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However, by comparing findings with mercury intrusion porosimetry (MIP), it becomes obvious that the imaged 3D volumes and 2D images do not sufficiently overlap at certain scales to allow a continuous quantification of the pore size distribution (PSD). This can be overcome by improving the resolution and increasing the measured volume. Furthermore, results show that the fibrous morphology of calcium\u2010silicate\u2010hydrates (C\u2010S\u2010H) phases is preserved during FIB\u2010nT. This is a requirement for characterisation of nano\u2010scale porosity. Finally, it was proven that the combination of FIB\u2010nT with energy\u2010dispersive X\u2010ray spectroscopy (EDX) data facilitates the phase segmentation of a 11 \u00d7 11 \u00d7 7.7\u00a0\u03bcm<jats:sup>3<\/jats:sup> volume of hydrated alite.<\/jats:p>","DOI":"10.1111\/jmi.13081","type":"journal-article","created":{"date-parts":[[2021,12,14]],"date-time":"2021-12-14T12:28:14Z","timestamp":1639484894000},"page":"102-107","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":6,"title":["Reconstruction of calcium silicate hydrates using multiple 2D and 3D imaging techniques: Light microscopy, \u03bc\u2010CT, SEM, FIB\u2010nT combined with EDX"],"prefix":"10.1111","volume":"286","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-6002-0829","authenticated-orcid":false,"given":"Florian","family":"Kleiner","sequence":"first","affiliation":[{"name":"F. A. 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