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A rapid and sensitive method was developed and validated for the simultaneous determination of 13 anticoagulant rodenticides (coumafuryl, pindone, valone, warfarin, coumatetralyl, coumachlor, diphacinone, dicumarol, chlorophacinone, bromadiolone, difenacoum, flocoumafen, and brodifacoum) in human blood by liquid chromatography\u2013tandem mass spectrometry. After liquid\u2013liquid extraction, the anticoagulant rodenticides were separated on an Eclipse Plus C18 column. Linearities were observed for each analyte in blood ranging from 0.5 to 50 ng\/mL, with correlation coefficients over 0.99. The limits of detection ranged from 0.01 to 0.2 ng\/mL, and the limits of quantification were 0.5 ng\/mL for all analytes. The intraday and interday precisions were &lt;15%, and accuracies ranged from 80.3% to 111.0%. This validated method with high sensitivity has been applied in three anticoagulant rodenticide poisoning cases and has been used successfully in monitoring blood concentrations for months.<\/jats:p>","DOI":"10.1111\/1556-4029.13613","type":"journal-article","created":{"date-parts":[[2018,5,3]],"date-time":"2018-05-03T22:54:57Z","timestamp":1525388097000},"page":"784-792","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Simultaneous Determination of 13 Anticoagulant Rodenticidesin Human Blood by Liquid Chromatography\u2013Tandem Mass Spectrometry and its Application in Three Poisoning Cases"],"prefix":"10.1111","volume":"63","author":[{"given":"Zheng","family":"Qiao","sequence":"first","affiliation":[{"name":"Department of Forensic Toxicology Institute of Forensic Science Ministry of Justice Shanghai Key Laboratory of Forensic Medicine No. 1347 West Guangfu Road Shanghai 200063 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