{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,19]],"date-time":"2026-10-19T13:55:35Z","timestamp":1792418135481,"version":"4.4.0"},"reference-count":51,"publisher":"Oxford University Press (OUP)","issue":"19","license":[{"start":{"date-parts":[[2026,7,11]],"date-time":"2026-07-11T00:00:00Z","timestamp":1783728000000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["92161202"],"award-info":[{"award-number":["92161202"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["22121005"],"award-info":[{"award-number":["22121005"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["22271159"],"award-info":[{"award-number":["22271159"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2026,10,5]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>As a pivotal industrial chemical, adipic acid (AA) is synthesizable through the electrocatalytic oxidation of cyclohexanol under ambient conditions, utilizing electrons as a clean oxidant. This approach circumvents the energy-intensive and environmentally detrimental nature of conventional petrochemical processes, thereby offering a sustainable alternative for AA production. However, existing electrocatalysts are often plagued by instability in alkaline media, and their structure\u2013activity relationships remain poorly understood. Here, we report a novel [Ni36] nanocage-based metal-organic framework ([Ni9]-MOF) synthesized via a bottom-up strategy from discrete [Ni9]-clusters, exhibiting excellent stability under both strong alkaline (8\u00a0M NaOH) and acidic (1\u00a0M HCl) conditions. [Ni9]-MOF demonstrates superior AA production (0.1239\u00a0mmol h\u22121\u00a0cm\u22122 at 1.61\u00a0V), and maintains this high activity over 25 cycles with negligible loss, surpassing all prior high-performance catalysts in durability. Mechanistic studies reveal a three-step oxidation pathway via cyclohexanone, 2-hydroxycyclohexanone and 6-hydroxyadipic acid. Density functional theory calculations indicate the MOF framework enhances the charge density at the active [Ni9] site, accelerating reaction kinetics. This work not only provides a rational design strategy for constructing highly stable MOFs, but also presents the first MOF-based electrocatalyst for AA synthesis, opening new avenues for sustainable chemical production under mild conditions.<\/jats:p>","DOI":"10.1093\/nsr\/nwag427","type":"journal-article","created":{"date-parts":[[2026,7,10]],"date-time":"2026-07-10T11:53:58Z","timestamp":1783684438000},"source":"Crossref","is-referenced-by-count":0,"title":["Highly recyclable and efficient electrocatalytic synthesis of adipic acid catalyzed by ultra-alkali-resistant [Ni36] nanocages in MOF"],"prefix":"10.1093","volume":"13","author":[{"given":"Ze-Long","family":"Liang","sequence":"first","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rui","family":"Li","sequence":"additional","affiliation":[{"name":"School of Medicine, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhen-Ting","family":"Wang","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jia-Can","family":"Lv","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin-Min","family":"Ai","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qi","family":"Li","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ying-Ying","family":"Yu","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yang-Xi","family":"Wang","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fang-Ting","family":"Zhu","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qi-Fan","family":"Wang","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hang","family":"Xu","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bin","family":"Zhao","sequence":"additional","affiliation":[{"name":"Frontiers Science Center for New Organic Matter, Key Laboratory of Advanced Energy Materials Chemistry (MOE), College of Chemistry, Nankai University , Tianjin 300071 ,","place":["China"]},{"name":"Ganjiang Innovation Academy, Jiangxi Institute of Rare Earths, Chinese Academy of Sciences , Ganzhou 341000 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