{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,3]],"date-time":"2026-10-03T09:48:41Z","timestamp":1791020921211,"version":"4.1.0"},"reference-count":44,"publisher":"Wiley","issue":"8","license":[{"start":{"date-parts":[[2012,3,6]],"date-time":"2012-03-06T00:00:00Z","timestamp":1330992000000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":["onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Int Endodontic J"],"published-print":{"date-parts":[[2012,8]]},"abstract":"<jats:sec><jats:label\/><jats:p><jats:bold>Camilleri J, Kralj P, Veber M, Sinagra E.<\/jats:bold> Characterization and analyses of acid\u2010extractable and leached trace elements in dental cements. <jats:italic>International Endodontic Journal<\/jats:italic>, <jats:bold>45<\/jats:bold>, 737\u2013743, 2012.<\/jats:p><\/jats:sec><jats:sec><jats:title>Abstract<\/jats:title><jats:p><jats:bold>Aims\u2002<\/jats:bold> Determination of the elemental constitution and investigation of the total and leachable arsenic, chromium and lead in Portland cement, pure tricalcium silicate, Biodentine, Bioaggregate and mineral trioxide aggregate (MTA) Angelus.<\/jats:p><jats:p><jats:bold>Methodology\u2002<\/jats:bold> The chemical composition of Portland cement, MTA Angelus, tricalcium silicate cement, Biodentine and Bioaggregate was determined using X\u2010ray fluorescence (XRF). Measurements of arsenic, lead and chromium were taken with inductively coupled plasma\u2010mass spectrometry (ICP\u2010MS), following acid digestion on the hydrated material and on leachates of cements soaked in Hank\u2019s balanced salt solution (HBSS).<\/jats:p><jats:p><jats:bold>Results\u2002<\/jats:bold> All the cements investigated had a similar oxide composition with the main oxide being calcium and silicon oxide. Both the Portland cement and MTA Angelus had an additional aluminium oxide. The dental cements included a radiopacifying material. All the materials tested had higher acid\u2010extractable arsenic content than the level set by ISO 9917\u20101 (2007) and an acceptable level of lead. Regardless these high levels of trace elements present in the materials, the leaching in HBSS was minimal for all the dental material tested in contrast to the high levels displayed by Portland cement.<\/jats:p><jats:p><jats:bold>Conclusions\u2002<\/jats:bold> Dental materials based on tricalcium silicate cement and MTA Angelus release minimal quantities of trace elements when in contact with simulated body fluids. The results of acid extraction could be affected by nonspecific matrix effects by the cement.<\/jats:p><\/jats:sec>","DOI":"10.1111\/j.1365-2591.2012.02027.x","type":"journal-article","created":{"date-parts":[[2012,3,6]],"date-time":"2012-03-06T19:14:37Z","timestamp":1331061277000},"page":"737-743","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":104,"title":["Characterization and analyses of acid\u2010extractable and leached trace elements in dental cements"],"prefix":"10.1111","volume":"45","author":[{"given":"J.","family":"Camilleri","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"P.","family":"Kralj","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"M.","family":"Veber","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"E.","family":"Sinagra","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2012,3,6]]},"reference":[{"key":"e_1_2_7_2_1","volume-title":"Heavy metals in cement and concrete resulting from the co\u2010incineration of wastes in cement kilns with regard to the legitimacy of waste utilisation","author":"Achternbosch M","year":"2003"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1747-4477.2004.tb00416.x"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2009.03.004"},{"key":"e_1_2_7_5_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2007.06.012"},{"key":"e_1_2_7_6_1","doi-asserted-by":"publisher","DOI":"10.1016\/0030-4220(81)90062-1"},{"key":"e_1_2_7_7_1","volume-title":"Active biosilicate technology\u2122, septodont","author":"Biodentine\u2122 Scientific file","year":"2010"},{"key":"e_1_2_7_8_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2008.12.018"},{"key":"e_1_2_7_9_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2005.08.009"},{"key":"e_1_2_7_10_1","unstructured":"British Standard Institution: Cement.Composition specifications and conformity criteria for common cements; BS EN 197\u20101: 2000"},{"key":"e_1_2_7_11_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2007.01248.x"},{"key":"e_1_2_7_12_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2007.01330.x"},{"key":"e_1_2_7_13_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2007.01370.x"},{"key":"e_1_2_7_14_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2009.01670.x"},{"key":"e_1_2_7_15_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2009.01621.x"},{"key":"e_1_2_7_16_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.dental.2004.05.010"},{"key":"e_1_2_7_17_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2005.01028.x"},{"key":"e_1_2_7_18_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2009.12.017"},{"key":"e_1_2_7_19_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2011.08.020"},{"key":"e_1_2_7_20_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2009.05.036"},{"key":"e_1_2_7_21_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.dental.2005.01.019"},{"key":"e_1_2_7_22_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2009.03.003"},{"key":"e_1_2_7_23_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2004.09.015"},{"key":"e_1_2_7_24_1","first-page":"3","article-title":"Antimicrobial and chemical study of MTA, Portland cement, calcium hydroxide paste, Sealapex and Dycal","volume":"11","author":"Estrela C","year":"2000","journal-title":"Brazilian Dental Journal"},{"key":"e_1_2_7_25_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0531-5565(97)00061-2"},{"key":"e_1_2_7_26_1","first-page":"43","article-title":"A comparative analysis of mineral trioxide aggregate and Portland cement","volume":"29","author":"Funteas UR","year":"2003","journal-title":"Australian Dental Journal"},{"key":"e_1_2_7_27_1","unstructured":"International Standards Organization.2007Dentistry\u2010 water based cements Part 1: powder\/liquid. Patent ISO EN 9917\u20101 2007."},{"key":"e_1_2_7_28_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2005.10.043"},{"key":"e_1_2_7_29_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2010.08.045"},{"key":"e_1_2_7_30_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2008.07.018"},{"key":"e_1_2_7_31_1","first-page":"34","volume-title":"Applications of admixtures in concrete","author":"Nagataki S","year":"1995"},{"key":"e_1_2_7_32_1","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2591.2010.01745.x"},{"key":"e_1_2_7_33_1","doi-asserted-by":"publisher","DOI":"10.1590\/S0103-64402007000100002"},{"key":"e_1_2_7_34_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2009.08.039"},{"key":"e_1_2_7_35_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2009.02.011"},{"key":"e_1_2_7_36_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2008.04.021"},{"key":"e_1_2_7_37_1","doi-asserted-by":"publisher","DOI":"10.1097\/01.DON.0000133155.04468.41"},{"key":"e_1_2_7_38_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2010.02.011"},{"key":"e_1_2_7_39_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0099-2399(99)80142-3"},{"key":"e_1_2_7_40_1","unstructured":"TorabinejadM WhiteDJ(1995)Tooth filling material and use. US Patent Number 5 769 638."},{"key":"e_1_2_7_41_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0099-2399(06)80967-2"},{"key":"e_1_2_7_42_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.tripleo.2009.07.037"},{"key":"e_1_2_7_43_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.dental.2007.02.006"},{"key":"e_1_2_7_44_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.joen.2007.06.016"},{"key":"e_1_2_7_45_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.biomaterials.2005.04.025"}],"container-title":["International Endodontic Journal"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1111%2Fj.1365-2591.2012.02027.x","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/pdf\/10.1111\/j.1365-2591.2012.02027.x","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2023,10,30]],"date-time":"2023-10-30T03:07:35Z","timestamp":1698635255000},"score":1,"resource":{"primary":{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/10.1111\/j.1365-2591.2012.02027.x"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2012,3,6]]},"references-count":44,"journal-issue":{"issue":"8","published-print":{"date-parts":[[2012,8]]}},"alternative-id":["10.1111\/j.1365-2591.2012.02027.x"],"URL":"https:\/\/doi.org\/10.1111\/j.1365-2591.2012.02027.x","archive":["Portico"],"relation":{},"ISSN":["0143-2885","1365-2591"],"issn-type":[{"value":"0143-2885","type":"print"},{"value":"1365-2591","type":"electronic"}],"subject":[],"published":{"date-parts":[[2012,3,6]]},"assertion":[{"value":"2012-03-06","order":2,"name":"published","label":"Published","group":{"name":"publication_history","label":"Publication History"}}]}}