{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,8]],"date-time":"2026-07-08T03:06:24Z","timestamp":1783479984285,"version":"3.55.0"},"reference-count":42,"publisher":"SAGE Publications","issue":"8","license":[{"start":{"date-parts":[[2011,8,1]],"date-time":"2011-08-01T00:00:00Z","timestamp":1312156800000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/journals.sagepub.com\/page\/policies\/text-and-data-mining-license"}],"content-domain":{"domain":["journals.sagepub.com"],"crossmark-restriction":true},"short-container-title":["Appl Spectrosc"],"published-print":{"date-parts":[[2011,8]]},"abstract":"<jats:p>\n                    This paper introduces a new approach to analysis of spectra called asynchronous orthogonal sample design (AOSD). Specifically designed concentration series are selected according to mathematical analysis of orthogonal vectors. Based on the AOSD approach, the interfering portion of the spectra arising strictly from the concentration effect can be completely removed from the asynchronous spectra. Thus, two-dimensional (2D) asynchronous spectra can be used as an effective tool to characterize intermolecular interactions that lead to apparent deviations from the Beer\u2013Lambert law, even if the characteristic peaks of two compounds are substantially overlapped. A model solution with two solutes is used to investigate the behavior of the 2D asynchronous spectra under different extents of overlap of the characteristic peaks. Simulation results demonstrate that the resulting spectral patterns can reflect subtle spectral variations in bandwidths, peak positions, and absorptivities brought about by intermolecular interaction, which are barely visualized in the conventional one-dimensional (1D) spectra. Intermolecular interactions between butanone and dimethyl formamide (DMF) in CCl\n                    <jats:sub>4<\/jats:sub>\n                    solutions were investigated using the proposed AOSD approach to prove the applicability of the AOSD method in real chemical systems.\n                  <\/jats:p>","DOI":"10.1366\/11-06250","type":"journal-article","created":{"date-parts":[[2011,8,5]],"date-time":"2011-08-05T11:25:21Z","timestamp":1312543521000},"page":"901-917","update-policy":"https:\/\/doi.org\/10.1177\/sage-journals-update-policy","source":"Crossref","is-referenced-by-count":45,"title":["Asynchronous Orthogonal Sample Design Scheme for Two-Dimensional Correlation Spectroscopy (2D-COS) and its Application in Probing Intermolecular Interactions from Overlapping Infrared (IR) Bands"],"prefix":"10.1177","volume":"65","author":[{"given":"Xiaopei","family":"Li","sequence":"first","affiliation":[{"name":"College of Chemistry and Material Science, Hebei Normal University, Shijiazhuang, 050016, P.R. 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China (Y.Z.); Department of Chemistry, School of Science and Technology, Kwansei-Gakuin University, Sanda 669-1337, Japan (Y.O.); and The Procter &amp; Gamble Company, West Chester, Ohio 45069..."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qinghua","family":"Pan","sequence":"additional","affiliation":[{"name":"College of Chemistry and Material Science, Hebei Normal University, Shijiazhuang, 050016, P.R. China (X.L., C.L., Y.W.); Beijing National Laboratory for Molecular Sciences, State Key Laboratory for Rare Earth Materials Chemistry and Applications, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, P.R. China (X.L., J.C., S.L., A.H., Y.X., J.W.); Institute of Process Engineering, Chinese Academy of Sciences, 100190, P.R. China (K.H.); State Key Laboratory of Nuclear Physics and Technology, Institute of Heavy Ion Physics, School of Physics, Peking University, Beijing 100871, P.R. 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