{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,1,12]],"date-time":"2025-01-12T05:18:48Z","timestamp":1736659128983,"version":"3.32.0"},"reference-count":5,"publisher":"International Union of Crystallography (IUCr)","issue":"9","license":[{"start":{"date-parts":[[2008,8,9]],"date-time":"2008-08-09T00:00:00Z","timestamp":1218240000000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"},{"start":{"date-parts":[[2008,8,9]],"date-time":"2008-08-09T00:00:00Z","timestamp":1218240000000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Struct Rep Online","Acta Crystallogr E","Acta Cryst E","Acta Cryst E Struct Rep Online","Acta Cryst Sect E","Acta Cryst Sect E Struct Rep Online","Acta Crystallogr Sect E","Acta Crystallogr Sect E Struct Rep Online"],"accepted":{"date-parts":[[2008,8,1]]},"published-print":{"date-parts":[[2008,9,1]]},"abstract":"<jats:p>The title compound, C<jats:sub>8<\/jats:sub>H<jats:sub>10<\/jats:sub>N<jats:sub>8<\/jats:sub>S<jats:sub>2<\/jats:sub>\u00b72C<jats:sub>2<\/jats:sub>H<jats:sub>6<\/jats:sub>SO, was obtained unintentionally during an attempt to prepare a thiolate derivative of trimethyltin. The complete disulfide molecule is generated by twofold rotation symmetry and the C\u2014S\u2014S\u2014C torsion angle around the S\u2014S bond is \u221285.70\u2005(10)\u00b0. The molecules are connected <jats:italic>via<\/jats:italic> N\u2014H...N hydrogen bonds into strongly corrugated layers parallel to (001), generating an <jats:italic>R<\/jats:italic>\n                  <jats:sub>2<\/jats:sub>\n                  <jats:sup>2<\/jats:sup>(8) motif. The solvent molecule, which exhibits minor disorder of its S atom [site occupancies = 0.9591\u2005(18) and 0.0409\u2005(18)], is linked to this layer <jats:italic>via<\/jats:italic> a pair of N\u2014H...O interactions.<\/jats:p>","DOI":"10.1107\/s160053680802480x","type":"journal-article","created":{"date-parts":[[2008,8,7]],"date-time":"2008-08-07T16:18:19Z","timestamp":1218125899000},"page":"o1724-o1724","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":1,"title":["Bis(4,6-diaminopyrimidin-2-yl) disulfide dimethyl sufoxide disolvate"],"prefix":"10.1107","volume":"64","author":[{"given":"Ephthymia","family":"Papastavrou","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Saleh","family":"Shakhatreh","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Pericles D.","family":"Akrivos","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Maria","family":"Gdaniec","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2008,8,9]]},"reference":[{"key":"hb2773_bb1","doi-asserted-by":"crossref","first-page":"453","DOI":"10.1107\/S002188980600731X","volume":"39","author":"Macrae","year":"2006","journal-title":"J. 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