{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,29]],"date-time":"2025-10-29T13:15:34Z","timestamp":1761743734052},"reference-count":15,"publisher":"Wiley","issue":"11","license":[{"start":{"date-parts":[[2013,4,18]],"date-time":"2013-04-18T00:00:00Z","timestamp":1366243200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Animal Science Journal"],"published-print":{"date-parts":[[2013,11]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>We improved the dry ash procedure for detecting titanium dioxide (<jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content>) in cattle feces containing chromium dioxide (<jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content>). First, the effect of amount of sodium sulfate (<jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content>) on the recovery of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> from cattle feces that contained <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content> was evaluated. Average recovery of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> at the 2.5\u2009g <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> level was significantly higher (<jats:italic>P<\/jats:italic>\u2009&lt;\u20090.0001) than that at 0.75\u2009g <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content>. Second, the effect of <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content> concentration on the recovery of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> of cattle feces by using two levels of <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> addition was examined. The recovery of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> decreased with the increase in the amount of <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content> at the 0.75\u2009g <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> level but was consistently high at 2.5\u2009g <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content>. Third, the recovery of <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content> from cattle feces was checked. The recoveries of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> and <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content> were high enough at the 2.5\u2009g <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> level. Fourth, the improved dry ash procedure (5\u2009mL of concentrated <jats:styled-content style=\"fixed-case\">H<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> and 2.5\u2009g of <jats:styled-content style=\"fixed-case\">Na<jats:sub>2<\/jats:sub>SO<jats:sub>4<\/jats:sub><\/jats:styled-content> were used for sample digestion) was compared to the wet ash procedure. Average recovery of <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> by the improved dry ash procedure was significantly higher (<jats:italic>P<\/jats:italic>\u2009=\u20090.0077) than that by the wet ash procedure. Thus, the improved dry ash procedure can be used for <jats:styled-content style=\"fixed-case\">TiO<jats:sub>2<\/jats:sub><\/jats:styled-content> analysis in cattle feces containing <jats:styled-content style=\"fixed-case\">Cr<jats:sub>2<\/jats:sub>O<jats:sub>3<\/jats:sub><\/jats:styled-content>.<\/jats:p>","DOI":"10.1111\/asj.12068","type":"journal-article","created":{"date-parts":[[2013,4,18]],"date-time":"2013-04-18T08:33:00Z","timestamp":1366273980000},"page":"726-731","source":"Crossref","is-referenced-by-count":7,"title":["An improved dry ash procedure for the detection of titanium dioxide in cattle feces"],"prefix":"10.1111","volume":"84","author":[{"given":"Hideyuki","family":"Ohmori","sequence":"first","affiliation":[{"name":"NARO Institute of Livestock and Grassland Science  Tsukuba Ibaraki Japan"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Itoko","family":"Nonaka","sequence":"additional","affiliation":[{"name":"NARO Kyushu Okinawa Agricultural Research Center  Koshi Kumamoto Japan"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Fumihiro","family":"Ohtani","sequence":"additional","affiliation":[{"name":"NARO Institute of Livestock and Grassland Science  Tsukuba Ibaraki Japan"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Kiyoshi","family":"Tajima","sequence":"additional","affiliation":[{"name":"NARO Institute of Livestock and Grassland Science  Tsukuba Ibaraki Japan"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Tomoyuki","family":"Kawashima","sequence":"additional","affiliation":[{"name":"Japan International Research Center for Agricultural Sciences  Tsukuba Ibaraki Japan"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yuji","family":"KAJI","sequence":"additional","affiliation":[{"name":"NARO Kyushu Okinawa Agricultural Research Center  Koshi Kumamoto 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