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The synthesis was carried out in the temperature range from 690 to 700\u2005K and at the general pressure of 480\u2013500\u2005atm [1\u2005atm = 101.325\u2005kPa] from the mixture in the molar ratio 2CuO:CaO:Rb<jats:sub>2<\/jats:sub>O:B<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub>:P<jats:sub>2<\/jats:sub>O<jats:sub>5<\/jats:sub>. The crystals studied by single-crystal X-ray analysis were found to be monoclinic, space group <jats:italic>C<\/jats:italic>2, <jats:italic>a<\/jats:italic> = 16.8913\u2005(4), <jats:italic>b<\/jats:italic> = 5.6406\u2005(1), <jats:italic>c<\/jats:italic> = 8.3591\u2005(3)\u2005\u00c5, \u03b2 = 93.919\u2005(3)\u00b0, <jats:italic>V<\/jats:italic> = 794.57\u2005(4)\u2005\u00c5<jats:sup>3<\/jats:sup>. The crystal structure of Rb<jats:sub>2<\/jats:sub>CaCu<jats:sub>6<\/jats:sub>(PO<jats:sub>4<\/jats:sub>)<jats:sub>4<\/jats:sub>O<jats:sub>2<\/jats:sub> is similar to that of shchurovskyite and dmisokolovite and is based upon a heteropolyhedral open framework formed by polar layers of copper polyhedra linked <jats:italic>via<\/jats:italic> isolated PO<jats:sub>4<\/jats:sub> tetrahedra. The presence of well-isolated 2D heteropolyhedral layers in the title compound suggests low-dimensional magnetic behavior which is masked, however, by the fierce competition between multiple ferromagnetic and antiferromagnetic exchange interactions. At <jats:italic>T<\/jats:italic>\n                  <jats:sub>C<\/jats:sub> = 25\u2005K, Rb<jats:sub>2<\/jats:sub>CaCu<jats:sub>6<\/jats:sub>(PO<jats:sub>4<\/jats:sub>)<jats:sub>4<\/jats:sub>O<jats:sub>2<\/jats:sub> reaches a magnetically ordered state with large residual magnetization.<\/jats:p>","DOI":"10.1107\/s2052520619008527","type":"journal-article","created":{"date-parts":[[2019,9,25]],"date-time":"2019-09-25T12:56:51Z","timestamp":1569416211000},"page":"903-913","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":4,"title":["Rb<sub>2<\/sub>CaCu<sub>6<\/sub>(PO<sub>4<\/sub>)<sub>4<\/sub>O<sub>2<\/sub>, a novel oxophosphate with a shchurovskyite-type topology: synthesis, structure, magnetic properties and crystal chemistry of rubidium copper phosphates"],"prefix":"10.1107","volume":"75","author":[{"given":"Sergey M.","family":"Aksenov","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9003-3695","authenticated-orcid":true,"given":"Elena Yu.","family":"Borovikova","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7313-8279","authenticated-orcid":true,"given":"Vladimir S.","family":"Mironov","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Natalia A.","family":"Yamnova","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Anatoly S.","family":"Volkov","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Dmitry A.","family":"Ksenofontov","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Olga A.","family":"Gurbanova","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Olga V.","family":"Dimitrova","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9422-1925","authenticated-orcid":true,"given":"Dina V.","family":"Deyneko","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Elena A.","family":"Zvereva","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Olga V.","family":"Maximova","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8352-1394","authenticated-orcid":true,"given":"Sergey V.","family":"Krivovichev","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Peter C.","family":"Burns","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Alexander N.","family":"Vasiliev","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2019,9,25]]},"reference":[{"key":"ra5054_bb1","doi-asserted-by":"crossref","first-page":"16","DOI":"10.1016\/j.solidstatesciences.2016.11.003","volume":"63","author":"Aksenov","year":"2017","journal-title":"Solid State Sci."},{"key":"ra5054_bb2","doi-asserted-by":"crossref","first-page":"8252","DOI":"10.1021\/ja201096b","volume":"133","author":"Armstrong","year":"2011","journal-title":"J. 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