature ranges demonstrated for efficient methanol-to-hydrogen conversion via heterogeneous catalysis, advancing methanol as a practical liquid H2 carrier for on-demand high-purity hydrogen production.<\/jats:p>","DOI":"10.1093\/nsr\/nwaf585","type":"journal-article","created":{"date-parts":[[2025,12,24]],"date-time":"2025-12-24T12:08:31Z","timestamp":1766578111000},"source":"Crossref","is-referenced-by-count":2,"title":["Low-temperature aqueous-phase dehydrogenation of methanol catalyzed by synergistic Ir single-atom and cluster dual sites"],"prefix":"10.1093","volume":"13","author":[{"given":"Xiaohui","family":"Liu","sequence":"first","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xin","family":"Guan","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xiaolong","family":"Jia","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jingsen","family":"Bai","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Wenjing","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Chemistry and Life Science, Changchun University of Technology , Changchun 130022 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xinying","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jianbing","family":"Zhu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]},{"name":"CIAC-HKUST Joint Laboratory for Hydrogen Energy , Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Minhua","family":"Shao","sequence":"additional","affiliation":[{"name":"Department of Chemical and Biological Engineering, The Hong Kong University of Science and Technology , Hong Kong 999077 ,","place":["China"]},{"name":"CIAC-HKUST Joint Laboratory for Hydrogen Energy, Energy Institute, The Hong Kong University of Science and Technology , Hong Kong 999077 ,","place":["China"]},{"name":"Guangzhou Key Laboratory of Electrochemical Energy Storage Technologies, Fok Ying Tung Research Institute, The Hong Kong University of Science and Technology , Guangzhou 511458 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Changpeng","family":"Liu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]},{"name":"CIAC-HKUST Joint Laboratory for Hydrogen Energy , Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 ,","place":["China"]}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Meiling","family":"Xiao","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Electroanalytic Chemistry, Jilin Province Key Laboratory of Low Carbon Chemistry Power, Jilin Provincial Science and Technology Innovation Center of Hydrogen Energy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences , Changchun 130022 ,","place":["China"]},{"name":"School of Applied Chemistry and Engineering, University of Science and Technology of China , Hefei 230026 ,","place":["China"]},{"name":"CIAC-HKUST Joint Laboratory for Hydrogen Energy , Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 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