{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,30]],"date-time":"2026-07-30T17:29:47Z","timestamp":1785432587722,"version":"3.56.0"},"reference-count":22,"publisher":"International Union of Crystallography (IUCr)","issue":"3","license":[{"start":{"date-parts":[[2024,2,8]],"date-time":"2024-02-08T00:00:00Z","timestamp":1707350400000},"content-version":"vor","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"},{"start":{"date-parts":[[2024,2,8]],"date-time":"2024-02-08T00:00:00Z","timestamp":1707350400000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"}],"funder":[{"DOI":"10.13039\/501100001843","name":"Science and Engineering Research Board","doi-asserted-by":"publisher","award":["EEQ\/2019\/000292"],"award-info":[{"award-number":["EEQ\/2019\/000292"]}],"id":[{"id":"10.13039\/501100001843","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["iucr.org","wiley.com","iucrj.org"],"crossmark-restriction":true},"short-container-title":["Acta Crystallogr E Cryst Commun","Acta Cryst E","Acta Cryst Sect E","Acta Crystallogr E","Acta Crystallogr Sect E","Acta Cryst E Cryst Commun","Acta Cryst Sect E Cryst Commun"],"accepted":{"date-parts":[[2024,2,3]]},"published-print":{"date-parts":[[2024,3,1]]},"abstract":"<jats:p>\n                    The title compound, (C\n                    <jats:sub>4<\/jats:sub>\n                    H\n                    <jats:sub>12<\/jats:sub>\n                    N)[V(C\n                    <jats:sub>12<\/jats:sub>\n                    H\n                    <jats:sub>8<\/jats:sub>\n                    N\n                    <jats:sub>4<\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    )O\n                    <jats:sub>2<\/jats:sub>\n                    ]\u00b7H\n                    <jats:sub>2<\/jats:sub>\n                    O, was synthesized\n                    <jats:italic>via<\/jats:italic>\n                    aerial oxidation on refluxing picolinohydrazide with ethyl picolinate followed by addition of V\n                    <jats:sup>IV<\/jats:sup>\n                    O(acac)\n                    <jats:sub>2<\/jats:sub>\n                    and diethylamine in methanol. It crystallizes in the triclinic crystal system in space group\n                    <jats:italic>P<\/jats:italic>\n                    \\overline{1}. In the complex anion, the dioxidovanadium(V) moiety exhibits a distorted square-pyramidal geometry. In the crystal, extensive hydrogen bonding links the water molecule to two complex anions and one diethylammonium ion. One of the CH\n                    <jats:sub>2<\/jats:sub>\n                    groups in the diethylamine is disordered over two sets of sites in a 0.7:0.3 ratio.\n                  <\/jats:p>","DOI":"10.1107\/s2056989024001166","type":"journal-article","created":{"date-parts":[[2024,2,8]],"date-time":"2024-02-08T10:00:58Z","timestamp":1707386458000},"page":"277-280","update-policy":"https:\/\/doi.org\/10.1107\/cm_01","source":"Crossref","is-referenced-by-count":0,"title":["Crystal structure of diethylammonium dioxido{\n                    <i>Z<\/i>\n                    )-\n                    <i>N<\/i>\n                    -[(pyridin-2-yl)carbonylazanidyl]pyridine-2-carboximidato}vanadate(1\u2212) monohydrate"],"prefix":"10.1107","volume":"80","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-8222-6182","authenticated-orcid":true,"given":"Bipul","family":"Mondal","sequence":"first","affiliation":[{"id":[{"id":"https:\/\/ror.org\/019wbnq12","id-type":"ROR","asserted-by":"publisher"}]}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"329","published-online":{"date-parts":[[2024,2,8]]},"reference":[{"key":"ev2002_bb23","unstructured":"Bruker (2016). 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