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In the case of [Pb(anti)\n                    <jats:sub>6<\/jats:sub>\n                    ](OTf)\n                    <jats:sub>2<\/jats:sub>\n                    , two polymorphic forms crystallizing in the monoclinic\n                    <jats:italic>I<\/jats:italic>\n                    2\/\n                    <jats:italic>a<\/jats:italic>\n                    (\n                    <jats:bold>1a<\/jats:bold>\n                    ) and triclinic\n                    <jats:italic>P<\/jats:italic>\n                    \\overline 1 (\n                    <jats:bold>1b<\/jats:bold>\n                    ) space groups were distinguished. [Pb(anti)\n                    <jats:sub>6<\/jats:sub>\n                    ](ClO\n                    <jats:sub>4<\/jats:sub>\n                    )\n                    <jats:sub>2<\/jats:sub>\n                    (\n                    <jats:bold>2<\/jats:bold>\n                    ) crystallized in the trigonal space group\n                    <jats:italic>P<\/jats:italic>\n                    \\overline 3. The crystal structures were determined by single-crystal X-ray diffraction. In all three structures, the metal ion is surrounded by six O atoms from the antipyrine molecules. Compounds\n                    <jats:bold>1a<\/jats:bold>\n                    and\n                    <jats:bold>2<\/jats:bold>\n                    display regular and holodirected octahedral geometry with three similar [2.496\u2005(1), 2.523\u2005(1) and 2.539\u2005(1)\u2005\u00c5] or six equivalent Pb\u2014O bond lengths [2.474\u2005(2)\u2005\u00c5]. Complex\n                    <jats:bold>1b<\/jats:bold>\n                    has lower hemidirected symmetry, forming a \u03c8-pentagonal bipyramid, with six different Pb\u2014O bond distances in the range 2.327\u2005(2)\u20132.852\u2005(2)\u2005\u00c5 and one position occupied by a lone electron pair. Shorter C\u2014H...O contacts in\n                    <jats:bold>1b<\/jats:bold>\n                    [2.998\u2005(4) and 3.141\u2005(4)\u2005\u00c5] compared to those in\n                    <jats:bold>1a<\/jats:bold>\n                    [3.354\u2005(2) and 3.365\u2005(2)\u2005\u00c5] and\n                    <jats:bold>2<\/jats:bold>\n                    [3.360\u2005(3) and 3.384\u2005(3)\u2005\u00c5] between the antipyrine molecules and the counter-ions seem to stabilize the active lone pair. In all three structures, the [Pb(anti)\n                    <jats:sub>6<\/jats:sub>\n                    ]\n                    <jats:sup>2+<\/jats:sup>\n                    cations organize into a hexagonal columnar packing, while the ordered counter-ions occupy the free cavities between them. Density functional theory (DFT) calculations reveal that the isolated [Pb(anti)\n                    <jats:sub>6<\/jats:sub>\n                    ]\n                    <jats:sup>2+<\/jats:sup>\n                    cation favours a distorted hemidirected geometry. The calculated eccentricity values [0.14 (\n                    <jats:bold>1b<\/jats:bold>\n                    ) and 0 (\n                    <jats:bold>1a<\/jats:bold>\n                    and\n                    <jats:bold>2<\/jats:bold>\n                    )] confirm the active and inert behaviour of the 6\n                    <jats:italic>s<\/jats:italic>\n                    <jats:sup>2<\/jats:sup>\n                    lone pair, respectively. The distribution of the Pb\u2014O bond lengths for the homoleptic lead(II) complexes with a PbO\n                    <jats:sub>6<\/jats:sub>\n                    core was presented. Correlations between Pb\u2014O bond lengths and cordination number (CN) for the selected lead(II) and lead(IV) complexes were analysed.\n                  <\/jats:p>","DOI":"10.1107\/s2053229626007333","type":"journal-article","created":{"date-parts":[[2026,7,27]],"date-time":"2026-07-27T11:21:32Z","timestamp":1785151292000},"page":"524-533","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":0,"title":["Structures of hexakis(antipyrine)lead(II) complexes: the first example of the stereochemically active and inactive 6\n                    <i>s<\/i>\n                    <sup>2<\/sup>\n                    lone pair for one lead(II) complex"],"prefix":"10.1107","volume":"82","author":[{"given":"Krzysztof","family":"\u0141yczko","sequence":"first","affiliation":[{"id":[{"id":"https:\/\/ror.org\/00w3hap50","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Monika","family":"\u0141yczko","sequence":"additional","affiliation":[{"id":[{"id":"https:\/\/ror.org\/00w3hap50","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"329","published-online":{"date-parts":[[2026,8,5]]},"reference":[{"key":"ux3016_bb1","doi-asserted-by":"crossref","first-page":"25806","DOI":"10.1021\/jacs.5c07547","volume":"147","author":"Acharyya","year":"2025","journal-title":"J. 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