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Until now, cumulative bonds beyond triple multiplicity have neither been experimentally isolated nor theoretically predicted. Here, we propose a new bonding model\u2014cumulative quintuple bonds\u2014and report the synthesis and characterization of a novel trinuclear species, [Co\u2013U\u2013Co], which exhibits bonding interactions approaching cumulative quintuple bonds. Advanced quantum chemical calculations reveal that the cumulative multiple bonds consist of one pair of U\u2013Co \u03c3 bonds, two pairs of U\u2013Co \u03c0 bonds, one pair of U\u2013Co \u03b4 bonds, a three-center-two-electron \u03b4 bond and a \u03b4 hyperconjugation. This species represents the first example of an all-metal uranyl analog featuring a linear M\u2013U\u2013M core with cumulative multiple bonds. This discovery not only extends the theoretical boundaries of cumulative multiple bonds but also establishes a transformative precedent for cumulative bonding multiplicity in trinuclear species.<\/jats:p>","DOI":"10.1093\/nsr\/nwag462","type":"journal-article","created":{"date-parts":[[2026,7,30]],"date-time":"2026-07-30T11:58:19Z","timestamp":1785412699000},"source":"Crossref","is-referenced-by-count":0,"title":["Approaching cumulative quintuple bonds in all-metal uranyl analogs"],"prefix":"10.1093","volume":"13","author":[{"given":"Xingxing","family":"Gong","sequence":"first","affiliation":[{"name":"State Key Laboratory of Coordination Chemistry, Jiangsu Key Laboratory of Advanced Organic Materials, School of Chemistry and Chemical Engineering, Nanjing University , Nanjing 210023 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