{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,21]],"date-time":"2026-09-21T13:11:48Z","timestamp":1789996308587,"version":"4.0.1"},"reference-count":53,"publisher":"Oxford University Press (OUP)","issue":"17","license":[{"start":{"date-parts":[[2026,6,11]],"date-time":"2026-06-11T00:00:00Z","timestamp":1781136000000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["22379168"],"award-info":[{"award-number":["22379168"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,9,7]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>The electrochemical stability of metastable lithium-rich layered cathodes is intrinsically governed by their synthetic history, yet the correlation between ion-exchange thermodynamics and structural evolution remains elusive. Here, using layered P3-Na0.6[Li0.2Mn0.8]O2 as a precursor, the spontaneous ion-exchange synthesis of O3-Li0.6[Li0.2Mn0.8]O2 (O3-LLM RT) at room temperature yields one of the most promising layered Li\u2013Mn\u2013O cathodes reported to date in LiPF6-based carbonate electrolyte at room temperature. However, elevated synthesis temperatures induce manganese ion migration, which hinders the reversible interlayer migration of Li+ into the transition metal layers. This structural impediment triggers irreversible lattice oxygen activation and degrades structural stability (e.g. at 280\u00b0C, denoted the high-temperature O3-LLM sample as (O3-LLM HT)). Consequently, the perfect layered O3-LLM RT cathode exhibits a high specific capacity of 250 mAh\/g with an excellent cycling stability of 88.1% capacity retention (vs. the 51.9% for O3-LLM HT) after 400 cycles at 2.0\u20134.8\u00a0V, ranking at the top of the Li\u2013Mn\u2013O layered cathodes. These findings provide insights into the design and optimization of metastable materials for high-energy-density batteries.<\/jats:p>","DOI":"10.1093\/nsr\/nwag356","type":"journal-article","created":{"date-parts":[[2026,6,11]],"date-time":"2026-06-11T11:49:15Z","timestamp":1781178555000},"source":"Crossref","is-referenced-by-count":0,"title":["Sustainable high-energy-density Li\u2013Mn\u2013O layered cathode via metastable synthetic kinetics"],"prefix":"10.1093","volume":"13","author":[{"given":"Yuansheng","family":"Shi","sequence":"first","affiliation":[{"name":"School of Materials, Sun Yat-sen University , Shenzhen 518107 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fushan","family":"Geng","sequence":"additional","affiliation":[{"name":"Shanghai Key Laboratory of Magnetic Resonance, Institute of Magnetic Resonance and Molecular Imaging in Medicine, School of Physics, East China Normal University , Shanghai 200421 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