{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,3,24]],"date-time":"2026-03-24T11:45:52Z","timestamp":1774352752195,"version":"3.50.1"},"reference-count":54,"publisher":"Wiley","issue":"3","license":[{"start":{"date-parts":[[2022,12,30]],"date-time":"2022-12-30T00:00:00Z","timestamp":1672358400000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100002322","name":"Coordena\u00e7\u00e3o de Aperfei\u00e7oamento de Pessoal de N\u00edvel Superior","doi-asserted-by":"publisher","award":["CNPq\u2010PDI\u2010300564\/2019\u20108"],"award-info":[{"award-number":["CNPq\u2010PDI\u2010300564\/2019\u20108"]}],"id":[{"id":"10.13039\/501100002322","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Orthod Craniofacial Res"],"published-print":{"date-parts":[[2023,8]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:sec><jats:title>Objectives<\/jats:title><jats:p>White spot lesions (WSL) are prevalent in patients using orthodontic appliances. The presence of ion\u2010releasing compounds in the tooth\u2010appliance interface may limit enamel demineralization to control WSL incidence. Thus, this study aims to evaluate the mineral formation on SiNb\u2010containing experimental orthodontic resins and the influence of these fillers on the physicochemical and biological properties of developed materials.<\/jats:p><\/jats:sec><jats:sec><jats:title>Materials and Methods<\/jats:title><jats:p>The SiNb particles were synthesized via the sol\u2013gel route and characterized by their molecular structure and morphology. Photopolymerizable orthodontic resins were produced with a 75\u2009wt% Bis\u2010GMA\/25\u2009wt% TEGDMA and 10\u00a0wt%, 20\u2009wt%, or 30\u2009wt% addition of SiNb. A control group was formulated without SiNb. These resins were tested for their degree of conversion, softening in solvent, cytotoxicity in fibroblasts, flexural strength, shear bond strength (SBS), and mineral deposition.<\/jats:p><\/jats:sec><jats:sec><jats:title>Results<\/jats:title><jats:p>The addition of 10\u00a0wt% of SiNb did not impair the conversion of monomers, cytotoxicity, and flexural strength. All groups with SiNb addition presented similar softening in solvent. The presence of these particles did not affect the bond strength between metallic brackets and enamel, with SBS values ranging from 16.41 to 18.66\u2009MPa. The mineral deposition was observed for all groups.<\/jats:p><\/jats:sec><jats:sec><jats:title>Conclusion<\/jats:title><jats:p>The use of niobium silicate as filler particles in resins may be a strategy for the adhesion of orthodontic appliances. The 10\u00a0wt% SiNb concentration resulted in a material with suitable physicochemical and biological properties while maintaining the bond strength to tooth enamel and promoting mineral deposition.<\/jats:p><\/jats:sec>","DOI":"10.1111\/ocr.12628","type":"journal-article","created":{"date-parts":[[2022,12,19]],"date-time":"2022-12-19T10:10:17Z","timestamp":1671444617000},"page":"442-450","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Orthodontic resins loaded with niobium silicate particles: Impact of filler concentration on the physicochemical and biological properties"],"prefix":"10.1111","volume":"26","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-9723-7933","authenticated-orcid":false,"given":"Lucas Dalcin","family":"Pinto","sequence":"first","affiliation":[{"name":"Dental Materials Laboratory, School of Dentistry Universidade Federal do Rio Grande do Sul  Porto Alegre RS 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