{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,2,21]],"date-time":"2025-02-21T21:49:20Z","timestamp":1740174560906,"version":"3.37.3"},"reference-count":29,"publisher":"International Union of Crystallography (IUCr)","issue":"3","license":[{"start":{"date-parts":[[2017,2,17]],"date-time":"2017-02-17T00:00:00Z","timestamp":1487289600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"},{"start":{"date-parts":[[2017,2,17]],"date-time":"2017-02-17T00:00:00Z","timestamp":1487289600000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by\/2.0\/uk\/legalcode"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Cryst Commun","Acta Cryst E","Acta Cryst Sect E","Acta Crystallogr E","Acta Crystallogr Sect E","Acta Cryst E Cryst Commun","Acta Cryst Sect E Cryst Commun"],"published-print":{"date-parts":[[2017,3,1]]},"abstract":"<jats:p>The title diorganotin compound, [Sn(CH<jats:sub>3<\/jats:sub>)<jats:sub>2<\/jats:sub>(C<jats:sub>28<\/jats:sub>H<jats:sub>32<\/jats:sub>N<jats:sub>2<\/jats:sub>O<jats:sub>4<\/jats:sub>)], features a distorted SnC<jats:sub>2<\/jats:sub>NO<jats:sub>2<\/jats:sub>coordination geometry almost intermediate between ideal trigonal\u2013bipyramidal and square-pyramidal. The dianionic Schiff base ligand coordinates in a tridentate fashion<jats:italic>via<\/jats:italic>two alkoxide O and hydrazinyl N atoms; an intramolecular hydroxy-O\u2014H...N(hydrazinyl) hydrogen bond is noted. The alkoxy chain has an all-<jats:italic>trans<\/jats:italic>conformation, and to the first approximation, the molecule has local mirror symmetry relating the two Sn-bound methyl groups. Supramolecular layers sustained by imine-C\u2014H...O(hydroxy), \u03c0\u2013\u03c0 [between decyloxy-substituted benzene rings with an inter-centroid separation of 3.7724\u2005(13)\u2005\u00c5], C\u2014H...\u03c0(arene) and C\u2014H...\u03c0(chelate ring) interactions are formed in the crystal; layers stack along the<jats:italic>c<\/jats:italic>axis with no directional interactions between them. The presence of C\u2014H...\u03c0(chelate ring) interactions in the crystal is clearly evident from an analysis of the calculated Hirshfeld surface.<\/jats:p>","DOI":"10.1107\/s2056989017002365","type":"journal-article","created":{"date-parts":[[2017,2,16]],"date-time":"2017-02-16T13:15:29Z","timestamp":1487250929000},"page":"390-396","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":3,"title":["[<i>N<\/i>\u2032-(4-Decyloxy-2-oxidobenzylidene)-3-hydroxy-2-naphthohydrazidato-\u03ba<sup>3<\/sup><i>N<\/i>,<i>O<\/i>,<i>O<\/i>\u2032]dimethyltin(IV): crystal structure and Hirshfeld surface analysis"],"prefix":"10.1107","volume":"73","author":[{"given":"Siti Nadiah Binti Mohd","family":"Rosely","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Rusnah Syahila Duali","family":"Hussen","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"See Mun","family":"Lee","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Nathan R.","family":"Halcovitch","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mukesh M.","family":"Jotani","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1401-1520","authenticated-orcid":true,"given":"Edward R. 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