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The prepared CdIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FSEM), transmission electron microscopy (TEM), UV-visible diffuse reflectance spectroscopy (UV-Vis DRS), and N<jats:sub>2<\/jats:sub>-sorption techniques. Aqueous photocatalytic activity was evaluated by the decomposition of methyl orange under visible light irradiation. The results indicate that the prepared CdIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>has spherical morphology with mesoporous structure which can efficiently degrade methyl orange in water. 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