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[1]Benzopyran and\npyridopyrimidine derivatives compose major classes of heterocyclic compounds, which have a\nwide spectrum of biological activities.<\/jats:p>\n<\/jats:sec>\n<jats:sec>\n<jats:title>Materials and Methods:<\/jats:title>\n<jats:p>In the present work, we report a facile and highly effective synthesis of 8-\naryl-8H-[1,3]dioxolo[4,5-g][1]benzopyran-6-carboxylic acids and 1,3-dimethyl-2,4-dioxo-5-\nphenyl-1,2,3,4,5,8-hexahydropyrido[2,3-d]pyrimidine-7-carboxylic acids via CdO NPs catalyzed\ncyclo condensation reaction of 4-substituted phenylmethylidenepyruvic acids with 3,4-\nmethylenedioxyphenol or 6-amino-1,3-dimethyluracil, which was accomplished under ethanoldrop\ngrinding at room temperature. The described catalyst was prepared successfully by a simple\nprecipitation method and characterized by the Fourier transformed infrared absorption (FT-IR)\nspectroscopy, X-Ray diffraction (XRD) analytical technique, and scanning electron microscopy\n(SEM).<\/jats:p>\n<\/jats:sec>\n<jats:sec>\n<jats:title>Results:<\/jats:title>\n<jats:p>A number of [1,3]dioxolo[g][1]benzopyran-6-carboxylic acids and pyrido[d]pyrimidine-\n7-carboxylic acids were effectively synthesized in high yields (96-98%) within short reaction\ntimes (10-15 min). All synthesized compounds were well-characterized by IR, 1H and 13C NMR\nspectroscopy, and also by elemental analyses.<\/jats:p>\n<\/jats:sec>\n<jats:sec>\n<jats:title>Conclusion:<\/jats:title>\n<jats:p>In summary, we have developed a very simple and impressive procedure for the\nsynthesis of 8-aryl-8H-[1,3]dioxolo[4,5-g][1]benzopyran-6-carboxylic acids and 1,3-dimethyl-\n2,4-dioxo-5-phenyl-1,2,3,4,5,8-hexahydropyrido[2,3-d]pyrimidine-7-carboxylic acids as\nbiologically interesting structures in the presence of CdO NPs as an efficient recyclable\nheterogeneous catalyst. The remarkable advantages for the offered protocol compared with\ntraditional methods are short reaction time, good yields of the products, and the ease of operation\nwith simple work-up procedure.<\/jats:p>\n<\/jats:sec>","DOI":"10.2174\/1386207323666200712145041","type":"journal-article","created":{"date-parts":[[2020,7,12]],"date-time":"2020-07-12T19:24:16Z","timestamp":1594581856000},"page":"139-147","update-policy":"https:\/\/doi.org\/10.2174\/bsp_crossmark_policy","source":"Crossref","is-referenced-by-count":5,"title":["Ethanol-Drop Grinding Approach: Cadmium Oxide Nanoparticles Catalyzed the Synthesis of [1,3]Dioxolo[g][1]benzopyran-6-carboxylic Acids and Pyrido[d]pyrimidine-7-carboxylic Acids"],"prefix":"10.2174","volume":"24","author":[{"given":"Saman","family":"Dahi-Azar","sequence":"first","affiliation":[{"name":"Department of Chemistry, Science and Research Branch, Islamic Azad University, P.O. 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