{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,1,14]],"date-time":"2025-01-14T05:17:25Z","timestamp":1736831845690,"version":"3.33.0"},"reference-count":29,"publisher":"International Union of Crystallography (IUCr)","issue":"5","license":[{"start":{"date-parts":[[2016,4,29]],"date-time":"2016-04-29T00:00:00Z","timestamp":1461888000000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"},{"start":{"date-parts":[[2016,4,29]],"date-time":"2016-04-29T00:00:00Z","timestamp":1461888000000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Cryst Commun","Acta Cryst E","Acta Cryst Sect E","Acta Crystallogr E","Acta Crystallogr Sect E","Acta Cryst E Cryst Commun","Acta Cryst Sect E Cryst Commun"],"published-print":{"date-parts":[[2016,5,1]]},"abstract":"<jats:p>The crystal structures of the building block tetramethylammonium (2,2\u2032-bipyridine-\u03ba<jats:sup>2<\/jats:sup><jats:italic>N<\/jats:italic>,<jats:italic>N<\/jats:italic>\u2032)tetracyanidoferrate(III) trihydrate, [N(CH<jats:sub>3<\/jats:sub>)<jats:sub>4<\/jats:sub>][Fe(CN)<jats:sub>4<\/jats:sub>(C<jats:sub>10<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)]\u00b73H<jats:sub>2<\/jats:sub>O, (I), and a new two-dimensional cyanide-bridged bimetallic coordination polymer, poly[[(2,2\u2032-bipyridine-\u03ba<jats:sup>2<\/jats:sup><jats:italic>N<\/jats:italic>,<jats:italic>N<\/jats:italic>\u2032)di-\u03bc<jats:sub>2<\/jats:sub>-cyanido-dicyanido(\u03bc-ethylenediamine-\u03ba<jats:sup>2<\/jats:sup><jats:italic>N<\/jats:italic>:<jats:italic>N<\/jats:italic>\u2032)(ethylenediamine-\u03ba<jats:sup>2<\/jats:sup><jats:italic>N<\/jats:italic>,<jats:italic>N<\/jats:italic>\u2032)cadmium(II)iron(II)] monohydrate], [CdFe(CN)<jats:sub>4<\/jats:sub>(C<jats:sub>10<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)(C<jats:sub>2<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>]\u00b7H<jats:sub>2<\/jats:sub>O, (II), are reported. In the crystal of (I), pairs of [Fe(2,2\u2032-bipy)(CN)<jats:sub>4<\/jats:sub>]<jats:sup>\u2212<\/jats:sup>units (2,2\u2032-bipy is 2,2\u2032-bipyridine) are linked together through \u03c0\u2013\u03c0 stacking between the pyridyl rings of the 2,2\u2032-bipy ligands to form a graphite-like structure parallel to the<jats:italic>ab<\/jats:italic>plane. The three independent water molecules are hydrogen-bonded alternately with each other, forming a ladder chain structure with<jats:italic>R<\/jats:italic><jats:sub>4<\/jats:sub><jats:sup>4<\/jats:sup>(8) and<jats:italic>R<\/jats:italic><jats:sub>6<\/jats:sub><jats:sup>6<\/jats:sup>(12) graph-set ring motifs, while the disordered [N(CH<jats:sub>3<\/jats:sub>)<jats:sub>4<\/jats:sub>]<jats:sup>+<\/jats:sup>cations lie above and below the water chains, and the packing is stabilized by weak C\u2014H...O hydrogen bonds. The water chains are further linked with adjacent sheets into a three-dimensional network<jats:italic>via<\/jats:italic>O\u2014H...O hydrogen bonds involving the lattice water molecules and the N atoms of terminal cyanide groups of the [Fe(2,2\u2032-bipy)(CN)<jats:sub>4<\/jats:sub>]<jats:sup>\u2212<\/jats:sup>building blocks, forming an<jats:italic>R<\/jats:italic><jats:sub>4<\/jats:sub><jats:sup>4<\/jats:sup>(12) ring motif. Compound (II) features a two-dimensional {[Fe(2,2\u2032-bipy)(CN)<jats:sub>4<\/jats:sub>Cd(en)<jats:sub>2<\/jats:sub>]}<jats:sub><jats:italic>n<\/jats:italic><\/jats:sub>layer structure (en is ethylenediamine) extending parallel to (010) and constructed from {[Fe(2,2\u2032-bipy)(CN)<jats:sub>4<\/jats:sub>Cd(en)]}<jats:sub><jats:italic>n<\/jats:italic><\/jats:sub>chains interlinked by bridging en ligands at the Cd atoms. Classical O\u2014H...N and N\u2014H...O hydrogen bonds involving the lattice water molecule and N atoms of terminal cyanide groups and the N\u2014H groups of the en ligands are observed within the layers. The layers are further connected<jats:italic>via<\/jats:italic>\u03c0\u2013\u03c0 stacking interactions between adjacent pyridine rings of the 2,2\u2032-bipy ligands, completing a three-dimensional supramolecular structure.<\/jats:p>","DOI":"10.1107\/s2056989016006848","type":"journal-article","created":{"date-parts":[[2016,4,29]],"date-time":"2016-04-29T09:59:49Z","timestamp":1461923989000},"page":"741-746","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":0,"title":["Crystal structures of tetramethylammonium (2,2\u2032-bipyridine)tetracyanidoferrate(III) trihydrate and poly[[(2,2\u2032-bipyridine-\u03ba<sup>2<\/sup><i>N<\/i>,<i>N<\/i>\u2032)di-\u03bc<sub>2<\/sub>-cyanido-dicyanido(\u03bc-ethylenediamine)(ethylenediamine-\u03ba<sup>2<\/sup><i>N<\/i>,<i>N<\/i>\u2032)cadmium(II)iron(II)] monohydrate]"],"prefix":"10.1107","volume":"72","author":[{"given":"Songwuit","family":"Chanthee","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Wikorn","family":"Punyain","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Supawadee","family":"Namuangrak","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Kittipong","family":"Chainok","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2016,4,29]]},"reference":[{"key":"bg2584_bb1","doi-asserted-by":"crossref","first-page":"335","DOI":"10.1107\/S0021889804003528","volume":"37","author":"Allen","year":"2004","journal-title":"J. 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