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Yet, up to now the aromatic product selectivity typically remains below 50%, mainly limited by competing hydrogenolysis. We report here a cascade process that combines the selective aerobic oxidation of hydrogen, in situ generated from PE via cleavage of C(sp3)\u2013H, with oxygen and the endothermic aromatization of PE. Our tandem aerobic oxidation\u2013aromatization approach boosts the catalytic activity at moderate temperatures of up to 280\u00b0C in ambient air. Concurrently, hydrogen removal shifts the chemical equilibrium favorably toward formation of aromatic products, achieving an aromatic selectivity of 78 mol%. Demonstrated on a near kilogram scale with upscaled catalysts under mild conditions, our approach offers a scalable, energy-efficient solution for the high-selectivity conversion of plastic waste into valuable chemical intermediates and solvents.<\/jats:p>","DOI":"10.1093\/nsr\/nwag207","type":"journal-article","created":{"date-parts":[[2026,4,2]],"date-time":"2026-04-02T11:47:07Z","timestamp":1775130427000},"source":"Crossref","is-referenced-by-count":1,"title":["Oxygen-mediated tandem polyethylene upcycling for selective aromatic synthesis"],"prefix":"10.1093","volume":"13","author":[{"given":"Shengming","family":"Li","sequence":"first","affiliation":[{"name":"State Key Laboratory of Bioinspired Interfacial Materials Science, Institute of Functional Nano & Soft Materials (FUNSOM), Soochow University , Suzhou 215123 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Weilin","family":"Tu","sequence":"additional","affiliation":[{"name":"State Key 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