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The complexes were characterized by elemental analyses and IR,<jats:sup>1<\/jats:sup>H NMR,<jats:sup>31<\/jats:sup>P NMR and electronic absorption spectroscopy. The crystal structures of dichlorido[1-diphenylphosphinoyl-1\u2032-(di-<jats:italic>tert<\/jats:italic>-butylphosphanyl)ferrocene-\u03ba<jats:sup>2<\/jats:sup><jats:italic>O<\/jats:italic>,<jats:italic>P<\/jats:italic>]cadmium(II), [CdCl<jats:sub>2<\/jats:sub>{(C<jats:sub>17<\/jats:sub>H<jats:sub>14<\/jats:sub>OP)(C<jats:sub>13<\/jats:sub>H<jats:sub>22<\/jats:sub>P)Fe}] or CdCl<jats:sub>2<\/jats:sub>(\u03ba<jats:sup>2<\/jats:sup><jats:italic>P<\/jats:italic>,<jats:italic>O<\/jats:italic>-dppOdtbpf) (<jats:bold>1<\/jats:bold>), bis[\u03bc-(<jats:italic>tert<\/jats:italic>-butyl)(1\u2032-diphenylphosphinoylferrocen-1-yl)phosphinato-\u03ba<jats:sup>3<\/jats:sup><jats:italic>O<\/jats:italic>,<jats:italic>O<\/jats:italic>\u2032:<jats:italic>O<\/jats:italic>\u2032\u2032]bis[chloridozinc(II)], [Zn<jats:sub>2<\/jats:sub>{(C<jats:sub>9<\/jats:sub>H<jats:sub>13<\/jats:sub>O<jats:sub>2<\/jats:sub>P)(C<jats:sub>17<\/jats:sub>H<jats:sub>14<\/jats:sub>OP)Fe}<jats:sub>2<\/jats:sub>Cl<jats:sub>2<\/jats:sub>] or [ZnOCl{\u03ba<jats:sup>2<\/jats:sup><jats:italic>O<\/jats:italic>,<jats:italic>O<\/jats:italic>\u2032-Ph<jats:sub>2<\/jats:sub>POFcPO<jats:sub>2<\/jats:sub>(<jats:italic>t<\/jats:italic>-Bu)}]<jats:sub>2<\/jats:sub>(<jats:bold>2<\/jats:bold>), 1,1\u2032-bis(di-<jats:italic>tert<\/jats:italic>-butylthiophosphinoyl)ferrocene, [Fe(C<jats:sub>13<\/jats:sub>H<jats:sub>22<\/jats:sub>PS)<jats:sub>2<\/jats:sub>] or dtbpfS<jats:sub>2<\/jats:sub>(<jats:bold>3<\/jats:bold>), and [1,1\u2032-bis(dicyclohexylphosphanyl)ferrocene-\u03ba<jats:sup>2<\/jats:sup><jats:italic>P<\/jats:italic>,<jats:italic>P<\/jats:italic>\u2032][chlorido\/cyanido(0.25\/1.75)]zinc(II), [Zn(CN)<jats:sub>1.75<\/jats:sub>Cl<jats:sub>0.25<\/jats:sub>{(C<jats:sub>17<\/jats:sub>H<jats:sub>26<\/jats:sub>P)<jats:sub>2<\/jats:sub>Fe}] or Zn(CN)<jats:sub>2<\/jats:sub>(\u03ba<jats:sup>2<\/jats:sup>-dcpf) (<jats:bold>4<\/jats:bold>), were determined crystallographically. Compound<jats:bold>1<\/jats:bold>has tetrahedral geometry in which the Cd<jats:sup>II<\/jats:sup>centre is coordinated by one dppOdtbpf ligand in a \u03ba<jats:sup>2<\/jats:sup>-manner and by two Cl atoms, while compound<jats:bold>2<\/jats:bold>displays a centrosymmetric dimeric unit in which two oxide atoms bridge the two Zn atoms to generate an eight-membered ring. Compound<jats:bold>3<\/jats:bold>revealed a sandwich structure with both phosphane groups sulfurized. In compound<jats:bold>4<\/jats:bold>, the Zn<jats:sup>II<\/jats:sup>atom adopts a tetrahedral geometry by coordinating to the 1,1\u2032-bis(dicyclohexylphosphanyl)ferrocene ligand in a \u03ba<jats:sup>2<\/jats:sup>-manner and to two cyanide ligands.<\/jats:p>","DOI":"10.1107\/s2053229621004162","type":"journal-article","created":{"date-parts":[[2021,4,26]],"date-time":"2021-04-26T14:10:24Z","timestamp":1619446224000},"page":"240-248","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":2,"title":["Transition-metal complexes of group 12 with 1,1\u2032-bis(phosphanyl)ferrocene ligands"],"prefix":"10.1107","volume":"77","author":[{"given":"Karan","family":"Chaudhary","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Manoj","family":"Trivedi","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Dhanraj T.","family":"Masram","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3109-9440","authenticated-orcid":true,"given":"Nigam P.","family":"Rath","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2021,4,26]]},"reference":[{"key":"yd3016_bb1","doi-asserted-by":"crossref","first-page":"235","DOI":"10.1016\/0022-328X(96)06137-2","volume":"516","author":"Abu-Gnim","year":"1996","journal-title":"J. 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