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The current study examines how substrate polarisation voltage affects the structural-mechanical relationships of WTiCN thin films made using a combination of HiPIMS and DCMS reactive sputtering. A chemical and structural study of the coatings conducted using EDS and XRD reveals the development of a composite phase structure. Additionally, the microstructure and morphology of the coating, as revealed by SEM and AFM, shows that defect-free surfaces are possible to obtain. Then, sliding (scratch and pin-on-disk) and indentation (nano-indentation) tests are used to examine the films\u2019 mechanical characteristics (hardness, adhesion, friction coefficient and wear rate). It shows that substrate polarisation voltage of \u221260\u2009V must be used to generate surfaces that are resistant to wear. The reason for this is the ideal levels of tungsten concentration (19\u2009at.%), root mean square surface roughness (4.5\u2009nm) and hardness (29\u2009GPa) have been reached. <\/jats:p>","DOI":"10.1177\/09544054231174976","type":"journal-article","created":{"date-parts":[[2023,5,17]],"date-time":"2023-05-17T09:09:57Z","timestamp":1684314597000},"page":"388-397","update-policy":"https:\/\/doi.org\/10.1177\/sage-journals-update-policy","source":"Crossref","is-referenced-by-count":0,"title":["Structural, mechanical and tribological properties of WCTiN coatings produced by HiPIMS"],"prefix":"10.1177","volume":"239","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-6483-1215","authenticated-orcid":false,"given":"Jos\u00e9","family":"Sanches","sequence":"first","affiliation":[{"name":"Department of Mechanical Engineering, University of Coimbra, CEMMPRE, ARISE, Coimbra, Portugal"}]},{"given":"F\u00e1bio","family":"Ferreira","sequence":"additional","affiliation":[{"name":"Department of 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