{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,1,14]],"date-time":"2025-01-14T05:10:27Z","timestamp":1736831427509,"version":"3.33.0"},"reference-count":16,"publisher":"International Union of Crystallography (IUCr)","issue":"12","license":[{"start":{"date-parts":[[2013,11,8]],"date-time":"2013-11-08T00:00:00Z","timestamp":1383868800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/journals.iucr.org\/services\/copyrightpolicy.html"},{"start":{"date-parts":[[2013,11,8]],"date-time":"2013-11-08T00:00:00Z","timestamp":1383868800000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/journals.iucr.org\/services\/copyrightpolicy.html#TDM"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr C Cryst Struct Commun","Acta Cryst C","Acta Cryst Sect C","Acta Crystallogr C","Acta Crystallogr Sect C","Acta Crystallogr Sect C Cryst Struct Commun"],"published-print":{"date-parts":[[2013,12,1]]},"abstract":"<jats:p>The distorted octahedral title complex, [V<jats:sup>V<\/jats:sup>(C<jats:sub>3<\/jats:sub>H<jats:sub>7<\/jats:sub>O)(C<jats:sub>3<\/jats:sub>H<jats:sub>8<\/jats:sub>O)<jats:sub>2<\/jats:sub>F<jats:sub>2<\/jats:sub>O], was synthesized<jats:italic>via<\/jats:italic>ligand exchange at [V<jats:sup>V<\/jats:sup>O(OiPr)<jats:sub>3<\/jats:sub>] with aqueous hydrogen fluoride in propan-2-ol and crystallized from (D)chloroform at 238\u2005K after a few weeks. 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