{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,11,2]],"date-time":"2025-11-02T12:25:01Z","timestamp":1762086301068,"version":"build-2065373602"},"reference-count":20,"publisher":"International Union of Crystallography (IUCr)","issue":"4","license":[{"start":{"date-parts":[[2023,3,10]],"date-time":"2023-03-10T00:00:00Z","timestamp":1678406400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"},{"start":{"date-parts":[[2023,3,10]],"date-time":"2023-03-10T00:00:00Z","timestamp":1678406400000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Cryst Commun","Acta Cryst E","Acta Cryst Sect E","Acta Crystallogr E","Acta Crystallogr Sect E","Acta Cryst E Cryst Commun","Acta Cryst Sect E Cryst Commun"],"accepted":{"date-parts":[[2023,3,3]]},"published-print":{"date-parts":[[2023,4,1]]},"abstract":"<jats:p>The syntheses and crystal structures of four hydrothermally prepared organo\u2013zinc phosphites, <jats:italic>viz<\/jats:italic>. poly[[(2-amino-3-methylpyridine)-\u03bc<jats:sub>3<\/jats:sub>-phosphonato-zinc] hemihydrate], {[Zn(HPO<jats:sub>3<\/jats:sub>)(C<jats:sub>6<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)]\u00b70.5H<jats:sub>2<\/jats:sub>O}<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (I), poly[(2-amino-4-methylpyridine)-\u03bc<jats:sub>3<\/jats:sub>-phosphonato-zinc], [Zn(HPO<jats:sub>3<\/jats:sub>)(C<jats:sub>6<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)]<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (II), poly[(2-amino-5-methylpyridine)-\u03bc<jats:sub>3<\/jats:sub>-phosphonato-zinc], [Zn(HPO<jats:sub>3<\/jats:sub>)(C<jats:sub>6<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)]<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (III), and poly[bis(2-amino-4-methylpyridinium) [tetra-\u03bc<jats:sub>3<\/jats:sub>-phosphonato-trizinc] monohydrate], {(C<jats:sub>6<\/jats:sub>H<jats:sub>9<\/jats:sub>N<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>[Zn<jats:sub>3<\/jats:sub>(HPO<jats:sub>3<\/jats:sub>)<jats:sub>4<\/jats:sub>]\u00b7H<jats:sub>2<\/jats:sub>O}<jats:sub>\n                     <jats:italic>n<\/jats:italic>\n                  <\/jats:sub>, (IV), are described. Compounds (I)\u2013(III) are constructed from vertex-sharing ZnO<jats:sub>3<\/jats:sub>N tetrahedra (the organic molecule acting as a ligand) and HPO<jats:sub>3<\/jats:sub> pseudo pyramids in a 1:1 ratio to generate the same <jats:italic>motif<\/jats:italic> of infinite 4-ring `ladder' chains propagating in the [010], [101] and [100] directions, respectively, whereas (IV) consists of (010) layers of vertex-sharing ZnO<jats:sub>4<\/jats:sub> and HPO<jats:sub>3<\/jats:sub> units in a 3:4 ratio with the protonated organic molecule acting as a template. When an excess of HCl is used in the synthesis, the simple hydrated molecular salt, bis(2-amino-3-methylpyridinium) tetrachlorozincate monohydrate, (C<jats:sub>6<\/jats:sub>H<jats:sub>8<\/jats:sub>N<jats:sub>2<\/jats:sub>)<jats:sub>2<\/jats:sub>[ZnCl<jats:sub>4<\/jats:sub>]\u00b7H<jats:sub>2<\/jats:sub>O, (V), arises. Compounds (I)\u2013(V) feature extensive networks of hydrogen bonds, both classical (N\u2014H...O, N\u2014H...Cl, O\u2014H...O) and non-classical (C\u2014H...O, C\u2014H...Cl) in nature, which help to consolidate the extended structures.<\/jats:p>","DOI":"10.1107\/s2056989023002062","type":"journal-article","created":{"date-parts":[[2023,3,10]],"date-time":"2023-03-10T08:58:53Z","timestamp":1678438733000},"page":"272-279","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":2,"title":["Consistent zincophosphite 4-ring `ladder' chain structural motif with isomeric ligands"],"prefix":"10.1107","volume":"79","author":[{"given":"Stephen","family":"Wark","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Megan J.","family":"Lyons","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9527-6418","authenticated-orcid":true,"given":"Alexandra M. Z.","family":"Slawin","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2253-4866","authenticated-orcid":true,"given":"William T. A.","family":"Harrison","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"329","published-online":{"date-parts":[[2023,3,10]]},"reference":[{"key":"pk2681_bb1","first-page":"J28articlee202200732","author":"Chen","year":"2022","journal-title":"Chem. Eur."},{"key":"pk2681_bb2","doi-asserted-by":"crossref","first-page":"849","DOI":"10.1107\/S0021889812029111","volume":"45","author":"Farrugia","year":"2012","journal-title":"J. Appl. Cryst."},{"key":"pk2681_bb3","doi-asserted-by":"crossref","first-page":"1808","DOI":"10.1021\/ic0346127","volume":"43","author":"Gordon","year":"2004","journal-title":"Inorg. 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