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The crystal structure of Ni\n                    <jats:sub>3<\/jats:sub>\n                    V\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>8<\/jats:sub>\n                    at 299\u2005(3)\u2005K and 1323\u2005(8)\u2005K was studied using X-ray powder diffraction. The sample was a single-phase orthorhombic kagome-staircase-Ni\n                    <jats:sub>3<\/jats:sub>\n                    (VO\n                    <jats:sub>4<\/jats:sub>\n                    )\n                    <jats:sub>2<\/jats:sub>\n                    -type structure (space group\n                    <jats:italic>Cmca<\/jats:italic>\n                    ) at both temperatures. The phase purity and morphology was studied using energy-dispersive X-ray spectroscopy and scanning electron microscopy. The refined unit-cell parameters at 299\u2005(3)\u2005K are\n                    <jats:italic>a<\/jats:italic>\n                    = 5.93384\u2005(4)\u2005\u00c5,\n                    <jats:italic>b<\/jats:italic>\n                    = 11.38318\u2005(7)\u2005\u00c5 and\n                    <jats:italic>c<\/jats:italic>\n                    = 8.23818\u2005(5)\u2005\u00c5, and at 1323\u2005(8)\u2005K are\n                    <jats:italic>a<\/jats:italic>\n                    \u00a0= 6.02077\u2005(7)\u2005\u00c5,\n                    <jats:italic>b<\/jats:italic>\n                    = 11.48838\u2005(7)\u2005\u00c5 and\n                    <jats:italic>c<\/jats:italic>\n                    = 8.32611\u2005(9)\u2005\u00c5. The obtained results indicate thermal expansion anisotropy, with a largest expansivity along\n                    <jats:bold>a<\/jats:bold>\n                    . Variations in Ni\u2014O and V\u2014O bonds with temperature are observed. The variation in the Ni\u2014O bond is about one order higher in magnitude than that of the V\u2014O bond, signifying the high rigidity of V\u2014O bonds. The unit-cell size variations with rising effective ionic volume of the divalent\n                    <jats:italic>A<\/jats:italic>\n                    ion in the\n                    <jats:italic>A<\/jats:italic>\n                    <jats:sub>3<\/jats:sub>\n                    <jats:italic>B<\/jats:italic>\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>8<\/jats:sub>\n                    family [\n                    <jats:italic>A<\/jats:italic>\n                    = Ni, Mg, Zn, Co, Mn (experimental data) and also\n                    <jats:italic>A<\/jats:italic>\n                    = Cu, Cd (theoretical data),\n                    <jats:italic>B<\/jats:italic>\n                    = V or As] are analyzed. Based on experimental and theoretical data, trends within the family are observed and the unit-cell size for reported solid solution of nickel (87%) and copper (13%) mixture in (Ni\n                    <jats:sub>\n                      1\u2013\n                      <jats:italic>x<\/jats:italic>\n                    <\/jats:sub>\n                    Cu\n                    <jats:sub>\n                      <jats:italic>x<\/jats:italic>\n                    <\/jats:sub>\n                    )\n                    <jats:sub>3<\/jats:sub>\n                    V\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>8<\/jats:sub>\n                    are predicted. Predictions are also provided for some hypothetical\n                    <jats:italic>A<\/jats:italic>\n                    <jats:sub>3<\/jats:sub>\n                    <jats:italic>B<\/jats:italic>\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>8<\/jats:sub>\n                    ternary compound and solid solutions.\n                  <\/jats:p>","DOI":"10.1107\/s2052520624006966","type":"journal-article","created":{"date-parts":[[2024,10,27]],"date-time":"2024-10-27T10:12:59Z","timestamp":1730023979000},"page":"715-723","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":2,"title":["Crystal structure of nickel orthovanadate (Ni\n                    <sub>3<\/sub>\n                    V\n                    <sub>2<\/sub>\n                    O\n                    <sub>8<\/sub>\n                    ) at 299\u2005(3)\u2005K and 1323\u2005(8)\u2005K: an X-ray diffraction study"],"prefix":"10.1107","volume":"80","author":[{"ORCID":"https:\/\/orcid.org\/0009-0001-3047-005X","authenticated-orcid":true,"given":"Fiza","family":"Aziz","sequence":"first","affiliation":[{"id":[{"id":"https:\/\/ror.org\/000sfad56","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6276-088X","authenticated-orcid":true,"given":"Wojciech","family":"Paszkowicz","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/000sfad56","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Roman","family":"Minikayev","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/000sfad56","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Christine","family":"Martin","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/01k40cz91","id-type":"ROR","asserted-by":"publisher"}],"department":["Laboratorie CHRISMAT"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Miroslaw","family":"Kozlowski","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/01bkj6835","id-type":"ROR","asserted-by":"publisher"}],"department":["Lukasiewicz Research Network"]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Henryk","family":"Teisseyre","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/000sfad56","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"329","published-online":{"date-parts":[[2024,10,23]]},"reference":[{"key":"dk5132_bb1","doi-asserted-by":"crossref","first-page":"136100","DOI":"10.1016\/j.chemosphere.2022.136100","volume":"308","author":"Arumugam","year":"2022","journal-title":"Chemosphere"},{"key":"dk5132_bb2","doi-asserted-by":"crossref","first-page":"457","DOI":"10.1107\/S0108768191002987","volume":"47","author":"Barbier","year":"1991","journal-title":"Acta Cryst. 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