{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,11,2]],"date-time":"2025-11-02T10:19:18Z","timestamp":1762078758437,"version":"3.32.0"},"reference-count":0,"publisher":"International Union of Crystallography (IUCr)","issue":"6","license":[{"start":{"date-parts":[[2005,11,14]],"date-time":"2005-11-14T00:00:00Z","timestamp":1131926400000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/journals.iucr.org\/services\/copyrightpolicy.html"},{"start":{"date-parts":[[2005,11,14]],"date-time":"2005-11-14T00:00:00Z","timestamp":1131926400000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/journals.iucr.org\/services\/copyrightpolicy.html#TDM"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr B Struct Sci","Acta Cryst B","Acta Cryst Sect B","Acta Crystallogr B","Acta Crystallogr Sect B","Acta Crystallogr Sect B Struct Sci"],"accepted":{"date-parts":[[2005,9,9]]},"published-print":{"date-parts":[[2005,12,1]]},"abstract":"<jats:p>The title compound poly[[bis(\u03bc-2-carboxylatoethylphosphonato)cadmium] dihydrate], Cd<jats:sub>3<\/jats:sub>(O<jats:sub>3<\/jats:sub>PC<jats:sub>2<\/jats:sub>H<jats:sub>4<\/jats:sub>CO<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>\u00b72H<jats:sub>2<\/jats:sub>O, was prepared by a hydrothermal reaction and its crystal structure determined from in-house powder data. The structure was solved in both <jats:italic>P<\/jats:italic>2<jats:sub>1<\/jats:sub>\/<jats:italic>c<\/jats:italic> and <jats:italic>P<\/jats:italic>2<jats:sub>1<\/jats:sub> space groups. The refinement converged with <jats:italic>R<jats:sub>p<\/jats:sub>\n                  <\/jats:italic> = 0.1046, <jats:italic>R<\/jats:italic>\n                  <jats:sub>wp<\/jats:sub> = 0.1378 and <jats:italic>R<jats:sub>f<\/jats:sub>\n                  <\/jats:italic> = 0.0763 in <jats:italic>P<\/jats:italic>2<jats:sub>1<\/jats:sub>\/<jats:italic>c<\/jats:italic>. However, the solid-state NMR data could not be explained. The structure was then solved in <jats:italic>P<\/jats:italic>2<jats:sub>1<\/jats:sub> and the refinement converged with <jats:italic>R<jats:sub>p<\/jats:sub>\n                  <\/jats:italic> = 0.0750, <jats:italic>R<\/jats:italic>\n                  <jats:sub>wp<\/jats:sub> = 0.1022 and <jats:italic>R<jats:sub>f<\/jats:sub>\n                  <\/jats:italic> = 0.0409 and satisfied the NMR requirements.<\/jats:p>","DOI":"10.1107\/s0108768105028387","type":"journal-article","created":{"date-parts":[[2005,11,23]],"date-time":"2005-11-23T14:56:27Z","timestamp":1132757787000},"page":"669-674","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":9,"title":["Structural characterization of Cd<sub>3<\/sub>(O<sub>3<\/sub>PC<sub>2<\/sub>H<sub>4<\/sub>CO<sub>2<\/sub>)<sub>2<\/sub>\u00b72H<sub>2<\/sub>O from in-house X-ray powder data and NMR"],"prefix":"10.1107","volume":"61","author":[{"given":"Naima","family":"Bestaoui","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xiang","family":"Ouyang","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Florence","family":"Fredoueil","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Bruno","family":"Bujoli","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Abraham","family":"Clearfield","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2005,11,14]]},"container-title":["Acta Crystallographica Section B Structural Science"],"original-title":[],"link":[{"URL":"http:\/\/journals.iucr.org\/b\/issues\/2005\/06\/00\/bs5017\/bs5017.pdf","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"http:\/\/journals.iucr.org\/b\/issues\/2005\/06\/00\/bs5017\/bs5017.pdf","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,1,11]],"date-time":"2025-01-11T13:43:55Z","timestamp":1736603035000},"score":1,"resource":{"primary":{"URL":"https:\/\/journals.iucr.org\/paper?S0108768105028387"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2005,11,14]]},"references-count":0,"journal-issue":{"issue":"6","published-print":{"date-parts":[[2005,12]]}},"alternative-id":["S0108768105028387"],"URL":"https:\/\/doi.org\/10.1107\/s0108768105028387","relation":{"is-supplemented-by":[{"id-type":"doi","id":"10.1107\/S0108768105028387\/bs5017sup1.cif","asserted-by":"subject"},{"id-type":"doi","id":"10.1107\/S0108768105028387\/bs5017sup2.rtv","asserted-by":"subject"},{"id-type":"doi","id":"10.1107\/S0108768105028387\/bs5017sup3.hkl","asserted-by":"subject"}]},"ISSN":["0108-7681"],"issn-type":[{"type":"print","value":"0108-7681"}],"subject":[],"published":{"date-parts":[[2005,11,14]]},"assertion":[{"value":"Acta Crystallographica Section B: Structural Science","order":0,"name":"journal","label":"Publication","explanation":{"URL":"http:\/\/journals.iucr.org\/b"},"group":{"name":"general","label":"General"}},{"value":"research papers","order":1,"name":"content_type","label":"Content type","explanation":{"URL":"https:\/\/journals.iucr.org\/b\/services\/notesforauthors.html"},"group":{"name":"general","label":"General"}},{"value":"Available","URL":"http:\/\/scripts.iucr.org\/cgi-bin\/citedin?bs5017","order":2,"name":"article_metrics","label":"Article metrics","group":{"name":"general","label":"General"}},{"value":"Yes","order":0,"name":"peer_reviewed","label":"Peer reviewed","group":{"name":"peer_review","label":"Peer review"}},{"value":"Single blind","order":1,"name":"review_process","label":"Review process","group":{"name":"peer_review","label":"Peer review"}},{"value":"11 April 2005","order":0,"name":"received","label":"Received","group":{"name":"publication_history","label":"Publication history"}},{"value":"9 September 2005","order":1,"name":"accepted","label":"Accepted","group":{"name":"publication_history","label":"Publication history"}},{"value":"14 November 2005","order":2,"name":"published_online","label":"Published online","group":{"name":"publication_history","label":"Publication history"}},{"value":"This article has supporting information","name":"supplementary_materials","label":"Supplementary materials","explanation":{"URL":"http:\/\/scripts.iucr.org\/cgi-bin\/sendsup?bs5017"}},{"value":"\u00a9 2005 International Union of Crystallography","order":0,"name":"copyright","label":"Copyright","explanation":{"URL":"http:\/\/journals.iucr.org\/services\/copyrightpolicy.html"},"group":{"name":"copyright_and_licensing","label":"Copyright and licencing"}}]}}