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Both materials form three-dimensional frameworks. The crystal structures were determined using data from powder X-ray diffraction measurements. The purity and morphology of the compounds were studied by elemental analyses and SEM investigations, and their thermal stabilities were determined by thermogravimetric and nonambient powder X-ray diffraction measurements, which indicated that<jats:bold>1<\/jats:bold>is stable up to 537\u2005K and<jats:bold>2<\/jats:bold>is stable up to 437\u2005K.<\/jats:p>","DOI":"10.1107\/s205322961901180x","type":"journal-article","created":{"date-parts":[[2019,10,8]],"date-time":"2019-10-08T14:22:57Z","timestamp":1570544577000},"page":"1502-1508","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":2,"title":["Synthesis, crystal structure solution and characterization of two organic\u2013inorganic hybrid layered materials based on metal sulfates and 1,4-phenylenediamine"],"prefix":"10.1107","volume":"75","author":[{"given":"Anabel","family":"Gonzalez Guillen","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8769-8023","authenticated-orcid":true,"given":"Marcin","family":"Oszajca","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Katarzyna","family":"Luberda-Durna\u015b","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7083-1860","authenticated-orcid":true,"given":"Wieslaw","family":"Lasocha","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2019,10,8]]},"reference":[{"key":"lg3241_bb1","doi-asserted-by":"crossref","first-page":"768","DOI":"10.1107\/S0021889809025503","volume":"42","author":"Altomare","year":"2009","journal-title":"J. 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