{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,6,29]],"date-time":"2026-06-29T20:20:32Z","timestamp":1782764432916,"version":"3.54.5"},"reference-count":17,"publisher":"Wiley","issue":"4","license":[{"start":{"date-parts":[[2025,5,6]],"date-time":"2025-05-06T00:00:00Z","timestamp":1746489600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":["onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Journal of Forensic Sciences"],"published-print":{"date-parts":[[2025,7]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>An explosion in an industrial filtering unit, resulting in a fatality, triggered a comprehensive forensic investigation. Sixteen pieces of evidentiary materials were collected from the scene of occurrence. The chemical residue at the explosion's origin was identified as 2\u2010IodoxyBenzoic Acid (IBX) using NMR spectroscopy. IBX's shock\u2010sensitive explosive nature became the focal point of the investigation. A comparative analysis, using the confirmed IBX as a reference standard, was conducted to detect its presence in other collected evidentiary materials. As no established methods for IBX analysis were available, novel high\u2010performance thin layer chromatography (HPTLC) and UV\u2013Vis spectroscopic techniques were developed and validated. The optimized HPTLC method, using a 9:1 ethyl acetate and methanol solvent system and UV visualization at 254\u2009nm, provided reliable Rf values for IBX identification. This was further supported by UV\u2013Vis spectroscopy, which confirmed the characteristic absorption patterns of IBX. The investigation successfully linked several evidence items to the explosion through the detection of IBX. This case underscores the complementary role of crime scene investigation and chemical analysis, where meticulous fieldwork combined with innovative laboratory techniques led to the resolution of the case. Furthermore, the development of a validated HPTLC method for IBX provides a valuable tool for future forensic investigations, enhancing the forensic community's capability to address similar incidents.<\/jats:p>","DOI":"10.1111\/1556-4029.70066","type":"journal-article","created":{"date-parts":[[2025,5,7]],"date-time":"2025-05-07T04:29:13Z","timestamp":1746592153000},"page":"1338-1347","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["From crime scene to laboratory: A case study of a comprehensive investigation into an <scp>IBX<\/scp>\u2010induced explosion"],"prefix":"10.1111","volume":"70","author":[{"ORCID":"https:\/\/orcid.org\/0009-0004-4171-180X","authenticated-orcid":false,"given":"Srikanth","family":"R. Veerabhadraiah","sequence":"first","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8562-6007","authenticated-orcid":false,"given":"Sachin Ashok","family":"Bhat","sequence":"additional","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2288-7792","authenticated-orcid":false,"given":"Vishwanath","family":"S. Vallabha","sequence":"additional","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6006-2025","authenticated-orcid":false,"given":"Anand N.","family":"Narayanappa","sequence":"additional","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Savitha","family":"Sujatha","sequence":"additional","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Muddaih","family":"Sujatha","sequence":"additional","affiliation":[{"name":"State Forensic Science Laboratory  Bengaluru India"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2025,5,6]]},"reference":[{"key":"e_1_2_9_2_1","doi-asserted-by":"publisher","DOI":"10.1002\/(SICI)1521\u20103773(20000103)39:1<44::AID\u2010ANIE44>3.0.CO;2\u2010L"},{"key":"e_1_2_9_3_1","doi-asserted-by":"publisher","DOI":"10.1021\/jo9824596"},{"key":"e_1_2_9_4_1","doi-asserted-by":"publisher","DOI":"10.1021\/ja00019a027"},{"issue":"29","key":"e_1_2_9_5_1","first-page":"3","article-title":"2\u2010Iodoxybenzoic acid","volume":"68","author":"Plumb JB","year":"1990","journal-title":"Chem Eng News Arch"},{"key":"e_1_2_9_6_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0950\u20104230(98)00062\u2010X"},{"key":"e_1_2_9_7_1","volume-title":"Chemical process safety: fundamentals with applications","author":"Crowl DA","year":"2001"},{"key":"e_1_2_9_8_1","doi-asserted-by":"publisher","DOI":"10.1002\/chin.200736067"},{"key":"e_1_2_9_9_1","doi-asserted-by":"publisher","DOI":"10.1055\/s\u20102003\u201041055"},{"key":"e_1_2_9_10_1","doi-asserted-by":"publisher","DOI":"10.1055\/s\u20102004\u2010834873"},{"key":"e_1_2_9_11_1","first-page":"1","volume-title":"Stabilized 2\u2010iodoxybenzoic acid (SIBX)","author":"Quideau S","year":"2012"},{"key":"e_1_2_9_12_1","first-page":"441","volume-title":"Forensic science handbook","author":"Midkiff CR","year":"2000"},{"key":"e_1_2_9_13_1","volume-title":"Forensic investigation of explosions","author":"Beveridge A","year":"2012"},{"key":"e_1_2_9_14_1","doi-asserted-by":"publisher","DOI":"10.1016\/s0039\u20109140(00)00546\u20104"},{"key":"e_1_2_9_15_1","volume-title":"Forensic and environmental detection of explosives","author":"Yinon J","year":"2012"},{"key":"e_1_2_9_16_1","first-page":"222","article-title":"The case of an ATM explosion","volume":"278","author":"Almeida MR","year":"2017","journal-title":"Forensic Sci Int"},{"key":"e_1_2_9_17_1","volume-title":"Forensic DNA typing: biology, technology, and genetics of STR markers","author":"Butler JM","year":"2005"},{"key":"e_1_2_9_18_1","doi-asserted-by":"publisher","DOI":"10.1002\/047084289X.rn00221"}],"container-title":["Journal of Forensic Sciences"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/pdf\/10.1111\/1556-4029.70066","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,7,3]],"date-time":"2025-07-03T06:12:35Z","timestamp":1751523155000},"score":1,"resource":{"primary":{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/10.1111\/1556-4029.70066"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2025,5,6]]},"references-count":17,"journal-issue":{"issue":"4","published-print":{"date-parts":[[2025,7]]}},"alternative-id":["10.1111\/1556-4029.70066"],"URL":"https:\/\/doi.org\/10.1111\/1556-4029.70066","archive":["Portico"],"relation":{},"ISSN":["0022-1198","1556-4029"],"issn-type":[{"value":"0022-1198","type":"print"},{"value":"1556-4029","type":"electronic"}],"subject":[],"published":{"date-parts":[[2025,5,6]]},"assertion":[{"value":"2025-02-08","order":0,"name":"received","label":"Received","group":{"name":"publication_history","label":"Publication History"}},{"value":"2025-04-22","order":2,"name":"accepted","label":"Accepted","group":{"name":"publication_history","label":"Publication History"}},{"value":"2025-05-06","order":3,"name":"published","label":"Published","group":{"name":"publication_history","label":"Publication History"}}]}}