{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,1,14]],"date-time":"2025-01-14T09:44:13Z","timestamp":1736847853897,"version":"3.33.0"},"reference-count":18,"publisher":"International Union of Crystallography (IUCr)","issue":"4","license":[{"start":{"date-parts":[[2023,3,7]],"date-time":"2023-03-07T00:00:00Z","timestamp":1678147200000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"},{"start":{"date-parts":[[2023,3,7]],"date-time":"2023-03-07T00:00:00Z","timestamp":1678147200000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"}],"funder":[{"DOI":"10.13039\/501100000266","name":"Engineering and Physical Sciences Research Council","doi-asserted-by":"publisher","award":["DTG012 EP\/K503162-1"],"award-info":[{"award-number":["DTG012 EP\/K503162-1"]}],"id":[{"id":"10.13039\/501100000266","id-type":"DOI","asserted-by":"publisher"}]},{"name":"Swedish Foundation for Strategic Research","award":["EM-16-0039"],"award-info":[{"award-number":["EM-16-0039"]}]}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Cryst Commun","Acta Cryst E","Acta Cryst Sect E","Acta Crystallogr E","Acta Crystallogr Sect E","Acta Cryst E Cryst Commun","Acta Cryst Sect E Cryst Commun"],"accepted":{"date-parts":[[2023,2,27]]},"published-print":{"date-parts":[[2023,4,1]]},"abstract":"<jats:p>Single crystals of three novel transition-metal oxalates, dirubidium diaquadioxalatocobalt(II) dihydrate or dirubidium cobalt(II) bis(oxalate) tetrahydrate, Rb<jats:sub>2<\/jats:sub>[Co(C<jats:sub>2<\/jats:sub>O<jats:sub>4<\/jats:sub>)<jats:sub>2<\/jats:sub>(H<jats:sub>2<\/jats:sub>O)<jats:sub>2<\/jats:sub>]\u00b72H<jats:sub>2<\/jats:sub>O, (I), <jats:italic>catena<\/jats:italic>-poly[dirubidium [[dichloridocobalt(II)]-\u03bc-oxalato]] or dirubidium cobalt(II) dichloride oxalate, {Rb<jats:sub>2<\/jats:sub>[CoCl<jats:sub>2<\/jats:sub>(C<jats:sub>2<\/jats:sub>O<jats:sub>4<\/jats:sub>)]}<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (II), and poly[dipotassium [tri-\u03bc-oxalato-copper(II)dilithium] dihydrate] or dipotassium dilithium copper(II) tris(oxalate) dihydrate, {K<jats:sub>2<\/jats:sub>[Li<jats:sub>2<\/jats:sub>Cu(C<jats:sub>2<\/jats:sub>O<jats:sub>4<\/jats:sub>)<jats:sub>3<\/jats:sub>]\u00b72H<jats:sub>2<\/jats:sub>O}<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (III), have been grown under hydrothermal conditions and their crystal structures determined using single-crystal X-ray diffraction. The structure of (I) exhibits isolated octahedral [Co(C<jats:sub>2<\/jats:sub>O<jats:sub>4<\/jats:sub>)<jats:sub>2<\/jats:sub>(H<jats:sub>2<\/jats:sub>O)<jats:sub>2<\/jats:sub>] units, whereas (II) consists of <jats:italic>trans<\/jats:italic> chains of Co<jats:sup>2+<\/jats:sup> ions bridged by bidentate oxalato ligands and (III) displays a novel tri-periodic network of Li<jats:sup>+<\/jats:sup> and Cu<jats:sup>2+<\/jats:sup> ions linked by oxalato bridging ligands.<\/jats:p>","DOI":"10.1107\/s2056989023001822","type":"journal-article","created":{"date-parts":[[2023,3,7]],"date-time":"2023-03-07T08:16:59Z","timestamp":1678177019000},"page":"267-271","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":0,"title":["Syntheses and crystal structures of three novel oxalate coordination compounds: Rb<sub>2<\/sub>Co(C<sub>2<\/sub>O<sub>4<\/sub>)<sub>2<\/sub>\u00b74H<sub>2<\/sub>O, Rb<sub>2<\/sub>CoCl<sub>2<\/sub>(C<sub>2<\/sub>O<sub>4<\/sub>) and K<sub>2<\/sub>Li<sub>2<\/sub>Cu(C<sub>2<\/sub>O<sub>4<\/sub>)<sub>3<\/sub>\u00b72H<sub>2<\/sub>O"],"prefix":"10.1107","volume":"79","author":[{"given":"Rebecca","family":"Clulow","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-7048-3982","authenticated-orcid":true,"given":"Philip","family":"Lightfoot","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2023,3,7]]},"reference":[{"key":"wm5668_bb1","doi-asserted-by":"crossref","first-page":"3734","DOI":"10.1080\/00958972.2014.937340","volume":"67","author":"Baran","year":"2014","journal-title":"J. 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