{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,27]],"date-time":"2026-10-27T01:29:08Z","timestamp":1793064548710,"version":"4.5.0"},"reference-count":68,"publisher":"The Angle Orthodontist (EH Angle Education & Research Foundation)","issue":"5","content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":[],"published-print":{"date-parts":[[2017,9]]},"abstract":"ABSTRACT<\/jats:title>\n \n Objective:<\/jats:title>\n The aim of this study was to develop an experimental orthodontic adhesive and evaluate how adding phosphate invert glass containing niobium pentoxide (PIG-Nb) affected the adhesive's properties.<\/jats:p>\n <\/jats:sec>\n \n Material and Methods:<\/jats:title>\n \n PIG-Nb was added at 1, 2.5, and 5 wt% to experimental adhesive (75 wt% bisphenol A methacrylate [BisGMA], 25 wt% triethylene glycol dimethacrylate [TEGDMA], 5 wt% colloidal silica and photoinitiator system). The adhesives were evaluated for mineral deposition, degree of conversion (DC), softening solvent by Knoop microhardness (KNH) variation, pH changes, and shear bond strength (SBS). One-way analysis of variance (ANOVA) (DC and \u0394KHN%), two-way ANOVA (SBS), repeated measures ANOVA (pH), and paired test (KNH1 and KNH2) were used at a significance level of\n P<\/jats:italic>\n < .05.\n <\/jats:p>\n <\/jats:sec>\n \n Results:<\/jats:title>\n Adding PIG-Nb to orthodontic adhesives induced deposition on its surface associated with a constant neutral pH. The SBS increased after immersion in artificial saliva, and the PIG-Nb5 exhibited less softening.<\/jats:p>\n <\/jats:sec>\n \n Conclusion:<\/jats:title>\n The addition of PIG-Nb into orthodontic adhesives induced mineral deposition. Experimental orthodontic adhesive containing 5% wt of PIG-Nb exhibited increased mineral deposition and suitable properties for orthodontic applications.<\/jats:p>\n <\/jats:sec>","DOI":"10.2319\/122417-140.1","type":"journal-article","created":{"date-parts":[[2017,7,7]],"date-time":"2017-07-07T11:11:34Z","timestamp":1499425894000},"page":"759-765","source":"Crossref","is-referenced-by-count":36,"title":["Niobium pentoxide phosphate invert glass as a mineralizing agent in an experimental orthodontic adhesive"],"prefix":"10.2319","volume":"87","author":[{"given":"Alinne Segatto Pires","family":"Altmann","sequence":"first","affiliation":[{"name":"Master's student, Dental Materials Laboratory, School of Dentistry, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fabricio Mezzomo","family":"Collares","sequence":"additional","affiliation":[{"name":"Associate Professor, Dental Materials Laboratory, School of Dentistry, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Gabriela de Souza","family":"Balbinot","sequence":"additional","affiliation":[{"name":"Master's student, Dental Materials Laboratory, School of Dentistry, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Vicente Castelo Branco","family":"Leitune","sequence":"additional","affiliation":[{"name":"Associate Professor, Dental Materials Laboratory, School of Dentistry, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Antonio Shigueaki","family":"Takimi","sequence":"additional","affiliation":[{"name":"Associate Professor, School of Metalurgic Engineering, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Susana Maria Werner","family":"Samuel","sequence":"additional","affiliation":[{"name":"Professor and Chair, Dental Materials Laboratory, School of Dentistry, Universidade Federal do Rio Grande do Sul, Porto Alegre, Brazil."}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"1164","reference":[{"key":"i0003-3219-87-5-759-b01","series-title":"Angle Orthod","first-page":"65","article-title":"Decalcification in relation to brackets bonded with glass ionomer cement or a resin adhesive","volume":"69","author":"Millett \n DT,","year":"1999","unstructured":"Millett \n DT, \n \n \n Nunn \n JH, \n \n \n Welbury \n RR, \n \n \n Gordon \n PH. \n \n \n Decalcification in relation to brackets bonded with glass ionomer cement or a resin adhesive. 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Mineral deposition at dental adhesive resin containing niobium pentoxide. Appl Adhes Sci. 2014;2:22. doi: 10.1186\/s40563-014-0022-0."},{"key":"i0003-3219-87-5-759-b11","series-title":"J Mater Sci","first-page":"4632","article-title":"Microwave synthesis and properties of NaPO3\u2013SnO\u2013Nb2O5 glasses","volume":"47","author":"Chenu \n S,","year":"2012","unstructured":"Chenu \n S, \n \n \n Lebullenger \n R, \n \n \n Rocherull\u00e9 \n J. \n \n \n Microwave synthesis and properties of NaPO3\u2013SnO\u2013Nb2O5 glasses. 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An in vitro study","volume":"81","author":"Brown \n ML,","year":"2011","unstructured":"Brown \n ML, \n \n \n Davis \n HB, \n \n \n Tufekci \n E, \n \n \n Crowe \n JJ, \n \n \n Covell \n DA, \n \n \n Mitchell \n JC. \n \n \n Ion release from a novel orthodontic resin bonding agent for the reduction and\/or prevention of white spot lesions. An in vitro study. 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Angle Orthod. 1999;69:65\u201370."},{"issue":"suppl","key":"i0003-3219-87-5-759-b02","series-title":"Am J Orthod Dentofac Orthop","first-page":"S56","article-title":"The evolution of bonding in orthodontics","volume":"147","author":"Gange \n P.","year":"2015","unstructured":"Gange \n P. \n \n \n The evolution of bonding in orthodontics. Am J Orthod Dentofac Orthop2015;147(suppl):S56\u2013S63. doi: 10.1016\/j.ajodo.2015.01.011."},{"key":"i0003-3219-87-5-759-b03","series-title":"Clin Oral Invest","first-page":"93","article-title":"In vitro antibacterial and remineralizing effect of adhesive containing triazine and niobium pentoxide phosphate inverted glass","volume":"21","author":"Altmann \n AS,","year":"2017","unstructured":"Altmann \n AS, \n \n \n Collares \n FM, \n \n \n Leitune \n VC, \n \n \n Arthur \n RA, \n \n \n Takimi \n AS, \n \n \n Samuel \n SM. \n \n \n In vitro antibacterial and remineralizing effect of adhesive containing triazine and niobium pentoxide phosphate inverted glass. Clin Oral Invest. 2017;21:93\u2013103. doi: 10.1007\/s00784-016-1754."},{"key":"i0003-3219-87-5-759-b04","series-title":"J Dent","first-page":"79","article-title":"Bonding performance of experimental bioactive\/biomimetic self-etch adhesives doped with calcium-phosphate fillers and biomimetic analogs of phosphoproteins","volume":"52","author":"Abuna \n G,","year":"2016","unstructured":"Abuna \n G, \n \n \n Feitosa \n VP, \n \n \n Correr \n AB, \n \n et al. \n Bonding performance of experimental bioactive\/biomimetic self-etch adhesives doped with calcium-phosphate fillers and biomimetic analogs of phosphoproteins. J Dent. 2016;52:79\u201386. doi: 10.1016\/j.jdent.2016.07.016."},{"key":"i0003-3219-87-5-759-b05","series-title":"Angle Orthod","first-page":"97","article-title":"A novel biomimetic orthodontic bonding agent helps prevent white spot lesions adjacent to brackets","volume":"83","author":"Manfred \n L,","year":"2013","unstructured":"Manfred \n L, \n \n \n Covell \n DA, \n \n \n Crowe \n JJ, \n \n et al. \n A novel biomimetic orthodontic bonding agent helps prevent white spot lesions adjacent to brackets. 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