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Adv."],"published-print":{"date-parts":[[2026,8,21]]},"abstract":"<jats:p>\n                    Halide double perovskite ferroelectrics have recently emerged as an environmentally friendly candidate in radiation detection, photovoltaics, and optoelectronic memory devices due to their unique spontaneous polarization and semiconductor properties. However, it is a huge challenge to achieve efficient carrier transport and high Curie temperature (\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    ) in double perovskite ferroelectrics, owing to the limitations of twisted frameworks and structural construction. Here, we present a high-\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    heterovalent metal solid solution double perovskite ferroelectric, (4Br2FBZ)\n                    <jats:sub>2<\/jats:sub>\n                    CsAgBiBr\n                    <jats:sub>7<\/jats:sub>\n                    (4Br2FBZ-CAB, 4Br2FBZ\u00a0=\u00a04-bromo-2-fluorobenzylammonium), through a strategy of cation-engineered symmetry regulation. The metal ions Ag and Bi transitioned from an alternating arrangement to a mixed-site solid solution pattern, effectively optimizing the electronic band structure to enhance carrier transport. Meanwhile, 4Br2FBZ-CAB exhibits a high\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    of 484\u00a0kelvin, substantially expanding the family of high-\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    lead-free ferroelectrics. Benefiting from its remarkable photoelectric and ferroelectric properties, a high self-powered x-ray detection sensitivity of 273.8 microcoulomb per gray per square centimeter (\u03bcC Gy\n                    <jats:sub>air<\/jats:sub>\n                    <jats:sup>\u22121<\/jats:sup>\n                    cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    ) was achieved at room temperature. In addition, this exceptionally high\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    enables the detector to operate self-powered at high temperatures, resulting in an excellent sensitivity of 896.9 \u03bcC Gy\n                    <jats:sub>air<\/jats:sub>\n                    <jats:sup>\u22121<\/jats:sup>\n                    cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    and a low detection limit of 13.9 nGy\n                    <jats:sub>air<\/jats:sub>\n                    s\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 425\u00a0kelvin. This work opens an avenue for expanding the family of high-\n                    <jats:italic toggle=\"yes\">T<\/jats:italic>\n                    <jats:sub>c<\/jats:sub>\n                    lead-free perovskite ferroelectrics with superior semiconducting properties.\n                  <\/jats:p>","DOI":"10.1126\/sciadv.aef7693","type":"journal-article","created":{"date-parts":[[2026,8,21]],"date-time":"2026-08-21T17:58:41Z","timestamp":1787335121000},"update-policy":"https:\/\/doi.org\/10.34133\/aaas_crossmark","source":"Crossref","is-referenced-by-count":0,"title":["Molecular-driven lead-free halide photoferroelectric solid solution for high-temperature sensitive self-powered x-ray detection"],"prefix":"10.1126","volume":"12","author":[{"ORCID":"https:\/\/orcid.org\/0009-0000-5636-889X","authenticated-orcid":true,"given":"Lijun","family":"Xu","sequence":"first","affiliation":[{"name":"State Key Laboratory of Functional Crystals and Devices, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian 350002, P.R. China."},{"name":"Fujian Science and Technology Innovation Laboratory for Optoelectronic Information of China, Fuzhou, Fujian 350108, P.R. China."},{"name":"University of Chinese Academy of Sciences, Chinese Academy of Sciences, Beijing 100049, P.R. China."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yao","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Functional Crystals and Devices, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian 350002, P.R. China."},{"name":"Fujian Science and Technology Innovation Laboratory for Optoelectronic Information of China, Fuzhou, Fujian 350108, P.R. China."},{"name":"University of Chinese Academy of Sciences, Chinese Academy of Sciences, Beijing 100049, P.R. China."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qianwen","family":"Guan","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Functional Crystals and Devices, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian 350002, P.R. China."},{"name":"Fujian Science and Technology Innovation Laboratory for Optoelectronic Information of China, Fuzhou, Fujian 350108, P.R. China."},{"name":"University of Chinese Academy of Sciences, Chinese Academy of Sciences, Beijing 100049, P.R. China."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hang","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Functional Crystals and Devices, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian 350002, P.R. 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